US5166006A
Expired / Lapsed
US
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Textured thin-film substrate and method
Assignee: WD Media LLC
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Filing: 1991-06-03
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Granted: 1992-11-24
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Expires: 2011-06-03
Abstract
Abstract A method of forming an isotropic texture having a selected summit density and surface roughness in a selected inner-diameter annular zone of a thin-film medium substrate having a polished metal coating on the substrate. The zone is selectively exposed to a chemical etchant, under etchant strength, temperature, and exposure time, until the selected summit density and roughness are achieved. In a preferred embodiment, the etching conditions are selected to produce a summit density between about 500-20,000/mm 2 , and an arithmetic mean roughness value between about 20-70 Å in the inner zone, and a substantially reduced roughness value in an annular, isotropically textured outer-diameter zone of the coating. A thin-film medium formed on the substrate is suitable for near-contact recording.
Inventors
- 👤 Brij B. Lal
- 👤 Atef H. Eltoukhy
Bibliographic Details
Application Number
—
Jurisdiction
US
Data Source
google_patents
Last Synchronized
2026-11-02 14:06
CPC Classifications
G; G11; G11B; G11B5/00; G11B5/74; G11B5/82; C; C23; C23F; C23F1/00; C23F1/02; G11B5/84; G11B5/8404; Y; Y10; Y10S; Y10S428/00; Y10S428/90; Y10T; Y10T29/00; Y10T29/49; Y10T29/49002; Y10T29/4902; Y10T29/49021; Y10T29/49032; Y10T29/49036; Y10T29/49043; Y10T29/49046; Y10T29/49048; Y10T29/49052; Y10T428/00; Y10T428/12; Y10T428/12472; Y10T428/12993
Claims Analysis
Total Claims: 20
Claim 1
Independent Claim
101 words
A method of texturing a polished, metal, annular-surface coating on a thin-film medium substrate, to produce a substantially isotropic texture with a selected roughness and summit density in a selected annular zone of the coating, comprising exposing such annular zone to an acidic chemical etchant effective to etch the surface coating, for an exposure period sufficient to produce such roughness and summit density, during at least a portion of such exposing, masking other annular zones of the coating from contact with the etchant, producing a lesser roughness and summit density in such other zones, and removing such etchant from the coating.
Claim 2
Independent Claim
101 words
A method of texturing a polished, metal, annular-surface coating on a thin-film medium substrate, to produce a substantially isotropic texture with a selected roughness and summit density in a selected annular zone of the coating, comprising exposing such annular zone to an acidic chemical etchant effective to etch the surface coating, for an exposure period sufficient to produce such roughness and summit density, during at least a portion of such exposing, masking other annular zones of the coating from contact with the etchant, producing a lesser roughness and summit density in such other zones, and removing such etchant from the coating.
Claim 3
Dependent Claim
43 words
The method of claim 1, wherein said coating contains between 86 and 93 atom percent nickel and 7 and 14 atom percent phosphorus, and said etchant contains 1-10 M nitric acid, 0.1-2 M phosphoric acid, and 0.1-1 M H 2 O 2 .
Claim 4
Dependent Claim
29 words
The method of claim 2, wherein said removing includes contacting the etching coating with a solution containing 0.3-3 M phosphoric acid and 0.1-2 M H 2 O 2 .
Claim 5
Dependent Claim
62 words
The method of claim 1, wherein the selected annular zone includes an annular inner diameter region of said coating corresponding substantially to the landing zone of a read-write head in a thin-film medium, said other zones include the annular outer-diameter region of the coating outside the inner diameter region, and said masking includes placing an annular seal against such outer annular region.
Claim 6
Dependent Claim
37 words
The method of claim 4, wherein said outer annular region is exposed to such etchant for a period sufficient to produce a selected roughness and summit density which is less than that of the inner diameter region.
Claim 7
Dependent Claim
41 words
The method of claim 1, wherein said exposing includes forming a photoresist layer on said coating, exposing the photoresist layer in such selected annular zone, removing the exposed portion of the photoresist layer, and contacting the coated substrate with such etchant.
Claim 8
Dependent Claim
31 words
The method of claim 1, wherein said exposing is effective to produce an isotropic summit density of between about 500-20,000/mm 2 and an arithmetic mean roughness value between about 20-70 Å.
Claim 9
Dependent Claim
22 words
The method of claim 7, wherein said exposing is effective to produce an isotropic summit density of between about 6,000-10,000/mm 2 .
