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US5508525A Expired / Lapsed US ⏱️ 0.0 years remaining

Identification of unknown gases using infrared absorption spectroscopy

Assignee: Thermo Environmental Instruments Inc
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Filing: 1995-05-11
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Granted: 1996-04-16
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Expires: 2015-05-11
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Abstract

Abstract A method and apparatus for identifying an unknown gas by generating an infrared spectrum of the unknown gas using an infrared spectrophotometer that includes a circular variable interference filter, compressing the infrared spectrum of the unknown gas, and comparing the compressed infrared spectrum of the unknown gas to a library of compressed infrared spectra of reference compounds. After comparison, the compressed spectra that most closely match the unknown gas are decompressed and displayed. Because frequency characteristics of circular variable interference filters vary from filter to filter, information designating these frequency characteristics for the particular filter employed are used in generating the infrared spectrum of the unknown gas.

Inventors

  • 👤 Stephen Day
  • 👤 Kailash Swarna

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-11-07 11:43
CPC Classifications
G; G01; G01J; G01J3/00; G01J3/28; G01N; G01N21/00; G01N21/17; G01N21/25; G01N21/31; G01N21/35; G01N21/3504; G01J3/12; G01J2003/1226; G01J2003/1234; G01J2003/283; G01J2003/2833; G01J2003/2866

