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US5211728A Expired / Lapsed US ⏱️ 0.0 years remaining

Clamshell retainer used in hollow fiber membrane devices

Assignee: MG Generon Inc
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Filing: 1992-06-04
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Granted: 1993-05-18
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Expires: 2012-06-04
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Abstract

Abstract The invention relates to a hollow fiber membrane device having a hollow fiber membrane bundle with tubesheets, separable end caps, clamshell-shaped retainers for joining the end caps to the tubesheets, associated circumferential keepers which positionally constrain the clamshell-shaped retainers, and an optional envelope which encloses the membrane bundle.

Inventors

  • 👤 Johnny L. Trimmer

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-10-24 17:48
CPC Classifications
B; B01; B01D; B01D53/00; B01D53/22; B01D63/00; B01D63/02; B01D63/031; B01D63/04; B01D65/00; F; F16; F16L; F16L55/00; F16L55/10; F16L55/115; B01D2313/00; B01D2313/42; B01D2317/00; B01D2317/02; B01D2317/04; B01D2319/00; B01D2319/04

Claims Analysis

Total Claims: 41
Claim 1
Independent Claim 482 words
A process for separating a feed gas mixture using a membrane separation device containing a plurality of hollow fiber semi-permeable gas separation membranes, comprising: (1) contacting one side of said membranes with a feed gas mixture under pressure; (2) maintaining a pressure differential across the membranes under conditions such that at least one gaseous component in the feed gas mixture selectively permeates through the membranes from the higher pressure side to the lower pressure side of said membranes; (3) removing from the lower pressure side of said membranes permeated gas which is enriched in at least one selectively permeating gaseous component; and (4) removing from the higher pressure side of said membranes non-permeated gas which is depleted in at least one selectively permeating gaseous component, wherein said device comprises: A. a hollow fiber membrane bundle containing said plurality of hollow fiber semi-permeable gas separation membranes; B. a tubesheet on each end of said bundle, each tubesheet having a radially outward surface with a circumferential groove therein, an inner face intersected by said hollow fiber membranes, said hollow fiber membranes being sealingly secured at each end in the respective tubesheet and communicating therethrough, and an outer face with a peripheral surface; C. first and second end caps, each having a radially outward surface and an inner face with a peripheral flange, said flange being positioned and adapted to sealingly mate against the mating peripheral surface on the outer face of an adjacent respective tubesheet, each flange having sufficient width in the axial direction to provide an enclosed space between the inner face of said end cap and the outer face of the adjacent tubesheet, the space serving as a fluid inlet or outlet region, and each end cap having a circumferential groove in the radially outward surface thereof; D. a clamshell retainer means for each adjacent end cap and associated tubesheet, said clamshell retainer means having the configuration of a segmented collar with a plurality of segments, the segments together forming the collar with flange portions on each segment extending radially inwardly, the flange portions of each segment being adapted to fit matingly, respectively, and coordinately into the peripheral groove pair of each respective end cap and associated tubesheet, the spacing between the flanges being such as to urge each end cap and associated tubesheet snugly together in a sealing relationship; E. a circumferential keeper means closely surrounding each clamshell retainer means to hold the flanges of the clamshell retainer means in the respective grooves in each end cap and associated tubesheet; F. a hollow envelope enclosing said hollow fiber membrane bundle, said envelope having ends which are fitted sealingly against each respective tubesheet to provide an enclosed space around the hollow fiber membrane bundle; and G. respective ports extending through each end cap and through said keeper means and said hollow envelope to provide fluid communication into and out of said device.
Claim 2
Dependent Claim 482 words
A process for separating a feed gas mixture using a membrane separation device containing a plurality of hollow fiber semi-permeable gas separation membranes, comprising: (1) contacting one side of said membranes with a feed gas mixture under pressure; (2) maintaining a pressure differential across the membranes under conditions such that at least one gaseous component in the feed gas mixture selectively permeates through the membranes from the higher pressure side to the lower pressure side of said membranes; (3) removing from the lower pressure side of said membranes permeated gas which is enriched in at least one selectively permeating gaseous component; and (4) removing from the higher pressure side of said membranes non-permeated gas which is depleted in at least one selectively permeating gaseous component, wherein said device comprises: A. a hollow fiber membrane bundle containing said plurality of hollow fiber semi-permeable gas separation membranes; B. a tubesheet on each end of said bundle, each tubesheet having a radially outward surface with a circumferential groove