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US5124091A Expired / Lapsed US ⏱️ 0.0 years remaining

Process for producing fine powders by hot substrate microatomization

Assignee: Global Tungsten and Powders LLC
•
Filing: 1991-05-17
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Granted: 1992-06-23
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Expires: 2011-05-17
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Abstract

Abstract A process for producing fine powder, which includes entraining a starting powder material in a carrier gas, injecting the starting powder material using the carrier gas into a high temperature jet to form a high velocity stream of molten droplets, fragmenting the resulting high velocity molten droplets by impacting against a substrate wherein the temperature of the substrate is above the melting point of the powder material, to form smaller droplets, and allowing the resulting fragmented smaller droplets to spheroidize and solidify in flight.

Inventors

  • 👤 Muktesh Paliwal
  • 👤 Robert J. Holland, Sr.

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-10-27 11:26
CPC Classifications
B; B22; B22F; B22F9/00; B22F9/02; B22F9/06; B22F9/08; B22F9/082; B01; B01J; B01J2/00; B01J2/02; B01J2/04; B22F1/00; B22F1/06; B22F1/065

Claims Analysis

Total Claims: 9
Claim 1
Independent Claim 113 words
A process for producing fine powder, said process comprising: a) entraining a starting powder material in a carrier gas; b) injecting said starting powder material using said carrier gas into a high temperature direct current plasma jet to form a high velocity stream of molten droplets; c) fragmenting said high velocity stream of molten droplets by impacting said droplets against a substrate to form smaller droplets wherein the temperature of said substrate is above the melting point of said starting powder material, said temperature being maintained by heating said substrate, said substrate being formed from a tungsten based material; and d) allowing the resulting fragmented smaller droplets to spheroidize and solidify in flight.
Claim 2
Dependent Claim 113 words
A process for producing fine powder, said process comprising: a) entraining a starting powder material in a carrier gas; b) injecting said starting powder material using said carrier gas into a high temperature direct current plasma jet to form a high velocity stream of molten droplets; c) fragmenting said high velocity stream of molten droplets by impacting said droplets against a substrate to form smaller droplets wherein the temperature of said substrate is above the melting point of said starting powder material, said temperature being maintained by heating said substrate, said substrate being formed from a tungsten based material; and d) allowing the resulting fragmented smaller droplets to spheroidize and solidify in flight.
Claim 3
Dependent Claim 27 words
A process of claim 1 wherein said starting powder material is selected from the group consisting of metal powders, metal alloy powders, ceramic based powders, and glasses.
Claim 4
Dependent Claim 25 words
A process of claim 1 wherein said substrate is made of material selected from the group consisting of metals, metal alloys, ceramics and combinations thereof.
Claim 5
Dependent Claim 17 words
A process of claim 1 wherein said powder is copper and said substrate is a tungsten-based material.
Claim 6
Dependent Claim 115 words
A process for producing fine powder, said process comprising: a) entraining a starting powder material in a carrier gas; b) injecting said starting powder material using said carrier gas into a high temperature direct current plasma jet to form a high velocity stream of molten droplets; c) fragmenting said high velocity stream of molten droplets by impacting said droplets against a substrate to form smaller droplets wherein the temperature of said substrate is above the melting point of said starting powder material, said temperature being maintained by heating said substrate including direct heating from said high temperature direct current plasma jet; and d) allowing the resulting fragmented smaller droplets to spheroidize and solidify in flight.
Claim 7
Dependent Claim 115 words
A process for producing fine powder, said process comprising: a) entraining a starting powder material in a carrier gas; b) injecting said starting powder material using said carrier gas into a high temperature direct current plasma jet to form a high velocity stream of molten droplets; c) fragmenting said high velocity stream of molten droplets by impacting said droplets against a substrate to form smaller droplets wherein the temperature of said substrate is above the melting point of said starting powder material, said temperature being maintained by heating said substrate including direct heating from said high temperature direct current plasma jet; and d) allowing the resulting fragmented smaller droplets to spheroidize and solidify in flight.
Claim 8
Dependent Claim 22 words
The process of claim 5 wherein the particle size of said starting powder material is less than about 100 micrometers in diameter.
Claim 9
Dependent Claim 25 words
The process of claim 5 wherein the particle size of the fine powder produced by the process is less than about 20 micrometers in diameter.

References Cited (Backward Citations)

US2699576A Cited
US2728107A Cited
US4435342A Cited
US4592781A Cited
US4781741A Cited
US4952144A Cited
US5076991A Cited
US4816067A Cited

USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1995-06-23 1995-12-23 1996-06-23 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 1999-06-23 1999-12-23 2000-06-23 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 2003-06-23 2003-12-23 2004-06-23 $7700.00 Window Closed / Lapsed

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