Claims Analysis

Total Claims: 19
Claim 1
Independent Claim 164 words
A method of identifying an unknown gas, comprising: generating a set of infrared spectra of reference compounds to produce a library of infrared spectra of reference compounds, capturing a sample of said unknown gas, directing infrared energy through the captured sample of said unknown gas, producing a set of data corresponding to infrared characteristics of said unknown gas using an infrared spectrophotometer including a circular variable interference filter configured to receive the infrared energy directed through the captured sample of said unknown gas, said variable interference filter being comprised of a plurality of segments, each of said segments transmitting infrared energy across a frequency band from a starting frequency at a first end of said segment to an ending frequency at a second end of said segment, and identifying said unknown gas by generating an infrared spectrum of said unknown gas using said set of data and information designating said starting and ending frequencies of each of said segments of said variable interference filter.
Claim 2
Independent Claim 164 words
A method of identifying an unknown gas, comprising: generating a set of infrared spectra of reference compounds to produce a library of infrared spectra of reference compounds, capturing a sample of said unknown gas, directing infrared energy through the captured sample of said unknown gas, producing a set of data corresponding to infrared characteristics of said unknown gas using an infrared spectrophotometer including a circular variable interference filter configured to receive the infrared energy directed through the captured sample of said unknown gas, said variable interference filter being comprised of a plurality of segments, each of said segments transmitting infrared energy across a frequency band from a starting frequency at a first end of said segment to an ending frequency at a second end of said segment, and identifying said unknown gas by generating an infrared spectrum of said unknown gas using said set of data and information designating said starting and ending frequencies of each of said segments of said variable interference filter.
Claim 3
Dependent Claim 21 words
The method of claim 1, wherein said information designating said starting and ending frequencies is unique to a particular infrared spectrophotometer.
Claim 4
Dependent Claim 35 words
The method of claim 1, further comprising: generating an infrared spectrum of a background air sample, and modifying said infrared spectrum of said unknown gas based on said infrared spectrum of said background air sample.
Claim 5
Dependent Claim 15 words
The method of claim 1, further comprising normalizing said infrared spectrum of said unknown gas.
Claim 6
Dependent Claim 55 words
The method of claim 1, further comprising: compressing infrared spectra from said set of infrared spectra of reference compounds to produce a library of compressed infrared spectra of reference compounds, compressing said infrared spectrum of said unknown gas, comparing said compressed infrared spectrum of said unknown gas to said compressed infrared spectra of reference compounds.
Claim 7
Dependent Claim 51 words
The method of claim 5, further comprising obtaining said infrared spectra from said set of infrared spectra of reference compounds using an infrared spectrophotometer that does not include a circular variable interference filter and has higher resolution than said infrared spectrophotometer used in generating said infrared spectrum of said unknown gas.
Claim 8
Dependent Claim 16 words
The method of claim 5, wherein said compressing steps use a compression ratio of about 10:1.
Claim 9
Dependent Claim 37 words
The method of claim 5, further comprising decompressing a plurality of said compressed infrared spectra from said library, said plurality including the compressed infrared spectra that most closely match the compressed infrared spectrum of said unknown gas.
Claim 10
Dependent Claim 20 words
The method of claim 8, wherein said plurality of decompressed infrared spectra comprises the three most closely matching infrared spectra.
Claim 11
Dependent Claim 14 words
The method of claim 8, further comprising displaying said plurality of decompressed infrared spectra.
Claim 12
Independent Claim 161 words
An apparatus for identifying an unknown gas, comprising: an infrared spectrophotometer including a gas cell configured to capture a sample of said unknown gas, a source of infrared energy configured to direct infrared energy through said unknown gas in said gas cell, and a circular variable interference filter configured to receive the infrared energy directed through said unknown gas in said gas cell for producing an infrared spectrum of said unknown gas, said variable interference filter being comprised of a plurality of segments, each of said segments transmitting infrared energy across a frequency band from a starting frequency at a first end of said segment to an ending frequency at a second end of said segment, a library of infrared spectra of reference compounds, and circuitry for comparing said infrared spectrum of said unknown gas to said infrared spectra from said library, said circuitry using information about the starting and ending frequencies of each of said segments in making said comparison.
Claim 13
Independent Claim 161 words
An apparatus for identifying an unknown gas, comprising: an infrared spectrophotometer including a gas cell configured to capture a sample of said unknown gas, a source of infrared energy configured to direct infrared energy through said unknown gas in said gas cell, and a circular variable interference filter configured to receive the infrared energy directed through said unknown gas in said gas cell for producing an infrared spectrum of said unknown gas, said variable interference filter being comprised of a plurality of segments, each of said segments transmitting infrared energy across a frequency band from a starting frequency at a first end of said segment to an ending frequency at a second end of said segment, a library of infrared spectra of reference compounds, and circuitry for comparing said infrared spectrum of said unknown gas to said infrared spectra from said library, said circuitry using information about the starting and ending frequencies of each of said segments in making said comparison.
Claim 14
Dependent Claim 13 words
The apparatus of claim 11, wherein said apparatus is battery operated and portable.
Claim 15
Dependent Claim 112 words
The apparatus of claim 11, further comprising circuitry for compressing said infrared spectrum of said unknown gas, wherein said library of infrared spectra of reference compounds comprises a library of compressed infrared spectra of reference compounds compressed from infrared spectra obtained using an infrared spectrophotometer that does not include a circular variable interference filter and has higher resolution than said infrared spectrophotometer used in generating said infrared spectrum of said unknown gas, and wherein said circuitry for comparing said infrared spectrum of said unknown gas to said infrared spectra from said library is operable to compare said compressed infrared spectrum of said unknown gas to said compressed infrared spectra of reference compounds.
Claim 16
Dependent Claim 39 words
The apparatus of claim 13, further comprising circuitry for decompressing a plurality of said compressed infrared spectra from said library, said plurality including the compressed infrared spectra that most closely match the compressed infrared spectrum of said unknown gas.
Claim 17
Dependent Claim 18 words
The apparatus of claim 14, said apparatus further including circuitry for displaying said plurality of decompressed infrared spectra.
Claim 18
Dependent Claim 26 words
The apparatus of claim 15, said apparatus further including circuitry for displaying said infrared spectrum of said unknown gas and said plurality of decompressed infrared spectra.
Claim 19
Dependent Claim 13 words
The apparatus of claim 16, wherein said apparatus is battery operated and portable.

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USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1999-04-16 1999-10-16 2000-04-16 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 2003-04-16 2003-10-16 2004-04-16 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 2007-04-16 2007-10-16 2008-04-16 $7700.00 Window Closed / Lapsed

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