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US3341645A Expired / Lapsed US ⏱️ 0.0 years remaining

Method of producing viscose rayon staple and a spinning apparatus for use in the method

Assignee: Teijin Ltd
•
Filing: 1964-02-26
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Granted: 1967-09-12
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Expires: 1984-02-26
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Abstract

No abstract record available.

Inventors

  • 👤 Horiuchi Soichiro
  • 👤 Hashimoto Junichi
  • 👤 Wakabayashi Kanji
  • 👤 Yamada Kazuhiko
  • 👤 Masunaga Eiji
  • 👤 Kishimoto Isamu

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-10-31 13:01
CPC Classifications
D; D01; D01D; D01D5/00; D01D5/06; D01D4/00; D01F; D01F2/00; D01F2/06; D01F2/08

Claims Analysis

Total Claims: 2
Claim 1
Independent Claim 271 words
METHOD OF PRODUCING A VISCOSE FIBERS COMPRISING EXTRUDING A VISCOSE HAVING A GAMMA VALUE OF AT LEAST 60 AND CONTAINING BETWEEN 4% AND 7% BY WEIGHT OF A CELLULOSE COMPONENT HAVING A DEGREE OF POLYMERIZATION OF AT LEAST 500 AND BETWEEN 3% AND 6% BY WEIGHT OF SODIUM HYDROXIDE THROUGH AN ANNULAR SPINNERET PROVIDED WITH A CHANNEL AT ABOUT ITS CENTER, WITH AT LEAST 10,000 ORIFICES AROUND THE CHANNEL AT A TEMPERATURE NOT HIGHER THAN 30* C. INTO A COAGULATION BATH CONTAINING NOT MORE THAN 30 G./L. OF SULPHURIC ACID, AT LEAST 0.1 G./L. OF ANHYDROUS ZINC SULPHATE AND NOT MORE THAN 80 G./L. OF ANHYDROUS SODIUM SULPHATE, THE COAGULATION LIQUID BEING ALLOWED TO FLOW INTO THE BATH IN SUBSTANTIALLY THE SAME DIRECTION AS THAT OF THE EXTRUSION OF THE VISCOSE, STRETCHING THE PARTIALLY REGENERATED FILAMENTS WITH A DRAW RATIO OF 1.5 TO 3.5 BY MEANS OF A PAIR OF ROLLERS OUTSIDE THE BATH, AND COMPLETING THE REGENERATION IN A HOT AQUEOUS BATH CHARACTERISED IN THAT THE VISCOSE IS EXTRUDED INTO THE COAGULATION BATH AT A SPINNING LINEAL SPEED NOT EXCEEDING 10 M./MIN., 1/4 TO 3/4 OF THE TOTAL AMOUNT OF THE FLOW OF THE COAGULATION LIQUID INTO THE BATH IS PASSED THROUGH SAID CHANNEL IN THE SPINNERET, WHEREIN THE DIFFERENCE IN THE SULPHURIC ACID CONTENT OF THE COAGULATION LIQUID CONTINUOUSLY SUPPLIED TO THE BATH AND THAT CONTINUOUSLY WITHDRAWN FROM THE BATH IS ADJUSTED TO BETWEEN 0.5 AND 3.0 G./L., AND WHEREBY THE FILAMENT WHICH HAS LEFT THE SECOND ROLLER IS RUN IN AIR PRIOR TO THE COMPLETION OF THE REGENERATION UNTIL ITS DEGREE OF REGENERATION REACHES BETWEEN 65 AND 85%.
Claim 2
Dependent Claim 271 words
METHOD OF PRODUCING A VISCOSE FIBERS COMPRISING EXTRUDING A VISCOSE HAVING A GAMMA VALUE OF AT LEAST 60 AND CONTAINING BETWEEN 4% AND 7% BY WEIGHT OF A CELLULOSE COMPONENT HAVING A DEGREE OF POLYMERIZATION OF AT LEAST 500 AND BETWEEN 3% AND 6% BY WEIGHT OF SODIUM HYDROXIDE THROUGH AN ANNULAR SPINNERET PROVIDED WITH A CHANNEL AT ABOUT ITS CENTER, WITH AT LEAST 10,000 ORIFICES AROUND THE CHANNEL AT A TEMPERATURE NOT HIGHER THAN 30* C. INTO A COAGULATION BATH CONTAINING NOT MORE THAN 30 G./L. OF SULPHURIC ACID, AT LEAST 0.1 G./L. OF ANHYDROUS ZINC SULPHATE AND NOT MORE THAN 80 G./L. OF ANHYDROUS SODIUM SULPHATE, THE COAGULATION LIQUID BEING ALLOWED TO FLOW INTO THE BATH IN SUBSTANTIALLY THE SAME DIRECTION AS THAT OF THE EXTRUSION OF THE VISCOSE, STRETCHING THE PARTIALLY REGENERATED FILAMENTS WITH A DRAW RATIO OF 1.5 TO 3.5 BY MEANS OF A PAIR OF ROLLERS OUTSIDE THE BATH, AND COMPLETING THE REGENERATION IN A HOT AQUEOUS BATH CHARACTERISED IN THAT THE VISCOSE IS EXTRUDED INTO THE COAGULATION BATH AT A SPINNING LINEAL SPEED NOT EXCEEDING 10 M./MIN., 1/4 TO 3/4 OF THE TOTAL AMOUNT OF THE FLOW OF THE COAGULATION LIQUID INTO THE BATH IS PASSED THROUGH SAID CHANNEL IN THE SPINNERET, WHEREIN THE DIFFERENCE IN THE SULPHURIC ACID CONTENT OF THE COAGULATION LIQUID CONTINUOUSLY SUPPLIED TO THE BATH AND THAT CONTINUOUSLY WITHDRAWN FROM THE BATH IS ADJUSTED TO BETWEEN 0.5 AND 3.0 G./L., AND WHEREBY THE FILAMENT WHICH HAS LEFT THE SECOND ROLLER IS RUN IN AIR PRIOR TO THE COMPLETION OF THE REGENERATION UNTIL ITS DEGREE OF REGENERATION REACHES BETWEEN 65 AND 85%.

References Cited (Backward Citations)

US2536092A Cited
US2536094A Cited
US2882122A Cited
US2987371A Cited
US2997365A Cited
US3046083A Cited
US3108849A Cited
US3277226A Cited
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US3139467A Cited

USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1970-09-11 1971-03-13 1971-09-12 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 1974-09-11 1975-03-13 1975-09-12 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 1978-09-11 1979-03-13 1979-09-12 $7700.00 Window Closed / Lapsed

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