US6285449B1
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US
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Optical method and apparatus for detection of defects and microstructural changes in ceramics and ceramic coatings
Assignee: UChicago Argonne LLC
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Filing: 1999-06-11
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Granted: 2001-09-04
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Expires: 2019-06-11
Abstract
Abstract Apparatus detects defects and microstructural changes in hard translucent materials such as ceramic bulk compositions and ceramic coatings such as after use under load conditions. The beam from a tunable laser is directed onto the sample under study and light reflected by the sample is directed to two detectors, with light scattered with a small scatter angle directed to a first detector and light scattered with a larger scatter angle directed to a second detector for monitoring the scattering surface. The sum and ratio of the two detector outputs respectively provide a gray-scale, or “sum” image, and an indication of the lateral spread of the subsurface scatter, or “ratio” image. This two detector system allows for very high speed crack detection for on-line, real-time inspection of damage in ceramic components. Statistical image processing using a digital image processing approach allows for the quantative discrimination of the presence and distribution of small flaws in a sample while improving detection reliability. The tunable laser allows for the penetration of the sample to detect defects from the sample's surface to the laser's maximum depth of penetration. A layered optical fiber directs the incoming laser beam to the sample and transmits each scattered signal to a respective one of the two detectors.
Inventors
- 👤 William A. Ellingson
- 👤 Judith A. Todd
- 👤 Jiangang Sun
Bibliographic Details
Application Number
—
Jurisdiction
US
Data Source
google_patents
Last Synchronized
2026-11-09 12:32
CPC Classifications
G; G01; G01N; G01N21/00; G01N21/84; G01N21/88; G01N21/8851; G01N21/8422; G01N21/95
Claims Analysis
Total Claims: 11
Claim 1
Independent Claim
335 words
Apparatus for detecting surface and subsurface defects and microstructural changes in translucent ceramic-based materials and coatings, said apparatus comprising: a tunable laser providing an output beam of high intensity light having a variable wavelength varying between a lower wavelength limit and an upper wavelength limit; optical means for directing said output beam onto a specimen of a ceramic-based material or coating and for receiving light scattered from the specimen, wherein the specimen is disposed in a machine, said optical means including polarizing means for polarizing said output beam prior to incidence upon the specimen, wherein the wavelength of said output beam varies between said lower and upper wavelength limits allowing said output beam to penetrate from the surface to a given depth of the specimen, and wherein said given depth corresponds to said upper wavelength limit; first polarization maintaining optical fiber means disposed between said optical means and the specimen for directing the output beam onto the specimen without removing the specimen from said machine, and wherein said polarization maintaining optical fiber means further directs light scattered by the specimen to said optical means to permit distinguishing surface defects and microstructural changes from subsurface defects and microstructural changes by comparing polarization states of the output beam and the light scattered by the specimen; first detector means for receiving light scattered at small scattering angles from the specimen's surface or subsurface being investigated and providing a first output signal representing light scattered at small scattering angles; second detector means for receiving light scattered at larger scattering angles from the specimen's surface or subsurface for providing a second output signal representing light scattered at larger scattering angles, wherein larger surface or subsurface defects and microstructural changes exhibit larger scattering angles than the scattering angles from smaller surface or subsurface defects and microstructure changes; and display processing means coupled to said first and second detectors for processing said first and second output signals and visually displaying defects and microstructural changes on and below the surface of the specimen.
