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EP0309596A1 Expired / Lapsed EP ⏱️ 0.0 years remaining

Pumping apparatus for delivering liquid at high pressure

Assignee: Hewlett Packard GmbH Germany
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Filing: 1987-09-26
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Granted: —
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Expires: 2007-09-26
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Abstract

Abstract A pumping apparatus for delivering liquid at a high pressure, in par­ticular for use in liquid chromatography, comprises two pistons (10, 20) which reciprocate in pump chambers (7,18) , respectively. The out­put of the first pump chamber (7) is connected via a valve (13) to the input of the second pump chamber (18). The pistons are driven by linear drives (30,31), e.g., ball-screw spindles. The stroke volume displaced by the piston (10) is freely adjustable by corresponding control of the angle by which the shaft of the drive motor (36) is rotated during a stroke cycle. The control circuitry is operative to reduce the stroke volume when the flow rate which can be selected by user at the user interface (42) is reduced, thus leading to reduced pulsations in the outflow of the pumping apparatus. The pumping ap­paratus can also be used for generating solvent gradients when a mixing valve (2) connected to different solvent containers (A,B,C,D) is coupled to the input of the pumping apparatus (Figure 1) .

Inventors

  • 👤 Fred Strohmeier
  • 👤 Klaus Witt

Bibliographic Details

Application Number —
Jurisdiction EP
Data Source google_patents
Last Synchronized 2026-11-07 21:54
CPC Classifications
F; F04; F04B; F04B49/00; F04B49/20; F04B11/00; F04B11/005; F04B11/0058; F04B11/0075; F04B49/06; F04B49/065; F04B49/12; F04B2201/00; F04B2201/12; F04B2201/1208; F04B2205/00; F04B2205/05; F04B2207/00; F04B2207/04; F04B2207/041; G; G01; G01N; G01N30/00; G01N30/02; G01N30/26; G01N30/28; G01N30/32; G01N2030/322; G01N2030/324; G01N2030/326; G01N30/34

