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US6069211A Expired / Lapsed US ⏱️ 0.0 years remaining

Chromate-free, one-part, non-curing corrosion inhibitive sealant with resistance to aviation fuel

Assignee: Courtaulds Aerospace Inc
•
Filing: 1998-11-06
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Granted: 2000-05-30
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Expires: 2018-11-06
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Abstract

Abstract A non-curing sealant composition includes a monoepoxy compound, a polysulfide, and a tertiary amine catalyst, and optionally a liquid polythioether polymer having a functionality between about 2 and about 3. The composition is substantially free of chromates.

Inventors

  • 👤 Alfredo Reyes, Jr.
  • 👤 Frank Campbell

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-10-28 21:41
CPC Classifications
C; C08; C08G; C08G75/00; C08L; C08L71/00; C08L71/02; C08L81/00; C08L81/04; C09; C09D; C09D171/00; C09D171/02; C09K; C09K3/00; C09K3/10; C09K3/1006; C09K3/1012; C08L2666/00; C08L2666/02; C08L2666/14; C08L2666/22

Claims Analysis

Total Claims: 26
Claim 1
Independent Claim 38 words
A non-curing sealant composition comprising (a) a monoepoxy compound selected from the group consisting of alkyl glycidyl ethers and aryl glycidyl ethers, (b) a polysulfide polymer (c) a tertiary amine catalyst, said composition being substantially free of chromates.
Claim 2
Dependent Claim 38 words
A non-curing sealant composition comprising (a) a monoepoxy compound selected from the group consisting of alkyl glycidyl ethers and aryl glycidyl ethers, (b) a polysulfide polymer (c) a tertiary amine catalyst, said composition being substantially free of chromates.
Claim 3
Dependent Claim 22 words
The composition of claim 1 which remains in an uncured state after exposure to a temperature of 250° F. for 1000 hours.
Claim 4
Dependent Claim 13 words
The composition of claim 1 having a mercaptan equivalent of at least 12,000.
Claim 5
Dependent Claim 16 words
The composition of claim 1 wherein said monoepoxy compound is a C 2-6 alkyl glycidyl ether.
Claim 6
Dependent Claim 13 words
The composition of claim 4 wherein said monoepoxy compound is butyl glycidyl ether.
Claim 7
Dependent Claim 13 words
The composition of claim 1 wherein said monoepoxy compound is phenyl glycidyl ether.
Claim 8
Dependent Claim 21 words
The composition of claim 1 further comprising (d) a liquid polythioether polymer having a functionality between about 2 and about 3.
Claim 9
Dependent Claim 23 words
The composition of claim 7 wherein said liquid polythioether polymer has a number average molecular weight ranging from about 500 to about 20,000.
Claim 10
Dependent Claim 13 words
The composition of claim 7 comprising a plurality of said liquid polythioether polymers.
Claim 11
Dependent Claim 22 words
The composition of claim 7 wherein the molar ratio of ingredient (d) to ingredient (a) ranges from about 1:1 to about 1:15.
Claim 12
Dependent Claim 14 words
The composition of claim 7 wherein said polysulfide polymer is a non-reactive alkyl polysulfide.
Claim 13
Dependent Claim 20 words
The composition of claim 1 further comprising an additive selected from the group consisting of fillers and salt corrosion inhibitors.
Claim 14
Dependent Claim 9 words
The composition of claim 1 further comprising a solvent.
Claim 15
Dependent Claim 11 words
The composition of claim 13 wherein said solvent is ethyl acetate.
Claim 16
Dependent Claim 100 words
A non-curing sealant composition comprising (a) about 0 to about 90 wt % of a liquid polythioether polymer having a functionality between about 2 and about 3, (b) about 0.5 to about 10 wt % of a monoepoxy compound selected from the group consisting of aryl glycidyl monoepoxides and alkyl glycidyl monoepoxides, (c) about 10 to about 90 wt % of a non-reactive alkyl polysulfide polymer, and (d) about 0.01 to about 2 wt % of a tertiary amine catalyst, wherein all wt % are based on the non-volatile components of the composition, said composition being substantially free of chromates.
Claim 17
Dependent Claim 100 words
A non-curing sealant composition comprising (a) about 0 to about 90 wt % of a liquid polythioether polymer having a functionality between about 2 and about 3, (b) about 0.5 to about 10 wt % of a monoepoxy compound selected from the group consisting of aryl glycidyl monoepoxides and alkyl glycidyl monoepoxides, (c) about 10 to about 90 wt % of a non-reactive alkyl polysulfide polymer, and (d) about 0.01 to about 2 wt % of a tertiary amine catalyst, wherein all wt % are based on the non-volatile components of the composition, said composition being substantially free of chromates.
Claim 18
Dependent Claim 16 words
The composition of claim 15 comprising about 10 to about 90 wt % of ingredient (a).
Claim 19
Dependent Claim 17 words
The composition of claim 15 further comprising about 0.05 to about 10 wt % of a solvent.
Claim 20
Dependent Claim 30 words
The composition of claim 15 further comprising about 1 to about 30 wt % of at least one additive selected from the group consisting of fillers and salt corrosion inhibitors.
Claim 21
Independent Claim 79 words
A method of making a non-curing sealant composition comprising: (i) forming a mixture by combining (a) a monoepoxy compound selected from the group consisting of alkyl glycidyl monoepoxides and aryl glycidyl monoepoxides, (b) a thiol terminated polysulfide polymer, (c) a tertiary amine catalyst said mixture being substantially free of chromates, and (ii) fleating said mixture at a temperature of at least about 160° F. for a time sufficient to afford a mercaptan equivalent weight of not less than 12,000.
Claim 22
Independent Claim 79 words
A method of making a non-curing sealant composition comprising: (i) forming a mixture by combining (a) a monoepoxy compound selected from the group consisting of alkyl glycidyl monoepoxides and aryl glycidyl monoepoxides, (b) a thiol terminated polysulfide polymer, (c) a tertiary amine catalyst said mixture being substantially free of chromates, and (ii) fleating said mixture at a temperature of at least about 160° F. for a time sufficient to afford a mercaptan equivalent weight of not less than 12,000.
Claim 23
Dependent Claim 27 words
The method of claim 19 wherein in step (i) said mixture further comprises (d) a liquid polythioether polymer having a functionality between about 2 and about 3.
Claim 24
Dependent Claim 17 words
The method of claim 20 wherein in step (i) said polysulfide polymer is a non-reactive alkyl polysulfide.
Claim 25
Dependent Claim 27 words
The method of claim 20 wherein after step (ii) an additive selected from the group consisting of fillers and salt corrosion inhibitors is added to said mixture.
Claim 26
Dependent Claim 16 words
The method of claim 20 wherein after step (ii) a solvent is added to said mixture.

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USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 2003-05-30 2003-11-29 2004-05-30 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 2007-05-30 2007-11-29 2008-05-30 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 2011-05-30 2011-11-29 2012-05-30 $7700.00 Window Closed / Lapsed

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