Claim 2
Dependent Claim
335 words
Apparatus for detecting surface and subsurface defects and microstructural changes in translucent ceramic-based materials and coatings, said apparatus comprising: a tunable laser providing an output beam of high intensity light having a variable wavelength varying between a lower wavelength limit and an upper wavelength limit; optical means for directing said output beam onto a specimen of a ceramic-based material or coating and for receiving light scattered from the specimen, wherein the specimen is disposed in a machine, said optical means including polarizing means for polarizing said output beam prior to incidence upon the specimen, wherein the wavelength of said output beam varies between said lower and upper wavelength limits allowing said output beam to penetrate from the surface to a given depth of the specimen, and wherein said given depth corresponds to said upper wavelength limit; first polarization maintaining optical fiber means disposed between said optical means and the specimen for directing the output beam onto the specimen without removing the specimen from said machine, and wherein said polarization maintaining optical fiber means further directs light scattered by the specimen to said optical means to permit distinguishing surface defects and microstructural changes from subsurface defects and microstructural changes by comparing polarization states of the output beam and the light scattered by the specimen; first detector means for receiving light scattered at small scattering angles from the specimen's surface or subsurface being investigated and providing a first output signal representing light scattered at small scattering angles; second detector means for receiving light scattered at larger scattering angles from the specimen's surface or subsurface for providing a second output signal representing light scattered at larger scattering angles, wherein larger surface or subsurface defects and microstructural changes exhibit larger scattering angles than the scattering angles from smaller surface or subsurface defects and microstructure changes; and display processing means coupled to said first and second detectors for processing said first and second output signals and visually displaying defects and microstructural changes on and below the surface of the specimen.
Claim 3
Dependent Claim
34 words
The apparatus of claim 1 wherein said first polarization maintaining optical fiber means includes first and second inner optical fibers for transmitting the output beam and light scattered by the specimen in opposed directions.
Claim 4
Dependent Claim
28 words
The apparatus of claim 2 further comprising second optical fiber means coupling said tunable laser to said optical means for providing the output beam to said optical means.
Claim 5
Dependent Claim
26 words
The apparatus of claim 1 wherein said tunable laser is a Ti:Sapphire laser having lower and upper wavelength limits of 700 nm and 1000 nm, respectively.
Claim 6
Dependent Claim
48 words
The apparatus of claim 1 wherein said optical means includes a plurality of polarizing beam-splitting cubes, quarter wave plates and positive focusing lenses for separating light scattered from the specimen into light scattered over small angles and light scattered over larger angles from the specimen's surface or subsurface.
Claim 7
Dependent Claim
47 words
The apparatus of claim 5 wherein said first detector includes a reflector having a pinhole aperture for passing light scattered over small angles from the specimen's surface or subsurface to said first detector and wherein said reflector directs light scattered over larger angles to said second detector.
Claim 8
Dependent Claim
69 words
The apparatus of claim 1 wherein said display processing means includes a video display having a plurality of image producing pixels arranged in a matrix array on said video display, with each pixel representing a particular location on the specimen, and wherein each pixel is assigned a gray scale value in accordance with the values of the first and second output signals of that particular location on the specimen.
Claim 9
Dependent Claim
34 words
The apparatus of claim 7 further comprising an automatic defect or microstructural change indication provided when the gray scale value of a pixel or a plurality of adjacent pixels exceeds a predetermined threshold value.
Claim 10
Dependent Claim
63 words
The apparatus of claim 1 wherein said display processing means includes means for combining said first and second signals to form a sum of said signals and a ratio of said signals, and wherein the sum of said signals is more sensitive to surface defects and microstructural changes and the ratio of said signals is more sensitive to subsurface defects and microstructural changes.
Claim 11
Dependent Claim
26 words
The apparatus of claim 1 further comprising displacement means coupled to the specimen for moving the specimen to permit the output beam to scan the specimen.
References Cited (Backward Citations)
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| Annuity Stage | Window Opens | Payment Deadline | Surcharge Period Until | Estimated Fee | Status |
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| 3.5 Years (Year 4) | 2004-09-03 | 2005-03-05 | 2005-09-04 | $2000.00 | Window Closed / Lapsed |
| 7.5 Years (Year 8) | 2008-09-03 | 2009-03-05 | 2009-09-04 | $3760.00 | Window Closed / Lapsed |
| 11.5 Years (Year 12) | 2012-09-03 | 2013-03-05 | 2013-09-04 | $7700.00 | Window Closed / Lapsed |