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Method for refining non-oxide ceramic powders

Assignee: JFE Engineering Corp
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Filing: 1987-07-02
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Granted: —
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Expires: 2007-07-02
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Abstract

Abstract A method for refining powders comprising the steps of: (a) adding fluororesin powders to non-oxide ceramic powders to form a mixture by mixing; and (b) heating the mixture in non-oxidizing atmosphere to allow oxides existing on the surface of the non-oxide ceramic powders to convert into gaseous fluorides, the gaseous fluorides being removed. The fluororesin is polytetra­fluoroethylene resins. The heating temperature in the non-oxidizing atmosphere is 500°C to 1300°C.

Inventors

  • 👤 Hiroaki c/o Patent &Licence and Nishio
  • 👤 Michitaka c/o Patent & Licence and Sato

Bibliographic Details

Application Number —
Jurisdiction EP
Data Source google_patents
Last Synchronized 2026-11-09 05:05
CPC Classifications
C; C04; C04B; C04B35/00; C04B35/622; C04B35/64; C04B35/65; C01; C01B; C01B21/00; C01B21/06; C01B21/0615; C01B21/062; C01B21/064; C01B21/068; C01B21/0687; C01B21/072; C01B21/0728; C01B21/076; C01B21/0768; C01B32/00; C01B32/90; C01B32/914; C01B32/921; C01B32/956; C01B35/00; C01B35/02; C01B35/04; C04B35/515; C04B35/56; C04B35/5607; C04B35/5611; C04B35/563; C04B35/565; C04B35/58; C04B35/58007; C04B35/58014; C04B35/5805; C04B35/58064; C04B35/58071; C04B35/58078; C04B35/583; C04B35/584; C01P; C01P2006/00; C01P2006/60; C01P2006/80

Claims Analysis

Total Claims: 17
Claim 1
Independent Claim 59 words
A method for refining non-oxide ceramic powders, characterized by of comprising the steps of; adding powders of polytetrafluoroethylene resins to non-oxide ceramic powders to form a mixture by mixing; and heating the mixture in non-oxidizing atmosphere to allow oxides existing on the surface of the non-oxide ceramic powders to convert into gaseous fluorides, thereby the gaseous fluorides being removed.
Claim 2
Independent Claim 59 words
A method for refining non-oxide ceramic powders, characterized by of comprising the steps of; adding powders of polytetrafluoroethylene resins to non-oxide ceramic powders to form a mixture by mixing; and heating the mixture in non-oxidizing atmosphere to allow oxides existing on the surface of the non-oxide ceramic powders to convert into gaseous fluorides, thereby the gaseous fluorides being removed.
Claim 3
Dependent Claim 34 words
A method according to claim 1, characterized in that said powders of polytetrafluoroethylene resins include being at least one selected from the group consisting of tetrafluoroethylene resin, tetrafluoro­ethylene-hexafluoropropylene copolymer, tetrafluoroethylene-­perfluoroalkylvinylether copolymer, and tetrafluoroethylene-­ethylene copolymer.
Claim 4
Dependent Claim 32 words
A method according to claim 1 or 2, characterized in that said step of adding the powders of polytetrafluoro­ethylene resins includes adding the powders of polytetrafluoroethylene resins by 1 to 10 wt.%.
Claim 5
Dependent Claim 30 words
A method according to claim 3, characterized in that said step of adding the powders of polytetrafluoroethylene resins includes adding the powders of polytetrafluoroethylene resins by 1 to 5 wt.%.
Claim 6
Independent Claim 33 words
A method according to any one of claims 1 to 4, characterized in that said non-oxide ceramic powders include being at least one selected from the group consisting of nitride, carbide and boride.
Claim 7
Dependent Claim 33 words
A method according to claim 5, characterized in that said nitride includes being at least one selected from the group consisting of silicon nitride, aluminium nitride, boron nitride, chromium nitride and titanium nitride.
Claim 8
Dependent Claim 29 words
A method according to claim 5, characterized in that said carbide includes being at least one selected from the group consisting of silicon carbide, boron carbide and titanium carbide.
Claim 9
Dependent Claim 27 words
A method according to claim 5. characterized in that said boride includes being at least one selected from the group consisting of titanium boride and zirconium boride.
Claim 10
Independent Claim 20 words
A method according to any one of claims 1 to 8, characterized in that said non-oxidizing atmosphere includes being vacuum.
Claim 11
Independent Claim 27 words
A method according to any one of claims 1 to 9, characteized in that said step of heating includes heating at the temperature of 500° to 1300°C.
Claim 12
Dependent Claim 20 words
A method according to claim 10, characterized in that said heating includes heating at the temperature of 600°C to 1000°C.
Claim 13
Independent Claim 67 words
A method for refining non-oxide ceramic powders which comprises the steps of: adding powders of polytetrafluoroethylene resins to non-oxide ceramic powders to form a mixture by mixing; compacting the mixture into a green compact; and heating the green compact at the temperature of 500°-1300°C to allow oxides existing on the surface of the non-oxide ceramic powders to convert into gaseous fluorides, thereby the gaseous fluorides being removed.
Claim 14
Independent Claim 67 words
A method for refining non-oxide ceramic powders which comprises the steps of: adding powders of polytetrafluoroethylene resins to non-oxide ceramic powders to form a mixture by mixing; compacting the mixture into a green compact; and heating the green compact at the temperature of 500°-1300°C to allow oxides existing on the surface of the non-oxide ceramic powders to convert into gaseous fluorides, thereby the gaseous fluorides being removed.
Claim 15
Dependent Claim 24 words
A method according to claim 12, characterized in that said step of compacting the mixture includes applying cold isostatistic press treatment to the mixture.
Claim 16
Dependent Claim 28 words
A method according to claim 12 or 13, characterized by further comprising the additional step of sintering the green compact from which the gaseous fluorides have been removed.
Claim 17
Dependent Claim 37 words
A method according to claim 12, 13 or 14, characterized in that said step of adding powders of polytetrafluoroethylene resins includes adding the powders of polytetrafluoroethylene resins of 0.5 to 2.5 wt.% to the non-oxide ceramic powders.

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