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US5266098A Expired / Lapsed US ⏱️ 0.0 years remaining

Production of charged uniformly sized metal droplets

Assignee: Massachusetts Institute of Technology
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Filing: 1992-01-07
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Granted: 1993-11-30
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Expires: 2012-01-07
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Abstract

Abstract A process for producing charged uniformly sized metal droplets in which a quantity of metal is placed in a container and liquified, the container having a plurality of orifices to permit passage of the liquified metal therethrough. The liquified metal is vibrated in the container. The vibrating liquified metal is forced through the orifices, the vibration causing the liquified metal to form uniformly sized metal droplets. A charge is placed on the liquified metal either when it is in the container or after the liquified metal exits the container, the charging thereof causing the droplets to maintain their uniform size. The uniformly sized droplets can be used to coat a substrate with the liquified metal.

Inventors

  • 👤 Jung-Hoon Chun
  • 👤 Christian H. Passow

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-10-29 14:36
CPC Classifications
B; B22; B22F; B22F9/00; B22F9/02; B22F9/06; B22F9/08; B22F9/082; B22F2009/0836; B22F2202/00; B22F2202/01; B22F2998/00; B22F2999/00

Claims Analysis

Total Claims: 20
Claim 1
Independent Claim 129 words
A process for producing and maintaining charged uniformly sized metal droplets comprising the steps of: (1) liquefying a quantity of metal disposed in a container having at least one orifice to permit the passage of metal; (2) vibrating the liquefied metal in said container; and (3) forcing the vibrating liquefied metal through the at least one orifice; said method further including a step of placing a positive or negative charge on the liquefied metal, either before or after it exits the at least one orifice, the vibration thereof thereby causing said liquefied metal to form uniformly sized liquid metal droplets, which droplets exhibit a degree of variation of less than about ±25% from the average droplet diameter, and the charging thereof causing said droplets to maintain their uniform size.
Claim 2
Dependent Claim 129 words
A process for producing and maintaining charged uniformly sized metal droplets comprising the steps of: (1) liquefying a quantity of metal disposed in a container having at least one orifice to permit the passage of metal; (2) vibrating the liquefied metal in said container; and (3) forcing the vibrating liquefied metal through the at least one orifice; said method further including a step of placing a positive or negative charge on the liquefied metal, either before or after it exits the at least one orifice, the vibration thereof thereby causing said liquefied metal to form uniformly sized liquid metal droplets, which droplets exhibit a degree of variation of less than about ±25% from the average droplet diameter, and the charging thereof causing said droplets to maintain their uniform size.
Claim 3
Dependent Claim 29 words
The process of claim 1, wherein said vibrating step includes applying at least one oscillating gas jet to the liquified metal as it exits the at least one orifice.
Claim 4
Dependent Claim 22 words
The process of claim 1, wherein the liquefied metal is charged after it exits the at least one orifice in the container.
Claim 5
Dependent Claim 56 words
The process of claim 3, wherein the placing of a positive or negative charge on the liquefied metal comprises using a charging plate having at least one opening therein aligned with the at least one orifice so as to permit the vibrated liquefied metal exiting the orifice to pass through the charging plate and become charged.
Claim 6
Dependent Claim 51 words
The process of claim 4, wherein the liquefied metal is forced through a plurality of orifices forming a plurality of streams of uniformly sized metal droplets and passing the droplets through a plurality of openings in the charge plate thereby forming a plurality of streams of charged uniformly sized metal droplets.
Claim 7
Dependent Claim 42 words
The process of claim 3, wherein the uniformly sized droplets have a diameter which is within the range of from about 10 to 500 μm and wherein the droplets exhibit a degree of variation of about ±5% of the average droplet diameter.
Claim 8
Dependent Claim 29 words
The process of claim 3, wherein said vibrating step includes applying at least one oscillating gas jet to the liquified metal as it exits the at least one orifice.
Claim 9
Dependent Claim 52 words
The process of claim 7, wherein the placing of a positive or negative charge on the liquefied metal comprises using a charging plate having at least one opening therein aligned with the at least one orifice so as to permit the liquefied metal exiting the orifice to pass through the charging plate.
Claim 10
Dependent Claim 42 words
The process of claim 7, wherein the uniformly sized droplets have a diameter which is within the range of from about 10 to 500 μm and wherein the droplets exhibit a degree of variation of about ±10% of the average droplet diameter.
Claim 11
Dependent Claim 23 words
The process of claim 1, wherein the liquefied metal is charged when it is in the container before it is formed into droplets.
Claim 12
Dependent Claim 29 words
The process of claim 10, wherein said vibrating step includes applying at least one oscillating gas jet to the liquified metal as it exits the at least one orifice.
Claim 13
Dependent Claim 42 words
The process of claim 10, wherein the uniformly sized droplets have a diameter which is within the range of from about 10 to 500 μm and wherein the droplets exhibit a degree of variation of about ±5% of the average droplet diameter.
Claim 14
Dependent Claim 17 words
The process of claim 1, wherein the process further comprises depositing the charged droplets onto a substrate.
Claim 15
Dependent Claim 42 words
The process of claim 1, wherein the uniformly sized droplets have a diameter which is within the range of from about 10 to 500 μm and wherein the droplets exhibit a degree of variation of about ±5% of the average droplet diameter.
Claim 16
Dependent Claim 23 words
The process of claim 1, wherein the uniformly sized charged metal droplets have an initial velocity of from about 1 to 25 m/sec.
Claim 17
Dependent Claim 23 words
The process of claim 1, wherein the uniformly sized metal droplets are charged to about 10 -5 to 10 -8 Coulombs per gram.
Claim 18
Dependent Claim 23 words
The process of claim 1, further comprising applying an electric field in a flow path of the metal droplets to change their trajectories.
Claim 19
Dependent Claim 26 words
The process of claim 1, further comprising monitoring the charged metal droplets after formation to determine the sizes and the velocities of said liquid metal droplets.
Claim 20
Dependent Claim 15 words
The process of claim 1, wherein the process is performed in an inert gas atmosphere.

References Cited (Backward Citations)

GB1587125A Cited
US4886547A Cited
US4762553A Cited
US5062936A Cited

USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1996-11-29 1997-05-31 1997-11-30 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 2000-11-29 2001-05-31 2001-11-30 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 2004-11-29 2005-05-31 2005-11-30 $7700.00 Window Closed / Lapsed

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