Claims Analysis

Total Claims: 16
Claim 1
Independent Claim 164 words
A pumping apparatus for delivering liquid at a high pressure, com­prising : a) a first piston (10) for reciprocation in a first pump chamber (7) , the first pump chamber having an inlet port and an outlet port, b) a second piston (20) for reciprocation in a second pump chamber (18) , the second pump chamber having an inlet port and an out­let port, c) a conduit connection (12,14) between the outlet port of the first pump chamber and the inlet port of the second pump chamber, d) an inlet valve (4) connected to the inlet port of the first pump chamber for allowing flow of liquid into the first pump chamber and for inhibiting flow in the opposite direction, e) an outlet valve (13) connected to the outlet of the first pump chamber for allowing flow of liquid into the second pump chamber and for inhibiting flow in the opposite direction, f) drive means (30,34;31,33;32,36) for reciprocating the first and the second piston,
Claim 2
Dependent Claim 164 words
A pumping apparatus for delivering liquid at a high pressure, com­prising : a) a first piston (10) for reciprocation in a first pump chamber (7) , the first pump chamber having an inlet port and an outlet port, b) a second piston (20) for reciprocation in a second pump chamber (18) , the second pump chamber having an inlet port and an out­let port, c) a conduit connection (12,14) between the outlet port of the first pump chamber and the inlet port of the second pump chamber, d) an inlet valve (4) connected to the inlet port of the first pump chamber for allowing flow of liquid into the first pump chamber and for inhibiting flow in the opposite direction, e) an outlet valve (13) connected to the outlet of the first pump chamber for allowing flow of liquid into the second pump chamber and for inhibiting flow in the opposite direction, f) drive means (30,34;31,33;32,36) for reciprocating the first and the second piston,
Claim 3
Dependent Claim 70 words
characterized by control means (41,42,43,44,35) coupled to the drive means (30,34;31,33;32,36) for adjusting the stroke lengths of the pistons (10,20) between their top dead centre and their bottom dead centre, respectively, permitting an adjustment of the amounts of liquid displaced by the first and second piston, respectively, during a pump cycle such that pulsations in the flow of the liquid delivered to the output of the pumping apparatus are reduced.
Claim 4
Dependent Claim 70 words
characterized by control means (41,42,43,44,35) coupled to the drive means (30,34;31,33;32,36) for adjusting the stroke lengths of the pistons (10,20) between their top dead centre and their bottom dead centre, respectively, permitting an adjustment of the amounts of liquid displaced by the first and second piston, respectively, during a pump cycle such that pulsations in the flow of the liquid delivered to the output of the pumping apparatus are reduced.
Claim 5
Dependent Claim 25 words
Pumping apparatus as in claim 1, characterized in that the drive means comprise ball-screw spindles (30,31) coupled to each of the pistons (10,20) , respectively.
Claim 6
Dependent Claim 119 words
Pumping apparatus as in claim 1 or 2, characterized in that the drive means for each piston comprise: - an actuating element (37) having a recess (38) for receiving a ball (27), - a ball (27) having such a diameter that it projects above the recess (38), but can freely move inside the recess, - a piston holder (25) to which the piston (10) is mounted having a surface for contacting the ball (27), - a return spring (15} for exerting a force on the piston (10) in a direction away from the pump chamber (7) , and - a guiding element (39) arranged between the actuating element (37) and the pump chamber (7) for guiding the piston (10).
Claim 7
Dependent Claim 75 words
Pumping apparatus as in claim 2 or 3, characterized in that each ball-screw spindle (30,31) is coupled to a gear (34,33) , with the gears of the spindles being coupled to each other and to a gear (32) coupled to the axis of a common drive motor (36) such that a rotary motion of the common drive motor causes a reciprocat­ing movement of the two pistons (10,20) with a fixed phase relationship to each other.
Claim 8
Dependent Claim 43 words
Pumping apparatus as in claim 2 or 3, characterized in that each ball-screw spindle (30,31) is coupled to a separate drive motor allowing an adjustment of the relative phase of the reciprocating motions of the first (10) and of the second piston (20).
Claim 9
Dependent Claim 61 words
Pumping apparatus according to any of the preceding claims, characterized in that the two pistons (10,20) are reciprocating with a phase difference of 180 degrees and that the amount of liquid delivered by the first piston (10) during a pump cycle is two times as large as the amount of liquid delivered by the second piston (20) during that pump cycle.
Claim 10
Dependent Claim 100 words
Pumping apparatus as in any of the preceding claims , characterized by a damping element (23) connected either to the outlet of the first pump chamber (7) or to the outlet of the second pump chamber (18) for damping pulsations of the flow of the delivered liquid caused by the compressibility of the liquid, the damping element comprising two chambers separated by an elastic partition, one chamber receiving the liquid to be damped, the other chamber holding a damping liquid, with an insert having a selected volume and temperature expansion coefficient being pro­vided in the chamber holding the damping liquid.
Claim 11
Dependent Claim 143 words
Pumping apparatus as in any of the preceding claims, characterized in that - the inlet port (9) of the first and the inlet port (9ʹ) of the second pump chamber are located at that end of the chamber, respectively, from which the piston enters the chamber during its reciprocating motion, and the outlet port of the first and the outlet port of the second chamber are located at the op­posite ends of the chambers, respectively, and - the inner diameters of the bores (8,19) of the pump chambers are larger than the diameters of the pistons (10,20), respectively, such that liquid can flow between the pistons and the inner walls of the bores of the pump chambers into the space above the pistons, respectively, so that liquid is drawn in when the pis­tons move in a direction out of the pump chambers, respectively.
Claim 12
Dependent Claim 67 words
Pumping apparatus as in any of the preceding claims, characterized in that the control means (41,43,44,35) control the drive means in such a way that during the reciprocating movement of the pistons, the distances which the pistons travel from their top dead centre to their bottom dead centre and from their bottom dead centre back to their top dead centre, respective­ly, increase linearly with time (Figure 3).
Claim 13
Dependent Claim 43 words
Pumping apparatus as in any of the preceding claims, characterized in that the control means (41,43,44,35) control the drive means such that the stroke lengths of the pistons (10,20) is decreased when the flow rate of the delivered liquid is decreased (Figure 4).
Claim 14
Dependent Claim 56 words
Pumping apparatus as in any of the preceding claims, characterized in that for adjusting the stroke length of the first piston (10) either the top dead centre of the piston motion is kept fixed and the bottom dead centre is varied or the bottom dead centre is kept fixed and the top dead centre is varied.
Claim 15
Dependent Claim 97 words
Pumping apparatus as in any of the preceding claims, characterized by a mixing valve (2) coupled with its output to the inlet valve (4) of the first pump chamber (7) , the mixing valve having a plurality of inputs (1a,1b,1c,1d), each cou­pled to different containers (A,B,C,D) containing different sol­vents, the mixing valve being responsive to control signals from a gradient controller (45) connected to the control means for es­tablishing connections to a selected solvent container during ad­justable portions of the inlet stroke of the first piston (10), so that a desired mixture of solvents can be generated.
Claim 16
Dependent Claim 13 words
Use of a pumping apparatus as in claim 12 for generating solvent gradients.

References Cited (Backward Citations)

US4128476A Cited
US4245963A Cited
US4352636A Cited
FR2500081A1 Cited
GB2156445A Cited
DE3306631C1 Cited
US4509904A Cited
WO1985001993A1 Cited

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