USRE32270E
Expired / Lapsed
US
⏱️ 0.0 years remaining
Polyester coated paperboard for forming food containers and process for producing the same
Assignee: Graphic Packaging International LLC
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Filing: 1984-01-27
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Granted: 1986-10-28
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Expires: 2004-01-27
Abstract
Abstract A coated paperboard product and a process for producing the same which includes corona discharge treatment of a paperboard surface and subsequent extrusion of molten polyester thereon. The resulting product has a very high degree of adhesion between the paperboard and polyester layers, and is capable of being utilized for forming pressed food trays which can be subjected to oven cooking temperatures.
Inventors
- 👤 Lee J. Murray, Jr.
Bibliographic Details
Application Number
—
Jurisdiction
US
Data Source
google_patents
Last Synchronized
2026-10-31 06:19
CPC Classifications
D; D21; D21H; D21H19/00; D21H19/10; D21H19/14; D21H19/24; D21H19/28; B; B32; B32B; B32B27/00; B32B27/06; B32B27/10; Y; Y10; Y10T; Y10T156/00; Y10T156/10; Y10T156/1002; Y10T156/1043; Y10T156/1044; Y10T156/1048; Y10T428/00; Y10T428/13; Y10T428/1303; Y10T428/26; Y10T428/263; Y10T428/264; Y10T428/31504; Y10T428/31786; Y10T428/3179
Claims Analysis
Total Claims: 5
Claim 1
Independent Claim
445 words
measured at a 180° pull angle at 5 inches per minute..]. .[.3. The process of claim 2 wherein the thickness of the extrusion coating on the paperboard is between 0.5 mil and 1.5 mils and the corona energy density applied to the paperboard is between about 0.35 joule per square inch and 5 joules per square inch, and wherein the paperboard is selected such that the corona treated surface thereof has a surface roughness above a minimum level and a concentration of organic contaminants below a maximum level such that the adhesion between the extrusion coating and the paperboard is at least 90 grams per linear inch as measured at a 180° pull angle at 5 inches per minute..]. .[.4. The process of claim 3 wherein the hot melt extrusion exits from the extrusion die at an initial temperature of between 580° F. and 640° F. through an air gap before insertion into the nip, the air gap distance being selected with respect to the speed of the paperboard and the ambient and chill roll temperatures such that the temperature of the extrusion at the time of contact with the paperboard is above its melting temperature and such that it is chilled below its glass transition temperature at the time that it leaves the chill roll to thereby facilitate separation therefrom..]. .[.5. The process of claims 1 or 2 wherein the paperboard is selected such that the corona treated surface has a surface roughness as determined by the Bendtsen test at 5 Kg of at least 100..]. .[.6. The process of claims 1 or 2 wherein the paperboard is selected such that the corona treated surface thereof has a level of impurities as detected by an iodine stain test on a Macbeth Ms-2000 Spectrophotometer relative to a white plate standard of less than 25..]. .[.7. The process of claims 1 or 2 wherein the paperboard is formed of solid bleached sulfate pulp..]. .[.8. The process of claims 1 or 2 wherein the paperboard has a moisture content of at least 6% by weight..]. .[.9. The process of claims 1 or 4 wherein the chill roll is maintained at a surface temperature between 60° F. and 120° F..]. .[.10. The process of claims 1 or 2 wherein the hot melt of polyethylene terephthalate has a particulate color pigment intermixed therewith..]. .[.11. The process of claims 1 or 2 including the additional step of applying water to the uncoated surface of the coated paperboard laminate and storing the moistened paperboard in a moisture proof container for 24 hours to allow moisture throughout the paperboard to reach at least 10% by weight..]. .[.12. A coated paperboard product made
Claim 2
Dependent Claim
285 words
