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US3620979A Expired / Lapsed US ⏱️ 0.0 years remaining

Process of forming free-flowing, particulate mixtures of phosphates and silicates

Assignee: FMC Corp
•
Filing: 1968-04-24
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Granted: 1971-11-16
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Expires: 1988-04-24
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Abstract

Abstract Free-flowing, fast-dissolving, completely soluble, strong, granular particles containing a mixture of a hydratable alkali metal phosphate and an alkali metal silicate wherein the SiO2 to said phosphate mole ratio is at least 1:1, were produced by maintaining the alkali metal phosphate at a temperature of 60* to 100* C., gradually adding an aqueous solution of alkali metal silicate to the alkali metal phosphate, continually evaporating water from the resulting mixture, controlling the rate of addition of the alkali metal silicate solution so that the resulting mixture is maintained in the form of discrete particles, continuing said alkali metal silicate addition until the discrete, granular particles have an SiO2 to said phosphate mole ratio of at least 1:1, and recovering dry-appearing, granular particles which yield a pH of at least 10.5 in an aqueous 1 percent solution.

Inventors

  • 👤 Duncan Simmons Corliss
  • 👤 Russell Raymond Keast
  • 👤 Saxman Richard Lewis

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-10-26 17:16
CPC Classifications
C; C11; C11D; C11D11/00; B; B01; B01J; B01J2/00; B01J2/30; C11D3/00; C11D3/02; C11D3/04; C11D3/06; C11D3/08

Claims Analysis

Total Claims: 7
Claim 1
Independent Claim 20 words
Process of claim 1 wherein said temperature of said resulting mixture is maintained between about 60* to about 70* C.
Claim 2
Dependent Claim 10 words
Process of claim 1 wherein said phosphate is sodium tripolyphosphate.
Claim 3
Dependent Claim 10 words
Process of claim 1 wherein said phosphate is tetrasodium pyrophosphate.
Claim 4
Dependent Claim 10 words
Process of claim 1 wherein said phosphate is trisodium orthophosphate.
Claim 5
Dependent Claim 21 words
Process of claim 1 wherein said aqueous, alkali metal silicate solution has an SiO2/Na2O weight ratio of about 2.00:1 or below.
Claim 6
Dependent Claim 19 words
Process of claim 1 wherein the viscosity of said alkali metal silicate solution is reduced by adding water thereto.
Claim 7
Dependent Claim 18 words
Process of claim 1 wherein said dry-appearing, granular particles have a size of about -10 to +80 mesh.

References Cited (Backward Citations)

US2909490A Cited
US3390093A Cited

USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1974-11-15 1975-05-17 1975-11-16 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 1978-11-15 1979-05-17 1979-11-16 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 1982-11-15 1983-05-17 1983-11-16 $7700.00 Window Closed / Lapsed

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