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US5328683A Expired / Lapsed US ⏱️ 0.0 years remaining

Water repellent and method of preparation

Assignee: DuPont Toray Specialty Materials KK
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Filing: 1993-07-06
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Granted: 1994-07-12
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Expires: 2013-07-06
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Abstract

Abstract A water repellent powdered material and a method of making the powder in which the powdered material is mixed with an organic solvent solution of a triorganosiloxysilicic acid having the formula (R3SiO1/2)2nSiO2 in which R is a monovalent hydrocarbon radical such as alkyl, aryl, and alkenyl; and n is an integer having a value of one to five; with the acid being present in an amount of from 0.1 to 20 parts by weight per one hundred parts by weight of the powdered material. The powder can be used to formulate cosmetic foundations.

Inventors

  • 👤 Asao Harashima

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-11-08 12:19
CPC Classifications
A; A61; A61K; A61K8/00; A61K8/02; A61K8/0241; A61K8/18; A61K8/30; A61K8/58; A61K8/585; A61Q; A61Q1/00; A61Q1/02; A61Q1/12; B; B82; B82Y; B82Y30/00; C; C09; C09C; C09C1/00; C09C1/36; C09C1/3607; C09C1/3684; C09C3/00; C09C3/12; A61K2800/00; A61K2800/40; A61K2800/41; A61K2800/412; A61K2800/60; A61K2800/61; A61K2800/62; A61K2800/621; C01; C01P; C01P2004/00; C01P2004/60; C01P2004/61; C01P2004/62; C01P2004/64; C01P2004/80; C01P2004/82; C01P2004/84; C01P2006/00; C01P2006/20; C01P2006/90

Claims Analysis

Total Claims: 5
Claim 1
Independent Claim 130 words
A cosmetic foundation comprising a wax, a liquid paraffin, a dimethylpolysiloxane, and a water repellent powder made by (i) mixing a powdered material with an organic solvent solution of a triorganosiloxy silicic acid having the formula (R 3 SiO 178 ) 2 nSiO 2 in which R is a monovalent hydrocarbon radical selected from the group consisting of alkyl, aryl, and alkenyl; and n is an integer having a value of one to five; the triorganosiloxy silicic acid being present in an amount of from 0.1 to 20 parts by weight per one hundred parts by weight of the powdered material; the triorganosiloxy silicic acid being prepared by reacting water glass and a hexaorganodisilizane with heating in an aromatic solvent/water mixture followed by extractive drying; and (ii) removing the solvent.
Claim 2
Dependent Claim 130 words
A cosmetic foundation comprising a wax, a liquid paraffin, a dimethylpolysiloxane, and a water repellent powder made by (i) mixing a powdered material with an organic solvent solution of a triorganosiloxy silicic acid having the formula (R 3 SiO 178 ) 2 nSiO 2 in which R is a monovalent hydrocarbon radical selected from the group consisting of alkyl, aryl, and alkenyl; and n is an integer having a value of one to five; the triorganosiloxy silicic acid being present in an amount of from 0.1 to 20 parts by weight per one hundred parts by weight of the powdered material; the triorganosiloxy silicic acid being prepared by reacting water glass and a hexaorganodisilizane with heating in an aromatic solvent/water mixture followed by extractive drying; and (ii) removing the solvent.
Claim 3
Dependent Claim 24 words
A cosmetic according to claim 1 in which the powdered material has an average particle size in the range of 0.05 to 500 micrometers.
Claim 4
Dependent Claim 23 words
A cosmetic according to claim 1 in which the triorganosiloxy silicic acid has a molecular weight in the range of 500 to 10,000.
Claim 5
Dependent Claim 29 words
A cosmetic according to claim 3 in which the triorganosiloxy silicic acid (R 3 SiO 1/2 ) units and SiO 2 units in a ratio of 1.0 to 1.1.

References Cited (Backward Citations)

JPS6130512A Cited
US4753977A Cited
US5219560A Cited

USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1997-07-11 1998-01-10 1998-07-12 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 2001-07-11 2002-01-10 2002-07-12 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 2005-07-11 2006-01-10 2006-07-12 $7700.00 Window Closed / Lapsed

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