therein, an inner face intersected by said hollow fiber membranes, said hollow fiber membranes being sealingly secured at each end in the respective tubesheet and communicating therethrough, and an outer face with a peripheral surface; C. first and second end caps, each having a radially outward surface and an inner face with a peripheral flange, said flange being positioned and adapted to sealingly mate against the mating peripheral surface on the outer face of an adjacent respective tubesheet, each flange having sufficient width in the axial direction to provide an enclosed space between the inner face of said end cap and the outer face of the adjacent tubesheet, the space serving as a fluid inlet or outlet region, and each end cap having a circumferential groove in the radially outward surface thereof; D. a clamshell retainer means for each adjacent end cap and associated tubesheet, said clamshell retainer means having the configuration of a segmented collar with a plurality of segments, the segments together forming the collar with flange portions on each segment extending radially inwardly, the flange portions of each segment being adapted to fit matingly, respectively, and coordinately into the peripheral groove pair of each respective end cap and associated tubesheet, the spacing between the flanges being such as to urge each end cap and associated tubesheet snugly together in a sealing relationship; E. a circumferential keeper means closely surrounding each clamshell retainer means to hold the flanges of the clamshell retainer means in the respective grooves in each end cap and associated tubesheet; F. a hollow envelope enclosing said hollow fiber membrane bundle, said envelope having ends which are fitted sealingly against each respective tubesheet to provide an enclosed space around the hollow fiber membrane bundle; and G. respective ports extending through each end cap and through said keeper means and said hollow envelope to provide fluid communication into and out of said device.
Claim 3
Dependent Claim 39 words
The process of claim 1 wherein said feed gas mixture comprises at least one of the gases selected from the group consisting of hydrogen, helium, oxygen, nitrogen, carbon monoxide, carbon dioxide, water vapor, hydrogen sulfide, ammonia, and light hydrocarbons.
Claim 4
Dependent Claim 22 words
The process of claim 2 wherein the pressure of the feed gas mixture is between about 10 psig and about 2000 psig.
Claim 5
Dependent Claim 22 words
The process of claim 3 wherein the temperature of the feed gas mixture is between about 0° C. and about 150° C.
Claim 6
Dependent Claim 20 words
The process of claim 3 wherein the temperature of said membrane is between about 0° C. and about 150° C.
Claim 7
Dependent Claim 222 words
A means for attaching an end cap to a tubesheet of a hollow fiber membrane separation module, the tubesheet having an inner face intersected by a plurality of hollow fiber membranes and an outer face, the end cap and the tubesheet having mating peripheral surfaces and the end cap and tubesheet each having an outer peripheral surface, comprising: A. a peripheral circumferential groove in the outer surface of each of the end cap and tubesheet, the groove in the outer surface of the tubesheet being adjacent to the inner face thereof; B. clamshell retainer means for each adjacent end cap and associated tubesheet in the form of a segmented collar with a plurality of curved segments, the segments together forming a substantially complete cylindrical collar with flange portions adjacent to both edges thereof, the flange portions on each segment extending radially inwardly, the flange portions of each segment being adapted to fit matingly, respectively, and coordinately into the peripheral groove pair of respective end cap and associated tubesheet, the spacing between the flanges being such as to urge each end cap and associated tubesheet snugly together in a sealing relationship; and C. a circumferential keeper means closely surrounding each clamshell retainer means to hold the flanges of the clamshell retainer means in the respective grooves in each end cap and associated tubesheet.
Claim 8
Dependent Claim 222 words
A means for attaching an end cap to a tubesheet of a hollow fiber membrane separation module, the tubesheet having an inner face intersected by a plurality of hollow fiber membranes and an outer face, the end cap and the tubesheet having mating peripheral surfaces and the end cap and tubesheet each having an outer peripheral surface, comprising: A. a peripheral circumferential groove in the outer surface of each of the end cap and tubesheet, the groove in the outer surface of the tubesheet being adjacent to the inner face thereof; B. clamshell retainer means for each adjacent end cap and associated tubesheet in the form of a segmented collar with a plurality of curved segments, the segments together forming a substantially complete cylindrical collar with flange portions adjacent to both edges thereof, the flange portions on each segment extending radially inwardly, the flange portions of each segment being adapted to fit matingly, respectively, and coordinately into the peripheral groove pair of respective end cap and associated tubesheet, the spacing between the flanges being such as to urge each end cap and associated tubesheet snugly together in a sealing relationship; and C. a circumferential keeper means closely surrounding each clamshell retainer means to hold the flanges of the clamshell retainer means in the respective grooves in each end cap and associated tubesheet.
