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USH922H Expired / Lapsed US ⏱️ 0.0 years remaining

Method for analyzing materials using x-ray fluorescence

Assignee: United States Department of the Navy
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Filing: 1988-08-01
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Granted: 1991-05-07
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Expires: 2008-08-01
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Abstract

Abstract A method of identifying the presence, and amount, of elemental constituents in a material. The method uses an apparatus known for use in measuring extended x-ray absorption fine structure, and adapts it to the measurement of x-ray appearance potential in a manner to yield both qualitative and quantitative information about the elemental constituents of the material. The source of x-rays can be a synchrotron, which, because of its high power output, increases the speed and sensitivity of the measurements, permitting the use of less sensitive x-ray detectors to yield statistically significant data.

Inventors

  • 👤 Johnny P. Kirkland
  • 👤 Wm. Timothy Ehm
  • 👤 John V. Gilfrich

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-10-31 17:56
CPC Classifications
G; G01; G01N; G01N23/00; G01N23/22; G01N23/223; G01N2223/00; G01N2223/07; G01N2223/076

Claims Analysis

Total Claims: 2
Claim 1
Independent Claim 142 words
A method of identifying at least one elemental; constituent of a material sample, said method comprising steps for: (a) exposing said sample for a preselected time to a substantially monochromatic x-ray beam of preselected frequency; (b) measuring the amount of fluorescence emitted by said sample into a preselected solid angle during said preselected time responsive to said step for exposing; (c) measuring the amount of energy delivered to said sample in said preselected time by step (a); (d) varying the frequency of said monochromatic x-ray beam; (e) repeating steps (a) through (d) a sufficient number of times to identify an absorption edge transition of said elemental constituent of said sample; (f) measuring the change of magnitude of said amount of fluorescence at said absorption edge; (g) using said change of magnitude to calculate the amount of said elemental constituent of said sample.
Claim 2
Independent Claim 142 words
A method of identifying at least one elemental; constituent of a material sample, said method comprising steps for: (a) exposing said sample for a preselected time to a substantially monochromatic x-ray beam of preselected frequency; (b) measuring the amount of fluorescence emitted by said sample into a preselected solid angle during said preselected time responsive to said step for exposing; (c) measuring the amount of energy delivered to said sample in said preselected time by step (a); (d) varying the frequency of said monochromatic x-ray beam; (e) repeating steps (a) through (d) a sufficient number of times to identify an absorption edge transition of said elemental constituent of said sample; (f) measuring the change of magnitude of said amount of fluorescence at said absorption edge; (g) using said change of magnitude to calculate the amount of said elemental constituent of said sample.

References Cited (Backward Citations)

US3102952A Cited
US3030512A Cited
US3198944A Cited
US3150261A Cited
US4080171A Cited
US4134012A Cited
US4748636A Cited

USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1994-05-06 1994-11-05 1995-05-07 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 1998-05-06 1998-11-05 1999-05-07 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 2002-05-06 2002-11-05 2003-05-07 $7700.00 Window Closed / Lapsed

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