US5626718A
Expired / Lapsed
US
⏱️ 0.0 years remaining
Use of polymers in the recycled fiber washing/deinking process
Assignee: Hercules LLC
•
Filing: 1994-09-16
•
Granted: 1997-05-06
•
Expires: 2014-09-16
Abstract
Abstract The present invention is directed to a method for increasing the retention on a washing/thickening device in an aqueous papermaking system. The method generally comprises adding to the furnish solids of the system an effective amount of a cationic polyacrylamide polymer.
Inventors
- 👤 Irenee J. Philippe
- 👤 Frank J. Sutman
- 👤 Thomas E. Taggart
- 👤 Mary B. K. Letscher
- 👤 Michael A. Schuster
- 👤 John C. Harrington, IV
Bibliographic Details
Application Number
—
Jurisdiction
US
Data Source
google_patents
Last Synchronized
2026-10-25 09:54
CPC Classifications
D; D21; D21C; D21C9/00; D21C9/001; D21C9/002; D21C9/005; D21C5/00; D21C5/02; D21C5/025; D21C9/02; D21C9/06; Y; Y02; Y02W; Y02W30/00; Y02W30/50; Y02W30/64
Claims Analysis
Total Claims: 37
Claim 1
Independent Claim
66 words
In the deinking of wastepaper in which ink particles are removed from an aqueous slurry of recycled fibers, followed by a washing and thickening step wherein said slurry is treated to further remove ink particles from said recycled fibers, the improvement comprising adding to the slurry an effective amount of cationic polyacrylamide polymer to increase the retention of recycled fibers in said washing and thickening step.
Claim 2
Dependent Claim
66 words
In the deinking of wastepaper in which ink particles are removed from an aqueous slurry of recycled fibers, followed by a washing and thickening step wherein said slurry is treated to further remove ink particles from said recycled fibers, the improvement comprising adding to the slurry an effective amount of cationic polyacrylamide polymer to increase the retention of recycled fibers in said washing and thickening step.
Claim 3
Dependent Claim
29 words
The method as recited in claim 1 wherein from about 0.025 to 25 pounds of active polymer per ton of furnish solids is added to the aqueous papermaking system.
Claim 4
Dependent Claim
17 words
The method as recited in claim 1 wherein the cationic polyacrylamide polymer is a cationic (meth)acrylamide copolymer.
Claim 5
Dependent Claim
68 words
The method as recited in claim 3 wherein the cationic (meth)acrylamide copolymer comprises as a substituent a monomer: ##STR3## wherein R 1 =H or CH 3 ; A=--NH or --O--; x=0-8; R 2 , R 3 , R 4 are each independently H, CH 3 , C 2 -C 8 alkyl, benzyl or C 2 -C 8 alkyl benzyl; and X=Cl, F, Br, I or SO 4 .
Claim 6
Dependent Claim
49 words
The method as recited in claim 3 wherein the cationic (meth)acrylamide copolymer comprises as a substituent a monomer: ##STR4## wherein x=0-8; R 1 =H, CH 3 , C 2 -C 8 alkyl, benzyl or C 2 -C 8 alkyl benzyl; and X=Cl, F, Br, I or SO 4 .
Claim 7
Dependent Claim
20 words
The method as recited in claim 3 wherein said washing and thickening step is performed on a double nip thickener.
Claim 8
Dependent Claim
22 words
The method as recited in claim 1 wherein said cationic polyacrylamide polymer has a molecular weight of from about 3,000,000 to 30,000,000.
Claim 9
Independent Claim
23 words
The method as recited in claim I wherein said cationic polyacrylamide polymer has a percent mole charge of from about 1 to 80%.
Claim 10
Dependent Claim
18 words
The method as recited in claim 1 wherein said cationic polyacrylamide polymer is a 2-acryloyloxyethyltrimethyl ammonium chloride/acrylamide copolymer.
Claim 11
Dependent Claim
75 words
In the manufacture of recycled fibers which includes (1) the repulping of recovered paper, followed by (2) the removal of printing inks from fibers, followed by (3) the treatment of the fibers through a double nip thickener in order to further remove contaminants, and retain furnish solids, the improvement comprising adding to said slurry an effective amount of a cationic polyacrylamide polymer to increase the retention of said furnish solids on said double nip thickener.
Claim 12
Dependent Claim
75 words
In the manufacture of recycled fibers which includes (1) the repulping of recovered paper, followed by (2) the removal of printing inks from fibers, followed by (3) the treatment of the fibers through a double nip thickener in order to further remove contaminants, and retain furnish solids, the improvement comprising adding to said slurry an effective amount of a cationic polyacrylamide polymer to increase the retention of said furnish solids on said double nip thickener.
