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US5061665A Expired / Lapsed US ⏱️ 0.0 years remaining

Process for producing an improved alumina-zirconia composite sintered material

Assignee: Japan Carlit Co Ltd
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Filing: 1990-01-08
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Granted: 1991-10-29
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Expires: 2010-01-08
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Abstract

Abstract Improved alumina-zirconia composite sintered materials with sufficient high mechanical strength and thermal shock resistance as well as excellent hardwearing resistance are made by mixing, heating and melting zirconia and alumina, then the produced melt was quenched, and the resulting solid was ground and milled while adding thereto at least one compound of ceria and/or titania, to an average grain size of from about 0.5 to about 1.5 mu m, and subjected the resulting powder to molding and sintering at a temperature of from 1450 DEG to about 1600 DEG C., said zirconia, ceria and titania being employed in the amount of about 10-20%, about 3-7%, and about 15-25% by weight, respectively, plus the balance of alumina. Said sintered materials are useful for employment in structural materials, refractorial materials, erosion resistance materials, cutting tool materials, grinding and polishing materials, etc.

Inventors

  • 👤 Ichiro Seki
  • 👤 Akihiro Kano
  • 👤 Toshiki Hasegawa
  • 👤 Minoru Abe
  • 👤 Isao Isa

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-11-09 05:48
CPC Classifications
C; C09; C09K; C09K3/00; C09K3/14; C09K3/1409; C09K3/1427; C04; C04B; C04B35/00; C04B35/01; C04B35/48; C04B35/484

Claims Analysis

Total Claims: 8
Claim 1
Independent Claim 95 words
A process for producing an alumina-zirconia composite sintered material comprising mixing, heating and melting zirconia and alumina to form a melt, then quenching said melt to form solids, grinding and milling said solids while admixing ceria therewith to powder having an average grain size of about 0.5 to about 1.5 μm, and molding and sintering said powder at a temperature of about 1450° to about 1600° C., said zirconia and ceria being employed in the amounts of about 10% to 20%, and about 3% to about 7% by weight, respectively, with the balance being alumina.
Claim 2
Dependent Claim 95 words
A process for producing an alumina-zirconia composite sintered material comprising mixing, heating and melting zirconia and alumina to form a melt, then quenching said melt to form solids, grinding and milling said solids while admixing ceria therewith to powder having an average grain size of about 0.5 to about 1.5 μm, and molding and sintering said powder at a temperature of about 1450° to about 1600° C., said zirconia and ceria being employed in the amounts of about 10% to 20%, and about 3% to about 7% by weight, respectively, with the balance being alumina.
Claim 3
Dependent Claim 28 words
The process according to claim 1, wherein the zirconia, ceria and alumina are employed in amounts of 10 weight %, 3 weight % and 87 weight %, respectively.
Claim 4
Dependent Claim 28 words
The process according to claim 1, wherein the zirconia, ceria and alumina are employed in amounts of 15 weight %, 5 weight % and 80 weight %, respectively.
Claim 5
Dependent Claim 28 words
The process according to claim 1, wherein the zirconia, ceria and alumina are employed in amounts of 20 weight %, 7 weight % and 73 weight %, respectively.
Claim 6
Dependent Claim 28 words
The process according to claim 1, wherein the zirconia, ceria and alumina are employed in amounts of 10 weight %, 7 weight % and 83 weight %, respectively.
Claim 7
Dependent Claim 28 words
The process according to claim 1, wherein the zirconia, ceria and alumina are employed in amounts of 20 weight %, 3 weight % and 77 weight %, respectively.
Claim 8
Dependent Claim 28 words
The process according to claim 2, which further comprises also admixing titania while grinding and milling, said titania being in an amount of 15 to 25% by weight.

USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1994-10-28 1995-04-29 1995-10-29 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 1998-10-28 1999-04-29 1999-10-29 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 2002-10-28 2003-04-29 2003-10-29 $7700.00 Window Closed / Lapsed

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