Claim 9
Dependent Claim 223 words
A means for attaching a tubesheet of a second hollow fiber membrane separation module to a tubesheet of a first hollow fiber membrane separation module, the tubesheets each having an inner face intersected by a plurality of hollow fiber membranes and an outer face, the tubesheet of the second module and the tubesheet of the first module having mating peripheral surfaces and the tubesheet of the second module and the tubesheet of the first module each having an outer peripheral surface, comprising: A. a peripheral circumferential groove in the outer surface of each of the tubesheets, the groove in the outer surface of the tubesheets being adjacent to the inner face thereof; B. clamshell retainer means for the tubesheets in the form of a segmented collar with a plurality of curved segments, the segments together forming a substantially complete cylindrical collar with flange portions adjacent to both edges thereof, the flange portions on each segment extending radially inwardly, the flange portions of each segment being adapted to fit matingly, respectively, and coordinately into the peripheral grooves of the tubesheets, the spacing between the flanges being such as to urge the tubesheets together in a sealing relationship; and C. a circumferential keeper means closely surrounding each clamshell retainer means to hold the flanges of the clamshell retainer means in the grooves in each tubesheet.
Claim 10
Dependent Claim 223 words
A means for attaching a tubesheet of a second hollow fiber membrane separation module to a tubesheet of a first hollow fiber membrane separation module, the tubesheets each having an inner face intersected by a plurality of hollow fiber membranes and an outer face, the tubesheet of the second module and the tubesheet of the first module having mating peripheral surfaces and the tubesheet of the second module and the tubesheet of the first module each having an outer peripheral surface, comprising: A. a peripheral circumferential groove in the outer surface of each of the tubesheets, the groove in the outer surface of the tubesheets being adjacent to the inner face thereof; B. clamshell retainer means for the tubesheets in the form of a segmented collar with a plurality of curved segments, the segments together forming a substantially complete cylindrical collar with flange portions adjacent to both edges thereof, the flange portions on each segment extending radially inwardly, the flange portions of each segment being adapted to fit matingly, respectively, and coordinately into the peripheral grooves of the tubesheets, the spacing between the flanges being such as to urge the tubesheets together in a sealing relationship; and C. a circumferential keeper means closely surrounding each clamshell retainer means to hold the flanges of the clamshell retainer means in the grooves in each tubesheet.
Claim 11
Dependent Claim 294 words
A housing device for a hollow fiber membrane separation module having a hollow fiber membrane bundle with a tubesheet on each end of the bundle, each tubesheet having a circumferential groove in the radially outward surface, an inner face intersected by a plurality of hollow fiber membranes and an outer face, the hollow fiber membranes being sealingly secured at each end in the respective tubesheet and communicating therethrough, comprising: A. first and second end caps, each having a radially outward surface and an inner face with a peripheral flange, said flange being positioned and adapted to sealingly mate against the mating peripheral surface on the outer face of an adjacent respective tubesheet, each flange having sufficient width in the axial direction to provide an enclosed space between the inner face of said end cap and the outer face of the adjacent tubesheet, the space serving as a fluid inlet or outlet region, and each end cap having a circumferential groove in the radially outward surface of each end cap; B. a clamshell retainer means for each adjacent end cap and associated tubesheet, said clamshell retainer means having the configuration of a segmented collar with a plurality of segments, the segments together forming the collar with flange portions on each segment extending radially inwardly, the flange portions of each segment being adapted to fit matingly, respectively, and coordinately into the peripheral groove pair of each respective end cap and associated tubesheet, the spacing between the flanges being such as to urge each end cap and associated tubesheet snugly together in a sealing relationship; and C. a circumferential keeper means closely surrounding each clamshell retainer means to hold the flanges of the clamshell retainer means in the respective grooves in each end cap and associated tubesheet.
Claim 12
Dependent Claim 294 words