Claim 13
Dependent Claim
29 words
The method as recited in claim 10 wherein from about 0.025 to 25 pounds of active polymer per ton of furnish solids is added to the aqueous papermaking system.
Claim 14
Dependent Claim
18 words
The method as recited in claim 10 wherein the cationic polyacrylamide polymer is a cationic (meth) acrylamide copolymer.
Claim 15
Dependent Claim
69 words
The method as recited in claim 12 wherein the cationic (meth) acrylamide copolymer comprises as a substituent a monomer: ##STR5## wherein R 1 =H or CH 3 ; A=--NH or --O--; x=0-8; R 2 , R 3 , R 4 are each independently H, CH 3 , C 2 -C 8 alkyl, benzyl or C 2 -C 8 alkyl benzyl; and X=Cl, F, Br, I or SO 4 .
Claim 16
Dependent Claim
48 words
The method as recited in claim 12 wherein the cationic (meth) acrylamide copolymer comprises as a substituent a monomer: ##STR6## wherein x=1-8; R 1 =H, CH 3 , C 2 -C 8 alkyl, benzyl or C 2 -C 8 alkyl benzyl; and X=Cl,F,Br, I or SO 4 .
Claim 17
Dependent Claim
22 words
The method as recited in claim 10 wherein said cationic polyacrylamide polymer has a molecular weight of from about 3,000,000 to 30,000,000.
Claim 18
Dependent Claim
23 words
The method as recited in claim 10 wherein said cationic polyacrylamide polymer has a percent mole charge of from about 1 to 80%.
Claim 19
Dependent Claim
18 words
The method as recited in claim 10 wherein said cationic polyacrylamide polymer is a 2-acryloyloxyethyltrimethyl ammonium chloride/acrylamide copolymer.
Claim 20
Dependent Claim
68 words
In the deinking of wastepaper in which ink particles are removed from an aqueous slurry of recycled fibers followed by a highspeed washing and thickening step wherein said slurry is treated to further remove ink particles from said recycled fibers, the improvement comprising adding to said slurry an effective amount of cationic polyacrylamide to increase the retention of fumish solids in said high speed washing and thickening step.
Claim 21
Dependent Claim
68 words
In the deinking of wastepaper in which ink particles are removed from an aqueous slurry of recycled fibers followed by a highspeed washing and thickening step wherein said slurry is treated to further remove ink particles from said recycled fibers, the improvement comprising adding to said slurry an effective amount of cationic polyacrylamide to increase the retention of fumish solids in said high speed washing and thickening step.
Claim 22
Independent Claim
143 words
A method of treating a pulp slurry containinq contaminant solid particles and fiber solids in a washing/thickening device of the type having a rotating roller and a wire in close proximity to said roller, said roller and said wire in combination, defining a nip interface therebetween, said method comprising: (1) treating said pulp slurry by adding a cationic polyacrylamide polymer thereto in an amount from about 0.025-25 pounds of said polymer per ton solids in said pulp slurry; (2) feeding said pulp slurry to said nip; and (3) forcing water and at least some of said contaminant solid particles from said pulp slurry through said wire along said nip interface to separate at least some of said contaminants from said slurry, whereby the amount of fiber solids remaining with said pulp after said step (3) is increased in comparison to untreated pulp slurries.
Claim 23
Independent Claim
143 words
A method of treating a pulp slurry containinq contaminant solid particles and fiber solids in a washing/thickening device of the type having a rotating roller and a wire in close proximity to said roller, said roller and said wire in combination, defining a nip interface therebetween, said method comprising: (1) treating said pulp slurry by adding a cationic polyacrylamide polymer thereto in an amount from about 0.025-25 pounds of said polymer per ton solids in said pulp slurry; (2) feeding said pulp slurry to said nip; and (3) forcing water and at least some of said contaminant solid particles from said pulp slurry through said wire along said nip interface to separate at least some of said contaminants from said slurry, whereby the amount of fiber solids remaining with said pulp after said step (3) is increased in comparison to untreated pulp slurries.
Claim 24
Dependent Claim
18 words
The method as recited in claim 19 wherein the cationic polyacrylamide polymer is a cationic (meth) acrylamide copolymer.
