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US5026671A Expired / Lapsed US ⏱️ 0.0 years remaining

Sintered silicon nitride and method for making the same

Assignee: NGK Insulators Ltd
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Filing: 1990-03-14
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Granted: 1991-06-25
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Expires: 2010-03-14
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Abstract

Abstract A sintered silicon nitride contains at least 90% of β-type silicon nitride, wherein said β-type silicon nitride consists essentially of 35 to 80% of large crystal particles with the remainder of small crystal particles, said large crystal particles having a mean particle length being at least two times as long as that of said small crystal particles. This sintered silicon nitride is obtained by a method wherein one batch of starting silicon nitride powders, whose primary particles have a mean particle size of 0.1 to 0.5 μm, and another batch of starting silicon nitride powders, whose primary particles have a mean particle size of 0.5 to 0.7 μm, are blended with a sintering aid or aids at a given weight ratio, and the thus obtained blend is formed or compacted and sintered.

Inventors

  • 👤 Shigeru Hanzawa
  • 👤 Hiroto Matsuda
  • 👤 Kouzi Fusimi

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-11-08 12:44
CPC Classifications
C; C04; C04B; C04B35/00; C04B35/515; C04B35/58; C04B35/584

Claims Analysis

Total Claims: 3
Claim 1
Independent Claim 91 words
A sintered silicon nitride comprising at least 90% of β-type silicon nitride, said β-type silicon nitride consisting essentially of 35 to 80% of large crystal particles having a mean particle length of 5.0 to 14 μm with the remainder being small crystal particles having a mean particle length of 0.5 to 5 μm, wherein the large and small crystal particles have an aspect ratio of at least 3 and the mean particle length of the large crystal particles is at least twice the mean particle length of the small crystal particles.
Claim 2
Dependent Claim 91 words
A sintered silicon nitride comprising at least 90% of β-type silicon nitride, said β-type silicon nitride consisting essentially of 35 to 80% of large crystal particles having a mean particle length of 5.0 to 14 μm with the remainder being small crystal particles having a mean particle length of 0.5 to 5 μm, wherein the large and small crystal particles have an aspect ratio of at least 3 and the mean particle length of the large crystal particles is at least twice the mean particle length of the small crystal particles.
Claim 3
Dependent Claim 95 words
A method for making a sintered silicon nitride as recited in claim 1, comprising blending a batch of silicon nitride powder A in which the primary particles have a mean particle size of 0.1 to 0.5 μm and a batch of silicon nitride powder B in which the primary particles have a mean particle size of 0.5 to 0.7 μm, the weight ratio of B/A being in the range of 35/65 to 80/20, with a sintering aid, forming or compacting the blend and then sintering the blend so as to obtain the sintered silicon nitride.

References Cited (Backward Citations)

US4073845A Cited
US4225356A Cited
US4365022A Cited
JPS6321254A Cited
EP0276334A1 Cited

USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1994-06-24 1994-12-24 1995-06-25 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 1998-06-24 1998-12-24 1999-06-25 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 2002-06-24 2002-12-24 2003-06-25 $7700.00 Window Closed / Lapsed

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