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Ceramic-metal bonding composition and composite article of manufacture

Assignee: General Electric Co
•
Filing: 1968-11-14
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Granted: 1971-08-10
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Expires: 1988-11-14
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Abstract

Abstract An improved seal or bond between a refractory metal body and a translucent alumina ceramic body is disclosed wherein the metal surface to be bonded to the alumina body is comprised of zirconium, either as a metallic coating thereon, diffused therein by ''''metalliding,'''' as an alloying constituent, or as the major constituent of the metal body. The bond is effected by means of an alumina glass between the zirconium present at the surface and the adjoining alumina ceramic surface, at least a portion of the zirconium being oxidized by the molten glass during the formation of the seal.

Inventors

  • 👤 Paul J Jorgensen

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-11-03 20:47
CPC Classifications
C; C04; C04B; C04B37/00; C04B37/02; C04B37/023; C04B37/025; H; H01; H01J; H01J61/00; H01J61/02; H01J61/36; C04B2237/00; C04B2237/02; C04B2237/04; C04B2237/06; C04B2237/10; C04B2237/30; C04B2237/32; C04B2237/34; C04B2237/343; C04B2237/40; C04B2237/403; C04B2237/50; C04B2237/61; C04B2237/70; C04B2237/706; C04B2237/72; C04B2237/76; C04B2237/765; C04B2237/88; Y; Y10; Y10T; Y10T428/00; Y10T428/24

Claims Analysis

Total Claims: 12
Claim 1
Independent Claim 34 words
A ceramic-to-metal seal formed of a refractory metal body joined to a ceramic body by a sealing glass and wherein the metal-to-sealing glass interface comprises metallic zirconium and a sealing glass zirconium dioxide mixture.
Claim 2
Dependent Claim 34 words
A ceramic-to-metal seal formed of a refractory metal body joined to a ceramic body by a sealing glass and wherein the metal-to-sealing glass interface comprises metallic zirconium and a sealing glass zirconium dioxide mixture.
Claim 3
Dependent Claim 15 words
The seal recited in claim 1 wherein said sealing glass is composed primarily of alumina.
Claim 4
Dependent Claim 41 words
The seal recited in claim 1 wherein said refractory metal is selected from the group consisting of niobium, niobium alloyed with a small but effective amount of zirconium, zirconium and zirconium containing a small but effective amount of a stabilizing element.
Claim 5
Dependent Claim 13 words
The seal recited in claim 1 wherein said refractory metal body is niobium.
Claim 6
Dependent Claim 22 words
The seal recited in claim 1 wherein said refractory metal body is niobium alloyed with a small but effective amount of zirconium.
Claim 7
Dependent Claim 21 words
The seal recited in claim 1 wherein said refractory metal body is niobium having zirconium diffused therein at the metal-glass interface.
Claim 8
Dependent Claim 13 words
The seal recited in claim 1 wherein said refractory metal body is zirconium.
Claim 9
Dependent Claim 23 words
The seal recited in claim 1 wherein said refractory metal body is zirconium containing a small but effective amount of a stabilizing element.
Claim 10
Dependent Claim 21 words
The seal recited in claim 1 wherein said ceramic body is a polycrystalline alumina composed of at least 99.5 percent alumina.
Claim 11
Dependent Claim 15 words
The seal recited in claim 1 wherein said sealing glass is composed predominantly of alumina.
Claim 12
Dependent Claim 32 words
The ceramic-to-metal seal recited in claim 1 wherein said ceramic body comprises a polycrystalline ceramic body and said sealing glass mixture comprises a composition consisting essentially of zirconium dioxide and aluminA glass.

References Cited (Backward Citations)

GB779819A Cited
US2918596A Cited
US3138228A Cited
US3281174A Cited
US3385463A Cited
US3473071A Cited
US3389215A Cited
US3425116A Cited
US3441421A Cited
US3448319A Cited
US3473999A Cited

USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1974-08-09 1975-02-08 1975-08-10 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 1978-08-09 1979-02-08 1979-08-10 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 1982-08-09 1983-02-08 1983-08-10 $7700.00 Window Closed / Lapsed

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