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Apparatus for determining crystalization temperature

Assignee: Monsanto Co
•
Filing: 1967-12-26
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Granted: 1971-05-04
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Expires: 1987-12-26
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Abstract

Abstract Method and apparatus for automatically determining the crystallization temperature of a flowing liquid. Temperature control means are adapted to vary the liquid viscosity within a crystallization zone. Changes in flow or pressure drop caused by the viscosity changes provide the basis for temperature control. Because operation of the system is cyclic, the effects of heat of crystallization of the liquid can be observed on a recording of crystallization zone temperature, thus identifying the crystallization temperature.

Inventors

  • 👤 Joseph Bertoglio
  • 👤 Philip L Deming
  • 👤 Joyce G Eckert
  • 👤 James R Shafer

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-10-30 12:39
CPC Classifications
G; G01; G01N; G01N25/00; G01N25/02; G01N25/04

Claims Analysis

Total Claims: 5
Claim 1
Independent Claim 62 words
Apparatus for determining the crystallization temperature of a flowing liquid comprising: a. conduit means adapted to house said flowing liquid; b. a crystallization member within said conduit means; c. viscosity sensing means responsive to viscosity changes within said crystallization member; d. liquid temperature control means cooperating with said viscosity sensing means; and e. temperature indicating means adapted to monitor crystallization zone temperature.
Claim 2
Dependent Claim 69 words
Apparatus for determining the crystallization temperature of a flowing liquid comprising: a. a sidestream conduit communicating with a process stream; b. sidestream flow control means within said conduit; c. a crystallization member within said conduit; d. viscosity sensing means responsive to viscosity changes within said crystallization member; e. liquid temperature control means cooperating with said viscosity sensing means; and f. temperature indicating means adapted to monitor crystallization zone temperature.
Claim 3
Dependent Claim 13 words
An apparatus of claim 1 wherein the viscosity sensing means is a flowmeter.
Claim 4
Dependent Claim 15 words
An apparatus of claim 1 wherein the viscosity sensing means is a differential pressure meter.
Claim 5
Dependent Claim 16 words
An apparatus of claim 2 wherein the crystallization member is a coil of temperature controlled tubing.

References Cited (Backward Citations)

US2997874A Cited
US2885885A Cited
US3143876A Cited

USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1974-05-03 1974-11-02 1975-05-04 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 1978-05-03 1978-11-02 1979-05-04 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 1982-05-03 1982-11-02 1983-05-04 $7700.00 Window Closed / Lapsed

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