Patent EP0625490B1 successfully refreshed from Google Patents.
← Back to Patent Explorer
EP0625490B1 Expired / Lapsed EP ⏱️ 0.0 years remaining

Method for the preparation of carbonated hydroxyapatite compositions

Assignee: Abonetics Ltd
•
Filing: 1994-05-16
•
Granted: 1996-06-19
•
Expires: 2014-05-16
📄 Original PDF 🌐 Google Patents 🔄 Sync Now

Abstract

No abstract record available.

Inventors

  • 👤 William Prof. Bonfield
  • 👤 Serena Michelle Best
  • 👤 Jake Edward Barralet

Bibliographic Details

Application Number —
Jurisdiction EP
Data Source google_patents
Last Synchronized 2026-11-08 22:37
CPC Classifications
A; A61; A61L; A61L27/00; A61L27/02; A61L27/12; C; C04; C04B; C04B35/00; C04B35/01; C04B35/447; A61F; A61F2310/00; A61F2310/00005; A61F2310/00179; A61F2310/00293

Claims Analysis

Total Claims: 14
Claim 1
Independent Claim 120 words
A method for the preparation of a carbonated hydroxyapatite composition which has a density of at least 95% of the theoretical density, which method comprises sintering at substantially atmosphere pressure a green carbonated hydroxyapatite composition containing up to 20% by weight of C0₃²⁻ ions and having a green density of from 25 to 60% of the theoretical density at a temperature in the range of from 750° to 1450°C in carbon dioxide containing from 0.001 to 0.10 grams of water per litre of gas, the sintering temperature being selected within the above range and the green composition being sintered for a period of time sufficient to cause the green composition to densify to at least 95% of the theoretical density.
Claim 2
Dependent Claim 22 words
A method as claimed in claim 1 wherein the green composition has a density of 30 to 40% of the theoretical density.
Claim 3
Dependent Claim 23 words
A method as claimed in claim 1 or claim 2 wherein the sintering temperature is in the range of from 750° to 1150°C.
Claim 4
Independent Claim 27 words
A method as claimed in any one of the preceding claims wherein the carbon dioxide contains from 0.01 to 0.02 grams of water per litre of gas.
Claim 5
Independent Claim 27 words
A method as claimed in any one of the preceding claims wherein the sintering is carried out for a period of time of up to 24 hours.
Claim 6
Dependent Claim 23 words
A method as claimed in claim 5 wherein the sintering is carried out for a period of time of up to 4 hours.
Claim 7
Independent Claim 28 words
A method as claimed in any one of the preceding claims wherein the green carbonated hydroxyapatite composition has a carbonate content of from 3 to 10% by weight.
Claim 8
Independent Claim 26 words
A method as claimed in any one of the preceding claims wherein the carbonated hydroxyapatite composition comprises from 4 to 6% by weight of C0₃²⁻ ions.
Claim 9
Independent Claim 27 words
A method as claimed in any one of the preceding claims wherein the carbonated hydroxyapatite has a density of from 98% to 100% of the theoretical density.
Claim 10
Dependent Claim 13 words
A method as claimed in claim 9 wherein the carbonated hydroxyapatite is translucent.
Claim 11
Independent Claim 91 words
A method for the preparation of a carbonated hydroxyapatite composition which has a density of at least 95% of the theoretical density, which method comprises sintering at substantially atmosphere pressure a green carbonated hydroxyapatite composition containing up to 20% by weight of C0₃²⁻ ions at a temperature in the range of from 1000° to 1450°C in carbon dioxide containing from 0.001 to 0.10 grams of water per litre of gas, for a period of time sufficient to cause the green compact to densify to at least 95% of the theoretical density.
Claim 12
Dependent Claim 20 words
A method as claimed in claim 11 wherein the sintering temperature is in the range of from 1100° to 1300°C.
Claim 13
Dependent Claim 26 words
A method as claimed in claim 11 or claim 12 wherein the carbon dioxide contains from 0.01 to 0.02 grams of water per litre of gas.
Claim 14
Dependent Claim 22 words
A method as claimed in claim 11 wherein the carbonated hydroxyapatite composition comprises from 4 to 6% by weight of C0₃²⁻ ions.

References Cited (Backward Citations)

No citation records indexed.

USPTO Annuity & Maintenance Windows

Maintenance schedule is calculated for granted US utility patents.

Assigned Categories & Tags

No categories assigned to this patent yet.

Assign Category Tag