US5074898A
Expired / Lapsed
US
⏱️ 0.0 years remaining
Cryogenic air separation method for the production of oxygen and medium pressure nitrogen
Assignee: Praxair Technology Inc
•
Filing: 1990-04-03
•
Granted: 1991-12-24
•
Expires: 2010-04-03
Abstract
Abstract A cryogenic air separation method for the production of oxygen and medium pressure nitrogen comprising a primary higher pressure column and an auxiliary smaller lower pressure stripping column wherein primary column bottom liquid is employed as stripping column downflow liquid and primary column top vapor condenses against stripping column bottom liquid to generate stripping vapor.
Inventors
- 👤 Harry Cheung
Bibliographic Details
Application Number
—
Jurisdiction
US
Data Source
google_patents
Last Synchronized
2026-11-07 18:37
CPC Classifications
F; F25; F25J; F25J3/00; F25J3/02; F25J3/04; F25J3/04406; F25J3/0443; F25J3/04248; F25J3/04284; F25J3/0429; F25J3/04296; F25J2200/00; F25J2200/50; F25J2200/52; F25J2215/00; F25J2215/50; Y; Y10; Y10S; Y10S62/00; Y10S62/939; Y10S62/94
Claims Analysis
Total Claims: 10
Claim 1
Independent Claim
190 words
A cryogenic air separation method for the production of nitrogen at elevated pressure and oxygen comprising: (a) providing feed air into a primary column operating at a pressure within the range of from 40 to 95 psia and separating feed air in the primary column into nitrogen-rich vapor and oxygen-enriched liquid; (B) passing oxygen-enriched liquid into an auxiliary stripping column at the top of the stripping column which is operating at a pressure less than that of the primary column and which has one third or less equilibrium stages than the primary column; (C) passing oxygen-enriched liquid down the stripping column against upflowing vapor to produce oxygen-rich liquid; (D) recovering a first portion of the nitrogen-rich vapor as product elevated pressure nitrogen; (E) condensing a second portion of the nitrogen-rich vapor by indirect heat exchange with oxygen-rich liquid to produce oxygen-rich vapor; (F) passing oxygen-rich vapor up the stripping column as the upflowing vapor; and (G) recovering a portion of the oxygen-rich vapor as product oxygen, said oxygen-rich vapor portion taken from the stripping column at a point below the point where oxygen-enriched liquid is passed into the stripping column.
Claim 2
Dependent Claim
190 words
A cryogenic air separation method for the production of nitrogen at elevated pressure and oxygen comprising: (a) providing feed air into a primary column operating at a pressure within the range of from 40 to 95 psia and separating feed air in the primary column into nitrogen-rich vapor and oxygen-enriched liquid; (B) passing oxygen-enriched liquid into an auxiliary stripping column at the top of the stripping column which is operating at a pressure less than that of the primary column and which has one third or less equilibrium stages than the primary column; (C) passing oxygen-enriched liquid down the stripping column against upflowing vapor to produce oxygen-rich liquid; (D) recovering a first portion of the nitrogen-rich vapor as product elevated pressure nitrogen; (E) condensing a second portion of the nitrogen-rich vapor by indirect heat exchange with oxygen-rich liquid to produce oxygen-rich vapor; (F) passing oxygen-rich vapor up the stripping column as the upflowing vapor; and (G) recovering a portion of the oxygen-rich vapor as product oxygen, said oxygen-rich vapor portion taken from the stripping column at a point below the point where oxygen-enriched liquid is passed into the stripping column.
Claim 3
Dependent Claim
32 words
The method of claim 1 wherein the feed air is divided into a major portion and a minor portion, and the major portion is turboexpanded prior to introduction into the primary column.
Claim 4
Dependent Claim
19 words
The method of claim 2 wherein the major portion comprises from 55 to 99 percent of the feed air.
Claim 5
Dependent Claim
28 words
The method of claim 2 wherein some of the minor portion is condensed by indirect heat exchange against boiling oxygen-enriched liquid and then passed into the primary column.
Claim 6
Dependent Claim
23 words
The method of claim 1 further comprising recovering a portion of the condensed second portion of the nitrogen-rich vapor as product liquid nitrogen.
Claim 7
Dependent Claim
18 words
The method of claim 1 further comprising recovering a portion of the oxygen-rich liquid as product liquid oxygen.
Claim 8
Dependent Claim
20 words
The method of claim 1 further comprising cleaning the feed air by passage through a zeolite molecular sieve adsorbent bed.
Claim 9
Dependent Claim
22 words
The method of claim 7 further comprising passing vapor from the auxiliary stripping column through the adsorbent bed to regenerate the adsorbent.
Claim 10
Dependent Claim
45 words
The method of claim 1 wherein product nitrogen is recovered at a pressure within the range of from 40 to 95 psia and the combined recovery of oxygen and nitrogen product is at least 50 percent of the feed air introduced into the primary column.
References Cited (Backward Citations)
US3210947A
Cited
US3203193A
Cited
US3217502A
Cited
US3508412A
Cited
US3905201A
Cited
US3736762A
Cited
US4224045A
Cited
US4400188A
Cited
US4555256A
Cited
US4496383A
Cited
US4416677A
Cited
US4439220A
Cited
US4617040A
Cited
US4560397A
Cited
US4617037A
Cited
US4594085A
Cited
US4704148A
Cited
US4715874A
Cited
US4783208A
Cited
US4775399A
Cited
US4783210A
Cited
US4871382A
Cited
US4806136A
Cited
US4834785A
Cited
US4848996A
Cited
US4957524A
Cited
USPTO Annuity & Maintenance Windows
| Annuity Stage | Window Opens | Payment Deadline | Surcharge Period Until | Estimated Fee | Status |
|---|---|---|---|---|---|
| 3.5 Years (Year 4) | 1994-12-23 | 1995-06-24 | 1995-12-24 | $2000.00 | Window Closed / Lapsed |
| 7.5 Years (Year 8) | 1998-12-23 | 1999-06-24 | 1999-12-24 | $3760.00 | Window Closed / Lapsed |
| 11.5 Years (Year 12) | 2002-12-23 | 2003-06-24 | 2003-12-24 | $7700.00 | Window Closed / Lapsed |