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US5039711A Expired / Lapsed US ⏱️ 0.0 years remaining

Production of flame-retardant polyol-oxidated silicon-acidic boron emulsion

Assignee: Individual
•
Filing: 1989-09-25
•
Granted: 1991-08-13
•
Expires: 2009-09-25
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Abstract

Abstract Stable flame-retardant polyol-oxidated silicon-acidic boron emulsions are produced by mixing and reacting a liquid organic polyol, and oxidated silicon compound and an acidic boron compound. This flame-retardant emulsion is useful in the production of flame-retardant polyurethane, polyester and polyesteramide products.

Inventors

  • 👤 David H. Blount

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-11-05 07:28
CPC Classifications
C; C08; C08K; C08K3/00; C08K3/38; C08G; C08G18/00; C08G18/06; C08G18/08; C08G18/0838; C08G18/0842; C08G18/0861; C08G18/0871; C08G18/0876; C08G18/28; C08G18/30; C08G18/38; C08G18/3893; C08G18/3895; C08G18/3897; C08G18/40; C08G18/42; C08G18/46; C08G18/4692; C08G18/48; C08G18/50; C08G18/5096; C08G2101/00

Claims Analysis

Total Claims: 28
Claim 1
Independent Claim 63 words
The process for the production of flame-retarded liquid polyol-oxidated silicon-acidic boron emulsion which process consist of emulsifying and reacting the following components: (A) oxidated silicon compound in the amount of 1 to 100 parts by weight; (B) acidic boron compound in the amount of 10 to 100 parts by weight; (C) liquid polyol in the amount of 50 to 200 parts by weight.
Claim 2
Dependent Claim 63 words
The process for the production of flame-retarded liquid polyol-oxidated silicon-acidic boron emulsion which process consist of emulsifying and reacting the following components: (A) oxidated silicon compound in the amount of 1 to 100 parts by weight; (B) acidic boron compound in the amount of 10 to 100 parts by weight; (C) liquid polyol in the amount of 50 to 200 parts by weight.
Claim 3
Dependent Claim 8 words
The product produced the process of claim 1.
Claim 4
Dependent Claim 33 words
The process of claim 1 wherein the oxidated silicon compound is selected from the group consisting of alkali metal silicates, alkaline earth metal silicates, hydrated oxidated silicon compounds, natural silicate and mixtures thereof.
Claim 5
Dependent Claim 13 words
The process of claim 1 wherein the acidic boron compound is boric acid.
Claim 6
Dependent Claim 31 words
The process of claim 1 wherein up to 20% by weight, based on weight of Components A, B and C of an emulsifier is added to components A, B or C.
Claim 7
Dependent Claim 31 words
The process claim 1 wherein up to 20% by weight, based on weight of Components A, B and C, of a foam stabilizer is added to Components A, B or C.
Claim 8
Dependent Claim 32 words
The process of claim 1 wherein up to 10% by weight, based on weight of Components A, B and C, of a dispersion stabilizer is added to Components A, B or C.
Claim 9
Dependent Claim 34 words
The process of claim 1 wherein the liquid polyol is selected from the group consisting of polyhydric alcohol, polyesters, polyethers, polythioethers, polyacetals, polycarbonates, polyester amides containing at least 2 hydroxy groups, and mixtures thereof.
Claim 10
Dependent Claim 44 words
The product produced by the process of claim 1 wherein an organic compound containing at least two isocyanate radicals in the amount of 25 to 300 parts by weight is added with Components A, B and C thereby producing a flame-retardant polyurethane silicate product.
Claim 11
Dependent Claim 75 words
The product produced by the process of claim 9 wherein up to 20% by weight of a foam stabilizer, up to 10% by weight of an amine urethane catalyst, up to 50% by weight of a blowing agent and up to 10% by weight of an organo-metal urethane catalyst is added to Components A, B and C, percentage based on weight of Components A, B and C, thereby producing a foamed flame-retardant polyurethane silicate product.
Claim 12
Dependent Claim 22 words
The product produced by the process of claim 9 wherein the compound containing at least 2 isocyanate radicals is an organic polyisocyanate.
Claim 13
Dependent Claim 37 words
