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US5151238A Expired / Lapsed US ⏱️ 0.0 years remaining

Process for producing composite materials

Assignee: BTG International Ltd
•
Filing: 1989-06-05
•
Granted: 1992-09-29
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Expires: 2009-06-05
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Abstract

Abstract Process for producing a composite material in which a cellulosic substrate is treated with a solution of a polyfunctional isocyanate in an aprotic swelling solvent and the substrate is then compressed to form the composite material. The substrate may take the form of wood chips, wood particles, wood flakes, wood fibers, wood flour, ground wood, wood veneers and wood laminates, paper, card, straw, refined cellulose such as cotton or viscose and plant fibers such as bamboo or palm fiber.

Inventors

  • 👤 Harold A. Earl
  • 👤 William B. Banks

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-11-04 23:02
CPC Classifications
C; C08; C08G; C08G18/00; C08G18/06; C08G18/28; C08G18/40; C08G18/64; C08G18/6484; C08L; C08L97/00; C08L97/02

Claims Analysis

Total Claims: 12
Claim 1
Independent Claim 55 words
A process for the production of a composite material, which process comprises the steps of: immersing a cellulosic substrate in a solution of a di-functional isocyanate in an aprotic swelling solvent to cause said cellulosic substrate to swell, said cellulosic substrate reacting with said isocyanate; and then compressing the substrate to form a composite material.
Claim 2
Dependent Claim 55 words
A process for the production of a composite material, which process comprises the steps of: immersing a cellulosic substrate in a solution of a di-functional isocyanate in an aprotic swelling solvent to cause said cellulosic substrate to swell, said cellulosic substrate reacting with said isocyanate; and then compressing the substrate to form a composite material.
Claim 3
Dependent Claim 18 words
A process according to claim 1 wherein the solution comprises from 0.1 to 5.0 moles/liter of di-functional isocyanate.
Claim 4
Dependent Claim 13 words
A process according to claim 1 wherein the di-functional isocyanate is a polyisocyanate.
Claim 5
Dependent Claim 13 words
A process according to claim 3 wherein the di-functional isocyanate is a di-isocyanate.
Claim 6
Dependent Claim 28 words
A process according to claim 4 wherein the di-isocyanate is selected from the group, consisting of hexamethylene diisocyanate, 2,4 toluene diisocyanate, 2,6 toluene diisocyanate and diphenyl methane diisocyanate.
Claim 7
Dependent Claim 21 words
A process according to claim 1 wherein the immersing is carried out for a period of from 0.02 to 200 hours.
Claim 8
Dependent Claim 20 words
A process according to claim 1 wherein the solvent is selected from the group consisting of pyridine, acetone and 2-methyl-2-pyrrolidinones.
Claim 9
Dependent Claim 23 words
A process according to claim 1 characterised in that the immersing is carried out at a temperature of from 25° to 150° C.
Claim 10
Dependent Claim 21 words
A process according to claim 1 characterised in that the compressing carried out at a temperature of less than 200° C.
Claim 11
Dependent Claim 23 words
A process according to claim 9 characterised in that the compressing is carried out at a temperature of from 125° to 175° C.
Claim 12
Dependent Claim 22 words
A process according to claim 1 characterised in that the compressing is applied for a period of from 2 to 30 minutes.

References Cited (Backward Citations)

GB1148016A Cited
FR2127925A5 Cited
US3930097A Cited
US3870665A Cited
US4029846A Cited
GB2076414A Cited
JPS58189278A Cited
US4623499A Cited
US4752637A Cited

USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1995-09-29 1996-03-30 1996-09-29 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 1999-09-29 2000-03-30 2000-09-29 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 2003-09-29 2004-03-30 2004-09-29 $7700.00 Window Closed / Lapsed

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