Claim 25
Dependent Claim
66 words
The method as recited in claim 20 wherein the cationic (meth)acrylamide copolymer comprises as a substituent a monomer: ##STR7## wherein R 1 =H or CH 3 ; A=--NH or --O--; x=0-8; R 2 , R 3 , R 4 are each independently H, CH 3 , C 2 -C 8 alkyl, benzyl or C 2 -C 8 alkyl benzyl; and X═Cl,F,Br, I or SO 4 .
Claim 26
Dependent Claim
47 words
The method as recited in claim 20 wherein the cationic (meth)acrylamide copolymer comprises as a substituent a monomer: ##STR8## wherein x=0-8; R 1 =H, CH 3 , C 2 -C 8 alkyl, benzyl or C 2 -C 8 alkyl benzyl; and X=Cl,F,Br, I or SO 4 .
Claim 27
Dependent Claim
22 words
The method as recited in claim 19 wherein said cationic polyacrylamide polymer has a molecular weight of from about 3,000,000 to 30,000,000.
Claim 28
Dependent Claim
23 words
The method as recited in claim 19 wherein said cationic polyacrylamide polymer has a percent mole charge of from about 1 to 80%.
Claim 29
Dependent Claim
18 words
The method as recited in claim 19 wherein said cationic polyacrylamide polymer is a 2-acryloyloxyethyltrimethyl ammonium chloride/acrylamide copolymer.
Claim 30
Independent Claim
109 words
A method for increasing the amount of fibrous solids material retained in a pulp stock containing contaminant solid particles and said fibrous solids material treated in a washer/thickener device having a rotatable roller and a wire trained around a portion of said roller to define a nip location; said method comprising: (1) adding a cationic polyacrylamide polymer to said pulp stock in an amount of about 0.025-25 pounds of said polymer per ton solids in said pulp slurry; (2) feeding said pulp stock to said nip location and subjecting said pulp stock to centrifugal force thereat to express liquid and some of said contaminant solid particles through said wire.
Claim 31
Independent Claim
109 words
A method for increasing the amount of fibrous solids material retained in a pulp stock containing contaminant solid particles and said fibrous solids material treated in a washer/thickener device having a rotatable roller and a wire trained around a portion of said roller to define a nip location; said method comprising: (1) adding a cationic polyacrylamide polymer to said pulp stock in an amount of about 0.025-25 pounds of said polymer per ton solids in said pulp slurry; (2) feeding said pulp stock to said nip location and subjecting said pulp stock to centrifugal force thereat to express liquid and some of said contaminant solid particles through said wire.
Claim 32
Dependent Claim
18 words
The method as recited in claim 26 wherein the cationic polyacrylamide polymer is a cationic (meth) acrylamide copolymer.
Claim 33
Dependent Claim
66 words
The method as recited in claim 27 wherein the cationic (meth)acrylamide copolymer comprises as a substituent a monomer: ##STR9## wherein R 1 =H or CH 3 ; A=--NH or --O--; x=0-8; R 2 , R 3 , R 4 are each independently H, CH 3 , C 2 -C 8 alkyl, benzyl or C 2 -C 8 alkyl benzyl; and X=Cl,F,Br, I or SO 4 .
Claim 34
Dependent Claim
46 words
The method as recited in claim 27 wherein the cationic (meth)acrylamide copolymer comprises as a substituent a monomer: ##STR10## wherein x=0-8;R 1 =H, CH 3 , C 2 -C 8 alkyl, benzyl or C 2 -C 8 alkyl benzyl; and X=Cl,F,Br, I or SO 4 .
Claim 35
Dependent Claim
22 words
The method as recited in claim 26 wherein said cationic polyacrylamide polymer has a molecular weight of from about 3,000,000 to 30,000,000.
Claim 36
Dependent Claim
23 words
The method as recited in claim 26 wherein said cationic polyacrylamide polymer has a percent mole charge of from about 1 to 80%.
Claim 37
Dependent Claim
18 words
The method as recited in claim 26 wherein said cationic polyacrylamide polymer is a 2-acryloyloxyethyltrimethyl ammonium chloride/acrylamide copolymer.
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USPTO Annuity & Maintenance Windows
| Annuity Stage | Window Opens | Payment Deadline | Surcharge Period Until | Estimated Fee | Status |
|---|---|---|---|---|---|
| 3.5 Years (Year 4) | 2000-05-05 | 2000-11-04 | 2001-05-06 | $2000.00 | Window Closed / Lapsed |
| 7.5 Years (Year 8) | 2004-05-05 | 2004-11-04 | 2005-05-06 | $3760.00 | Window Closed / Lapsed |
| 11.5 Years (Year 12) | 2008-05-05 | 2008-11-04 | 2009-05-06 | $7700.00 | Window Closed / Lapsed |