A housing device for a hollow fiber membrane separation module having a hollow fiber membrane bundle with a tubesheet on each end of the bundle, each tubesheet having a circumferential groove in the radially outward surface, an inner face intersected by a plurality of hollow fiber membranes and an outer face, the hollow fiber membranes being sealingly secured at each end in the respective tubesheet and communicating therethrough, comprising: A. first and second end caps, each having a radially outward surface and an inner face with a peripheral flange, said flange being positioned and adapted to sealingly mate against the mating peripheral surface on the outer face of an adjacent respective tubesheet, each flange having sufficient width in the axial direction to provide an enclosed space between the inner face of said end cap and the outer face of the adjacent tubesheet, the space serving as a fluid inlet or outlet region, and each end cap having a circumferential groove in the radially outward surface of each end cap; B. a clamshell retainer means for each adjacent end cap and associated tubesheet, said clamshell retainer means having the configuration of a segmented collar with a plurality of segments, the segments together forming the collar with flange portions on each segment extending radially inwardly, the flange portions of each segment being adapted to fit matingly, respectively, and coordinately into the peripheral groove pair of each respective end cap and associated tubesheet, the spacing between the flanges being such as to urge each end cap and associated tubesheet snugly together in a sealing relationship; and C. a circumferential keeper means closely surrounding each clamshell retainer means to hold the flanges of the clamshell retainer means in the respective grooves in each end cap and associated tubesheet.
Claim 13
Dependent Claim 68 words
The device of claim 8 additionally comprising: D. a hollow envelope enclosing said hollow fiber membrane bundle, said envelope having ends which are fitted sealingly against each respective tubesheet to provide an enclosed space around the hollow fiber membrane bundle; and E. respective ports extending through each end cap and through said keeper means and said hollow envelope to provide fluid communication into and out of said device.
Claim 14
Dependent Claim 14 words
The device of claim 9 wherein said clamshell retainer is comprised of non-contiguous segments.
Claim 15
Dependent Claim 18 words
The device of claim 9 wherein said clamshell retainer means is comprised of no more than two segments.
Claim 16
Dependent Claim 18 words
The device of claim 9 wherein said circumferential keeper means is comprised of a clamp of adjustable sizing.
Claim 17
Dependent Claim 37 words
The device of claim 9 wherein said circumferential keeper means is comprised of a two-part cylindria keeper, joined along one axial edge by means of a hinge and joined along the other edge by a clamping means.
Claim 18
Dependent Claim 25 words
The device of claim 9 wherein said circumferential keeper means is comprised of two cylindrical sections, joined along both axial edges by a clamping means.
Claim 19
Dependent Claim 15 words
The device of claim 9 wherein said hollow envelope serves as the circumferential keeper means.
Claim 20
Dependent Claim 46 words
The device of claim 9 wherein said circumferential grooves, said flanges extending radially inwardly from said clamshell retainer means, and peripheral interior edges of the ends of said hollow envelope are chamfered such that said clamshell retainer means and said hollow envelope are more easily assembled.
Claim 21
Dependent Claim 20 words
The device of claim 9 wherein said end cap possesses a means for indexing and aligning said circumferential keeper means.
Claim 22
Dependent Claim 19 words
The device of claim 17 wherein said indexing and aligning means is a cap screw, set screw, or pin.
Claim 23
Dependent Claim 297 words
A hollow fiber membrane separation device comprising: A. a hollow fiber membrane bundle containing a plurality of hollow fiber semi-permeable membranes; B. a tubesheet on each end of said bundle, each tubesheet having a radially outward surface with a circumferential groove therein, an inner face intersected by said hollow fiber membranes, said hollow fiber membranes being sealingly secured at each end in the respective tubesheet and communicating therethrough, and an outer face with a peripheral surface; C. first and second end caps, each having a radially outward surface and an inner face with a peripheral flange, said flange being positioned and adapted to sealingly mate against the mating peripheral surface on the outer face of an adjacent respective tubesheet, each flange having sufficient width in the axial direction to provide an enclosed space between the inner face of said end cap and the outer face of the adjacent tubesheet, the space serving as a fluid inlet or outlet region, and each end cap having a circumferential groove in the radially outward surface thereof; D. a clamshell retainer means for each adjacent end cap and associated tubesheet, said clamshell retainer means having the configuration of a segmented collar with a plurality of segments, the segments together forming the collar with flange portions on each segment extending radially inwardly, the flange portions of each segment being adapted to fit matingly, respectively, and coordinately into the peripheral groove pair of respective end cap and associated tubesheet, the spacing between the flanges being such as to urge each end cap and associated tubesheet snugly together in a sealing relationship; and E. a circumferential keeper means closely surrounding each clamshell retainer means to hold the flanges of the clamshell retainer means in the respective grooves in each end cap and associated tubesheet.
Claim 24
Dependent Claim 297 words