Claim 10
Independent Claim
191 words
A method of texturing a polished metal annular-surface coating on a thin-film medium substrate, to produce a first substantially isotropic texture with a selected roughness and summit density, in an annular inner diameter region of the coating corresponding substantially to the landing zone of a read-write head in a thin-film medium, and a second substantially isotropic texture with a roughness and summit density which are substantially less than that of the selected summit density, in an annular outer diameter region of the coating, for use in preparing a thin-film medium for operation at a flying height of less than about 1 micro-inch, comprising exposing such annular inner-diameter zone to a chemical etchant effective to etch such coating, for an exposure period sufficient to produce such selected texture having a summit density between about 500-20,000/mm 2 , and an arithmetic mean roughness value between about 20 and 70 Å, exposing such annular outer diameter zone to a chemical etchant effective to etch such coating, for an exposure period sufficient to produce such second texture having an arithmetic roughness value between about 10 and 50 Å, and removing such etchant from the coating.
Claim 11
Independent Claim
191 words
A method of texturing a polished metal annular-surface coating on a thin-film medium substrate, to produce a first substantially isotropic texture with a selected roughness and summit density, in an annular inner diameter region of the coating corresponding substantially to the landing zone of a read-write head in a thin-film medium, and a second substantially isotropic texture with a roughness and summit density which are substantially less than that of the selected summit density, in an annular outer diameter region of the coating, for use in preparing a thin-film medium for operation at a flying height of less than about 1 micro-inch, comprising exposing such annular inner-diameter zone to a chemical etchant effective to etch such coating, for an exposure period sufficient to produce such selected texture having a summit density between about 500-20,000/mm 2 , and an arithmetic mean roughness value between about 20 and 70 Å, exposing such annular outer diameter zone to a chemical etchant effective to etch such coating, for an exposure period sufficient to produce such second texture having an arithmetic roughness value between about 10 and 50 Å, and removing such etchant from the coating.
Claim 12
Dependent Claim
43 words
The method of claim 9, wherein said coating contains between 86 and 93 atom percent nickel and 7 and 14 atom percent phosphorus, and said etchant contains 1-10 M nitric acid, 0.1-2 M phosphoric acid, and 0.1-1 M H 2 O 2 .
Claim 13
Dependent Claim
29 words
The method of claim 10, wherein said removing includes contacting the etching coating with a solution containing 0.3-3 M phosphoric acid and 0.1-2 M H 2 O 2 .
Claim 14
Dependent Claim
49 words
The method of claim 10, wherein the second exposing step is carried out during a portion of the first exposing step, employing a common chemical etchant for both steps, and masking said annular outer-diameter zone during a portion of the period of etchant exposure to the annular inner-diameter zone.
Claim 15
Dependent Claim
72 words
A substrate for use in a thin-film magnetic medium, comprising a annular support, and an annular metal coating formed on the support, and characterized by a substantially isotropic texture with a selected roughness and summit density in a selected annular zone of the coating which includes the landing zone of a read-write head in a thin-film medium, and a lesser roughness in a region of the disc outside the selected annular zone.
Claim 16
Dependent Claim
72 words
A substrate for use in a thin-film magnetic medium, comprising a annular support, and an annular metal coating formed on the support, and characterized by a substantially isotropic texture with a selected roughness and summit density in a selected annular zone of the coating which includes the landing zone of a read-write head in a thin-film medium, and a lesser roughness in a region of the disc outside the selected annular zone.
Claim 17
Dependent Claim
27 words
The substrate of claim 13, wherein said annular inner-diameter region has a summit density between about 500-20,000/mm 2 and an arithmetic mean roughness between about 20-70 Å.
Claim 18
Dependent Claim
23 words
The substrate of claim 14, wherein said annular outer-diameter region has an arithmetic mean roughness of between about 10 and 50 521 .
Claim 19
Dependent Claim
36 words
The substrate of claim 13, wherein the annular, outer-diameter region of the coating which lies outside the annular inner-diameter region is characterized by a substantially isotropic texture having a summit density between about 500-20,000/mm 2 .
Claim 20
Dependent Claim
39 words
The substrate of claim 13, which further includes, layered in succession over said coating, a chromium underlayer, a magnetic thin-film layer, and a carbon overcoat, forming a thin film medium with a surface roughness less than about 0.5 μinch.
References Cited (Backward Citations)
US4726006A
Cited
USPTO Annuity & Maintenance Windows
| Annuity Stage | Window Opens | Payment Deadline | Surcharge Period Until | Estimated Fee | Status |
|---|---|---|---|---|---|
| 3.5 Years (Year 4) | 1995-11-24 | 1996-05-25 | 1996-11-24 | $2000.00 | Window Closed / Lapsed |
| 7.5 Years (Year 8) | 1999-11-24 | 2000-05-25 | 2000-11-24 | $3760.00 | Window Closed / Lapsed |
| 11.5 Years (Year 12) | 2003-11-24 | 2004-05-25 | 2004-11-24 | $7700.00 | Window Closed / Lapsed |