Sonochemical apparatus

Claim 1

An apparatus for subjecting a liquid to an ultrasonic intensity comprising: (a) a cylindrical tube defining a chamber for the liquid; (b) a plurality of collars fixed at one of their ends in fluid-tight manner to the outside surface of the wall of the tube so as to project outwardly from the wall, equally spaced around the tube and lying in a common plane; (c) a plurality of transducer assemblies adapted when energised to generate ultrasonic waves at an operating frequency; (d) a plurality of ultrasonic couplers adapted to resonate at the operating frequency, each coupler having a nodal flange by which it is fixed to the other end of a respective collar remote from the wall so part of the coupler is enclosed by the collar, each transducer assembly being fixed to the end of the respective coupler which is located outside the liquid-filled collar, the collar being of such dimensions that within the collar there is a gap between the end of the coupler and the nearest part of the wall of width less than 10 mm, and a gap between the sides of the coupler and the collar of width between 2 mm and 10 mm; (e) a buffer liquid, with a cavitation threshold above that of the liquid in the chamber, filling the collar and so occupying the gaps between the coupler and both the collar and the wall; and (f) means to circulate the buffer liquid.

Claim 2

An apparatus for subjecting a liquid to an ultrasonic intensity comprising: (a) a cylindrical tube defining a chamber for the liquid; (b) a plurality of collars fixed at one of their ends in fluid-tight manner to the outside surface of the wall of the tube so as to project outwardly from the wall, equally spaced around the tube and lying in a common plane; (c) a plurality of transducer assemblies adapted when energised to generate ultrasonic waves at an operating frequency; (d) a plurality of ultrasonic couplers adapted to resonate at the operating frequency, each coupler having a nodal flange by which it is fixed to the other end of a respective collar remote from the wall so part of the coupler is enclosed by the collar, each transducer assembly being fixed to the end of the respective coupler which is located outside the liquid-filled collar, the collar being of such dimensions that within the collar there is a gap between the end of the coupler and the nearest part of the wall of width less than 10 mm, and a gap between the sides of the coupler and the collar of width between 2 mm and 10 mm; (e) a buffer liquid, with a cavitation threshold above that of the liquid in the chamber, filling the collar and so occupying the gaps between the coupler and both the collar and the wall; and (f) means to circulate the buffer liquid.

Claim 3

An apparatus for subjecting a liquid to an ultrasonic intensity comprising means defining a chamber for the liquid, at least one collar fixed at one of its ends in a fluid-tight manner to the outside surface of a wall of the chamber so as to project outwardly from the wall, each collar enclosing part of an ultrasonic coupler adapted to resonate at an operating frequency and having a nodal flange by which it is fixed to the other end of the collar remote from the wall such that there is a gap between the sides of the coupler and the collar, and a gap between the end of the coupler in the collar and the wall, a buffer liquid with a cavitation threshold above that of the liquid in the chamber filling the collar and so occupying the gaps between the coupler and both the collar and the wall, a transducer assembly fixed to the end of the coupler which is located outside the liquid-filled collar and adapted when energized to generate ultrasonic waves of the operating frequency in the coupler, and means to circulate the buffer liquid and to cool it.

Claim 4

An apparatus for subjecting a liquid to an ultrasonic intensity comprising means defining a chamber for the liquid, at least one collar fixed at one of its ends in a fluid-tight manner to the outside surface of a wall of the chamber so as to project outwardly from the wall, each collar enclosing part of an ultrasonic coupler adapted to resonate at an operating frequency and having a nodal flange by which it is fixed to the other end of the collar remote from the wall such that there is a gap between the sides of the coupler and the collar, and a gap between the end of the coupler in the collar and the wall, a buffer liquid with a cavitation threshold above that of the liquid in the chamber filling the collar and so occupying the gaps between the coupler and both the collar and the wall, a transducer assembly fixed to the end of the coupler which is located outside the liquid-filled collar and adapted when energized to generate ultrasonic waves of the operating frequency in the coupler, and means to circulate the buffer liquid and to cool it.