A hollow fiber membrane separation device comprising: A. a hollow fiber membrane bundle containing a plurality of hollow fiber semi-permeable membranes; B. a tubesheet on each end of said bundle, each tubesheet having a radially outward surface with a circumferential groove therein, an inner face intersected by said hollow fiber membranes, said hollow fiber membranes being sealingly secured at each end in the respective tubesheet and communicating therethrough, and an outer face with a peripheral surface; C. first and second end caps, each having a radially outward surface and an inner face with a peripheral flange, said flange being positioned and adapted to sealingly mate against the mating peripheral surface on the outer face of an adjacent respective tubesheet, each flange having sufficient width in the axial direction to provide an enclosed space between the inner face of said end cap and the outer face of the adjacent tubesheet, the space serving as a fluid inlet or outlet region, and each end cap having a circumferential groove in the radially outward surface thereof; D. a clamshell retainer means for each adjacent end cap and associated tubesheet, said clamshell retainer means having the configuration of a segmented collar with a plurality of segments, the segments together forming the collar with flange portions on each segment extending radially inwardly, the flange portions of each segment being adapted to fit matingly, respectively, and coordinately into the peripheral groove pair of respective end cap and associated tubesheet, the spacing between the flanges being such as to urge each end cap and associated tubesheet snugly together in a sealing relationship; and E. a circumferential keeper means closely surrounding each clamshell retainer means to hold the flanges of the clamshell retainer means in the respective grooves in each end cap and associated tubesheet.
Claim 25
Dependent Claim 66 words
The device of claim 19 additionally comprising: F. a hollow envelope enclosing said hollow fiber membrane bundle, said envelope having ends fitted sealingly against each respective tubesheet to provide an enclosed space around the hollow fiber membrane bundle; and G. respective ports extending through each end cap and through said keeper means and said hollow envelope to provide fluid communication into and out of said device.
Claim 26
Dependent Claim 14 words
The device of claim 20 wherein said clamshell retainer is comprised of non-contiguous segments.
Claim 27
Dependent Claim 18 words
The device of claim 20 wherein said clamshell retainer means is comprised of no more than two segments.
Claim 28
Dependent Claim 18 words
The device of claim 20 wherein said circumferential keeper means is comprised of a clamp of adjustable sizing.
Claim 29
Dependent Claim 37 words
The device of claim 20 wherein said circumferential keeper means is comprised of a two-part cylindrical keeper, joined along one axial edge by means of a hinge and joined along the other edge by a clamping means.
Claim 30
Dependent Claim 25 words
The device of claim 20 wherein said circumferential keeper means is comprised of two cylindrical sections, joined along both axial edges by a clamping means.
Claim 31
Dependent Claim 15 words
The device of claim 20 wherein said hollow envelope serves as the circumferential keeper means.
Claim 32
Dependent Claim 46 words
The device of claim 20 wherein said circumferential grooves, said flanges extending radially inwardly from said clamshell retainer means, and peripheral interior edges of the ends of said hollow envelope are chamfered such that said clamshell retainer means and said hollow envelope are more easily assembled.
Claim 33
Dependent Claim 19 words
The device of claim 20 wherein said end cap possesses a means for indexing and aligning said circumferential means.
Claim 34
Dependent Claim 19 words
The device of claim 28 wherein said indexing and aligning means is a set screw, cap screw, or pin.
Claim 35
Dependent Claim 54 words
The device of claim 20 wherein said hollow fiber membranes comprise at least one polymer selected from the group consisting of olefinic polymers; polytetrafluoroethylene; cellulosic esters; cellulose ethers; regenerated cellulose; polyamides; polyetherketones; polyestercarbonates; polycarbonates; polyesters; polyarylates; polyethers; polybenzoxazoles; polyoxadiazoles; polytriazoles; polycyanoarylethers; polyamideimides; polythioethers; polystyrenes; polysulfones; polyimides; polyetherimides; polyethersulfones; and copolymers and physical blends thereof.
Claim 36
Dependent Claim 25 words
The device of claim 30 wherein said hollow fiber membranes have an outside diameter in the range of about 50 microns to about 400 microns.
Claim 37
Dependent Claim 24 words
The device of claim 31 wherein said hollow fiber membranes have an outside to inside diameter ratio of between about 1.5 and about 1.15.
Claim 38
Dependent Claim 12 words
The device of claim 32 wherein the hollow fiber membranes are asymmetric.
Claim 39
Dependent Claim 12 words
The device of claim 32 wherein the hollow fiber membranes are composite.
Claim 40
Dependent Claim 13 words
The device of claim 32 wherein the hollow fiber membrane bundle is parallel-wrapped.
Claim 41
Dependent Claim 13 words
The device of claim 32 wherein the hollow fiber membrane bundle is bias-wrapped.

USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1996-05-17 1996-11-16 1997-05-18 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 2000-05-17 2000-11-16 2001-05-18 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 2004-05-17 2004-11-16 2005-05-18 $7700.00 Window Closed / Lapsed

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