US5273779A
Expired / Lapsed
US
⏱️ 0.0 years remaining
Method of fabricating a gas sensor and the product fabricated thereby
Assignee: Industrial Technology Research Institute
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Filing: 1991-12-09
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Granted: 1993-12-28
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Expires: 2011-12-09
Abstract
Abstract A method of fabricating a gas sensor which comprises a substrate; a buffer layer coated on the substrate; at least one gas sensing layer arranged on the buffer layer; a pair of electrodes disposed on the gas sensing layer; and a catalytic layer coated on the gas sensing layer. A spin coating process is performed, using centrifugal force, to form the layers which are thin and evenly deposited on the substrate. The gas sensing layer of the gas sensor is formed before forming the electrodes of the same such that the heat treatment thereto can be carried out at 800° C. which is much higher than the conventional temperature of 600° C. The bonding of the gas sensing layer to the substrate is thereby much stronger than the conventional gas sensor.
Inventors
- 👤 I-Cherng Chen
- 👤 Ming-Hann Tzeng
- 👤 Ping-Ping Tsai
- 👤 Chiu-Fong Liaw
- 👤 James C. H. Ku
Bibliographic Details
Application Number
—
Jurisdiction
US
Data Source
google_patents
Last Synchronized
2026-10-28 23:24
CPC Classifications
G; G01; G01N; G01N27/00; G01N27/02; G01N27/04; G01N27/12
Claims Analysis
Total Claims: 12
Claim 1
Independent Claim
147 words
A method of fabricating a gas sensor, comprising the following steps of: (a) coating a buffer layer onto the surface of a substrate by spin coating a substrate with a buffer from a metallo-organic solution and heat treating the buffer layer at an elevated temperature at about 800° C.; (b) coating a gas sensing layer onto said buffer layer by spin coating said buffer layer with a gas sensing layer from a metallo-organic solution on said buffer layer and heat treating said gas sensing layer at an elevated temperature at about 800° C.; (c) screen printing a pair of electrodes onto said gas sensing layer with a conductive paste, and heat treating the printed electrodes at about 600° C.; and (d) coating a catalytic layer from a metallo-organic solution onto said gas sensing layer by spin coating and heat treating said catalytic layer at about 600° C.
Claim 2
Independent Claim
147 words
A method of fabricating a gas sensor, comprising the following steps of: (a) coating a buffer layer onto the surface of a substrate by spin coating a substrate with a buffer from a metallo-organic solution and heat treating the buffer layer at an elevated temperature at about 800° C.; (b) coating a gas sensing layer onto said buffer layer by spin coating said buffer layer with a gas sensing layer from a metallo-organic solution on said buffer layer and heat treating said gas sensing layer at an elevated temperature at about 800° C.; (c) screen printing a pair of electrodes onto said gas sensing layer with a conductive paste, and heat treating the printed electrodes at about 600° C.; and (d) coating a catalytic layer from a metallo-organic solution onto said gas sensing layer by spin coating and heat treating said catalytic layer at about 600° C.
Claim 3
Dependent Claim
36 words
A method of fabricating a gas sensor according to claim 1, wherein in said Step (a) the metal contained in the metallo-organic solution is selected from the group consisting of Sn, Zn, Ni, Fe, and In.
Claim 4
Dependent Claim
31 words
A method of fabricating a gas sensor according to claim 1, wherein the spin speed provided by the spin coating process is controlled within the range from 2000 to 4000 rpm.
Claim 5
Dependent Claim
26 words
A method of fabricating a gas sensor according to claim 1, wherein in said Step (b) the heat treatment is carried out for about 5 hours.
Claim 6
Dependent Claim
43 words
A method of fabricating a gas sensor according to claim 1, wherein said Step (d) the metallo-organic solution is selected from the group consisting of a resinate solution, an alkoxide, or a metal acetylacetonate which contains either Pt, Au, Pd, Sb, or Ag.
Claim 7
Independent Claim
172 words
A method of fabricating a gas sensor comprising the following steps of: (a) coating a buffer layer onto the surface of a substrate by spin coating a substrate with a buffer from a metallo-organic solution and heat treating said layer; (b) coating a first gas sensing layer onto said buffer layer by spin coating said buffer layer with a sensor from a metallo-organic solution and heat treating said first gas sensing layer at about 800° C.; (c) screen printing a pair of electrodes onto said first gas sensing layer with a gel of inductive material, and heat treating said printed electrodes at about 600° C.; (d) coating a second gas sensing layer onto said first gas sensing layer by spin coating said first gas sensing layer with a second gas sensor from a metallo-organic solution and heat treating said second gas sensing layer at about 600° C.; and (e) coating a catalytic layer onto said second gas sensing layer by spin coating and heat treating said catalytic layer at about 600° C.
Claim 8
Independent Claim
172 words
A method of fabricating a gas sensor comprising the following steps of: (a) coating a buffer layer onto the surface of a substrate by spin coating a substrate with a buffer from a metallo-organic solution and heat treating said layer; (b) coating a first gas sensing layer onto said buffer layer by spin coating said buffer layer with a sensor from a metallo-organic solution and heat treating said first gas sensing layer at about 800° C.; (c) screen printing a pair of electrodes onto said first gas sensing layer with a gel of inductive material, and heat treating said printed electrodes at about 600° C.; (d) coating a second gas sensing layer onto said first gas sensing layer by spin coating said first gas sensing layer with a second gas sensor from a metallo-organic solution and heat treating said second gas sensing layer at about 600° C.; and (e) coating a catalytic layer onto said second gas sensing layer by spin coating and heat treating said catalytic layer at about 600° C.
Claim 9
Dependent Claim
36 words
A method of fabricating a gas sensor according to claim 6, wherein in said Step (a) the metal contained in the metallo-organic solution is selected from the group consisting of Sn, Zn, Ni, Fe, and In.
Claim 10
Dependent Claim
31 words
A method of fabricating a gas sensor according to claim 6, wherein the spin speed provided by the spin coating process is controlled within the range from 2000 to 4000 rpm.
Claim 11
Dependent Claim
26 words
A method of fabricating a gas sensor according to claim 6, wherein in said Step (b) the heat treatment is carried out for about 5 hours.
Claim 12
Dependent Claim
46 words
A method of fabricating a gas sensor according to claim 6, wherein in said Step (d) the metallo-organic solution is selected from the group consisting of a resinate solution, an alkoxide, or an acetylacetonate metal containing at least one of Pt, Au, Pd, Sb, or Ag.
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USPTO Annuity & Maintenance Windows
| Annuity Stage | Window Opens | Payment Deadline | Surcharge Period Until | Estimated Fee | Status |
|---|---|---|---|---|---|
| 3.5 Years (Year 4) | 1996-12-27 | 1997-06-28 | 1997-12-28 | $2000.00 | Window Closed / Lapsed |
| 7.5 Years (Year 8) | 2000-12-27 | 2001-06-28 | 2001-12-28 | $3760.00 | Window Closed / Lapsed |
| 11.5 Years (Year 12) | 2004-12-27 | 2005-06-28 | 2005-12-28 | $7700.00 | Window Closed / Lapsed |