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US3607115A Expired / Lapsed US ⏱️ 0.0 years remaining

Crystal pulling from molten melts including solute introduction means below the seed-melt interface

Assignee: Motors Liquidation Co
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Filing: 1969-10-29
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Granted: 1971-09-21
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Expires: 1989-10-29
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Abstract

Abstract An apparatus and method are disclosed for growing crystals from a melt of a molten solvent metal that is saturated with a solute. Heat is withdrawn through a seed contacting the surface of the melt to precipitate the solute onto said seed at the seed-melt interface. The seed is pulled away from the melt at a rate commensurate with the precipitation rates. Simultaneously, more solute is dissolved into the melt from a solute source in the melt beneath the growth interface while maintaining a close source-growth interface spacing substantially constant.

Inventors

  • 👤 Carl E Bleil

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-10-25 13:48
CPC Classifications
C; C30; C30B; C30B29/00; C30B29/02; C30B29/06; C30B15/00; C30B15/06; C30B29/08; Y; Y10; Y10T; Y10T117/00; Y10T117/10; Y10T117/1024; Y10T117/1032; Y10T117/1036; Y10T117/1044; Y10T117/1048

Claims Analysis

Total Claims: 5
Claim 1
Independent Claim 87 words
The apparatus for growing crystalline bodies as defined in claim 1 wherein means is provided for maintaining the surface of the melt at a substantially constant level during crystal growth, and the solute introducing means is an immovably supported, substantially closed container within the melt having a surface portion under the seed-melt contact interface, the surface portion is generally parallel to and within about one-eighth inch below the seed-melt interface, and the surface portion has a porous opening therein through which solute diffuses to the seed-melt interface.
Claim 2
Independent Claim 200 words
An apparatus for horizontally grooving a crystalline ribbonlike body which comprises means for containing a liquid melt of a solvent metal and a solute, means for maintaining said melt at a selected temperature, means for maintaining said melt at a substantially constant level, means for horizontally holding a crystalline seed with one end in contact with said melt, means for removing the heat of fusion from said one end of said seed to produce progressive precipitation of said solute on said one end, means for suppressing the net loss of the heat of fusion from the balance of said seed contacting said melt to regulate progressive precipitation of said solute thereon, a substantially closed solute container means disposed within the melt container and having a surface portion generally parallel to and within about one-eighth inch below said melt level, a porous opening in said surface portion through which solute passes to substantially continuously introduce solute into said melt under said seed-melt contact region, and means for horizontally pulling said seed away from said melt at a rate commensurate with the rate of progressive solute precipitation on said one end thereof to thereby produce a flat crystalline ribbon of predetermined thickness.
Claim 3
Dependent Claim 52 words
The apparatus for horizontally growing a crystalline ribbonlike body as defined in claim 3 wherein the surface portion of the solute container is generally flat and includes a thin wall and the porous opening in said flat surface portion is at least one slot lying transverse to the direction of crystal pull.
Claim 4
Dependent Claim 39 words
The apparatus for horizontally growing a crystalline ribbonlike body as defined in claim 3 wherein the surface portion of the solute container is generally flat and includes a thin porous sheet through which the solute diffuses into the melt.
Claim 5
Dependent Claim 43 words
The apparatus for horizontally growing a crystalline ribbonlike body as defined in claim 3 wherein the surface portion of the solute container under the seed-melt contact interface is grooved in the direction of crystal pull to produce a ribbon of predetermined cross section.

USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1974-09-20 1975-03-22 1975-09-21 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 1978-09-20 1979-03-22 1979-09-21 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 1982-09-20 1983-03-22 1983-09-21 $7700.00 Window Closed / Lapsed

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