in accordance with the processes of claims 1 or 2..]. .Iadd.13. A process for producing coated paperboard material suitable for forming pressed heatable food trays, comprising the steps of: (a) passing a web of paperboard material through a corona discharge device at a corona energy density level sufficient to subject the paperboard to an energy density of at least 0.35 joules per square inch of paperboard surface; (b) passing the corona treated paperboard into a nip formed between a chill roll and a backup roll while simultaneously passing a hot melt extrusion of polyethylene terephthalate into the nip between the corona treated side of the paperboard and the chill roll to produce a thickness of the extrusion coating on the paperboard of between 0.5 mil and 1.5 mils, the hot melt extrusion exiting from the extrusion die at an initial temperature of between 580° F. and 640° F. through an air gap before insertion into the nip, the air gap distance being selected with respect to the speed of the paperboard and the ambient and chill roll temperatures such that the temperature of the extrusion at the time of contact with said paperboard is above its melting temperature of about 480° F. and such that it is chilled below its glass transition temperature of about 179° F. at the time that it leaves the chill roll to thereby facilitate separation therefrom, said paperboard being selected such that the corona treated surface has a surface roughness, as determined by the Bendtsen test at 5 Kg, of at least 100, and a level of impurities, as detected by an iodine stain test (ΔL) on a Macbeth MS-2000 Spectrophotometer relative to a white plate standard, of less than
Claim 3
Dependent Claim
59 words
.Iaddend. .Iadd.14. The process of claim 13 wherein said level of impurities, so detected, is about 15 to 25. .Iaddend. .Iadd.15. The process of claim 13, wherein said air gap distance and said paperboard speed are selected to provide a residence time of said extrusion in said air gap of from about 0.05 second to about 0.15 second. .Iaddend.
Claim 4
Dependent Claim
309 words
.Iadd. In a process for producing coated paperboard suitable for forming pressed oven-heatable food trays, the steps comprising: passing a web of paperboard through a corona discharge device at a corona energy density level sufficient to subject said surface of said paperboard to an energy density of at least 0.35 joule per square inch thereof; passing the corona-treated paperboard into a nip formed between a chill roll and a backup roll, while simultaneously passing into the nip between the corona-treated side of said paperboard and the chill roll a hot melt extrusion, in a thickness of between 0.5 and 1.5 mils, of a polyethylene terephthalate resin having a melting point temperature of about 480°; causing said hot melt extrusion to exit from the extrusion die at an initial temperature of from about 580° F. to about 640° F., and to pass, before insertion into said nip, through an air gap distance so selected with respect to the speed of said paperboard and the ambient and chill roll temperatures that said extrusion is, at the time of contact with said paperboard, above said melting point temperature and in a substantially fluid state, so as to flow into said fibrous surface of said paperboard; and quickly chilling said extrusion below the glass transition temperature of said resin of about 179° F. at the time that it leaves the chill roll, said paperboard being selected such that the corona treated surface has a surface roughness, as determined by the Bendtsen test at 5 Kg, of at least 100, and a level of impurities, as detected by an iodine stain test (ΔL) on a Macbeth MS-2000 Spectrophotometer relative to a white plate standard, of less than 25, the level of adhesion between said extrusion coating and said paperboard so attained being at least 90 grams per linear inch width, as measured at a
Claim 5
Dependent Claim
29 words
180 degree pull angle at 5 inches per minute. .Iaddend. .Iadd.17. A coated paperboard product made in accordance with the process of claims 13, 14, 15 or 16. .Iaddend.
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USPTO Annuity & Maintenance Windows
| Annuity Stage | Window Opens | Payment Deadline | Surcharge Period Until | Estimated Fee | Status |
|---|---|---|---|---|---|
| 3.5 Years (Year 4) | 1989-10-27 | 1990-04-28 | 1990-10-28 | $2000.00 | Window Closed / Lapsed |
| 7.5 Years (Year 8) | 1993-10-27 | 1994-04-28 | 1994-10-28 | $3760.00 | Window Closed / Lapsed |
| 11.5 Years (Year 12) | 1997-10-27 | 1998-04-28 | 1998-10-28 | $7700.00 | Window Closed / Lapsed |