The flame-retardant product produced by mixing and reacting the following components: (A) oxidated silicon compound (B) boric acid (C) liquid polyol (D) organic polyisocyanate (E) water (F) amine urethane catalyst (G) organo-metal urethane catalyst (H) foam stabilizer
Claim 14
Dependent Claim 37 words
The flame-retardant product produced by mixing and reacting the following components: (A) oxidated silicon compound (B) boric acid (C) liquid polyol (D) organic polyisocyanate (E) water (F) amine urethane catalyst (G) organo-metal urethane catalyst (H) foam stabilizer
Claim 15
Dependent Claim 40 words
The flame-retardant product produced by mixing and reacting the following components (A) oxidated silicon compound (B) boric acid (C) liquid polyol (D) organic polyisocyante (E) foam stabilizer (F) amine urethane catalyst (G) organic tin catalyst (H) blowing agent for urethanes
Claim 16
Dependent Claim 40 words
The flame-retardant product produced by mixing and reacting the following components (A) oxidated silicon compound (B) boric acid (C) liquid polyol (D) organic polyisocyante (E) foam stabilizer (F) amine urethane catalyst (G) organic tin catalyst (H) blowing agent for urethanes
Claim 17
Dependent Claim 38 words
The flame-retardant product produced by the process of claim 13 wherein up to 25 percent by weight of phase-change materials are added to Components A, B and C, percentage based on weight of Components A, B and C.
Claim 18
Dependent Claim 39 words
The flame-retardant product produced by the process of claim 13 wherein up to 300 percent by weight of a modifying compound is added to Components A, B or C, percentage based on weight of Components A, B and C.
Claim 19
Dependent Claim 40 words
The flame-retardant product produced by mixing and reacting the following components: (A) oxidated silicon compound (B) boric acid (C) polyol (D) compound containing one or more isocyanate radicals and one or more unsaturated bond which will polymerize (E) free-radical initiator
Claim 20
Dependent Claim 40 words
The flame-retardant product produced by mixing and reacting the following components: (A) oxidated silicon compound (B) boric acid (C) polyol (D) compound containing one or more isocyanate radicals and one or more unsaturated bond which will polymerize (E) free-radical initiator
Claim 21
Dependent Claim 43 words
The flame-retardant product produced by the process of claim 13 wherein up to 300 percent by weight of inorganic or organic particulates or pulverulent material is added to Compounents A, B and C, percentage based on weight of Components A, B and C.
Claim 22
Dependent Claim 18 words
The flame-retardant product produced by the process of claim 12 wherein the oxidated silicon compound is sodium silicate.
Claim 23
Dependent Claim 18 words
The flame-retardant product produced by the process of claim 13 wherein the oxidated silicon compound is sodium silicate.
Claim 24
Dependent Claim 21 words
The flame-retardant product produced by emulsifying and reacting the following components: (A) hydrated sodium silicate (B) boric acid (C) liquid polyol
Claim 25
Dependent Claim 21 words
The flame-retardant product produced by emulsifying and reacting the following components: (A) hydrated sodium silicate (B) boric acid (C) liquid polyol
Claim 26
Dependent Claim 42 words
The flame-retardant product produced by mixing and reacting 100 parts by weight of the flame-retardant liquid polyol-oxidated silicon-acidic boron emulsion produced by the process of claim 1 and 10 to 50 parts by weight of polycarboxylic acid and/or a polycarboxylic acid anhydride.
Claim 27
Dependent Claim 34 words
The process of claim 1 wherein liquid polyol and acidic boron compound is first mixed and reacted to produce a partically esterified polyol with acidic boron compounds before the oxidated silicon compound is added.
Claim 28
Dependent Claim 9 words
The product produced by the process of claim 22.

References Cited (Backward Citations)

US4306035A Cited
US4280006A Cited
US4760099A Cited

USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1994-08-12 1995-02-11 1995-08-13 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 1998-08-12 1999-02-11 1999-08-13 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 2002-08-12 2003-02-11 2003-08-13 $7700.00 Window Closed / Lapsed

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