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US5486564A Expired / Lapsed US ⏱️ 0.0 years remaining

High purity polyhydrogen silsesquioxane resin for electronic coatings

Assignee: Dow Silicones Corp
•
Filing: 1995-02-13
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Granted: 1996-01-23
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Expires: 2015-02-13
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Abstract

Abstract Disclosed is a highly reproducible method for the molecular weight fractionation of polyhydrogen silsesquioxane that gives a very storage-stable polyhydrogen silsesquioxane having a freely selectable molecular weight. The method involves dissolving polyhydrogen silsesquioxane in active-hydrogen-free nonpolar solvent; adding an active-hydrogen-free polar solvent to the resulting solution in order to precipitate polyhydrogen silsesquioxane; and collecting the desired molecular weight fraction of polyhydrogen silsesquioxane.

Inventors

  • 👤 Katsutoshi Mine
  • 👤 Takashi Nakamura
  • 👤 Motoshi Sasaki

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-11-05 08:12
CPC Classifications
C; C08; C08G; C08G77/00; C08G77/04; C08G77/12; C08G77/32; C08G77/36

Claims Analysis

Total Claims: 9
Claim 1
Independent Claim 35 words
A high purity electronic coating composition comprising polyhydrogen silsesquioxane resin having a sodium content of 9 ppb or less, a sulfur content of 14 ppm or less and a chlorine content less than 1 ppm.
Claim 2
Dependent Claim 35 words
A high purity electronic coating composition comprising polyhydrogen silsesquioxane resin having a sodium content of 9 ppb or less, a sulfur content of 14 ppm or less and a chlorine content less than 1 ppm.
Claim 3
Dependent Claim 15 words
The coating composition of claim 1 wherein the sodium content is 6 ppb or less.
Claim 4
Dependent Claim 15 words
The coating composition of claim 1 wherein the sodium content is 2 ppb or less.
Claim 5
Dependent Claim 15 words
The coating composition of claim 1 wherein the sulfur content is 5 ppm or less.
Claim 6
Dependent Claim 15 words
The coating composition of claim 1 wherein the sulfur content is 4 ppm or less.
Claim 7
Dependent Claim 15 words
The coating composition of claim 1 wherein the sulfur content is 2 ppm or less.
Claim 8
Dependent Claim 15 words
The coating composition of claim 1 wherein the sulfur content is less than 1 ppm.
Claim 9
Dependent Claim 10 words
The coating composition of claim 1 dissolved in a solvent.

References Cited (Backward Citations)

US3615272A Cited
JPS59189126A Cited
JPS6042426A Cited
JPS6086017A Cited
JPS61127732A Cited
US4808653A Cited
US5063267A Cited

USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1999-01-22 1999-07-24 2000-01-23 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 2003-01-22 2003-07-24 2004-01-23 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 2007-01-22 2007-07-24 2008-01-23 $7700.00 Window Closed / Lapsed

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