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US5026427A Expired / Lapsed US ⏱️ 0.0 years remaining

Process for making pigmented ink jet inks

Assignee: EIDP Inc
•
Filing: 1988-10-12
•
Granted: 1991-06-25
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Expires: 2008-10-12
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Abstract

Abstract In accordance with this invention there is provided a process for the preparation of pigmented ink jet inks comprising: (a) mixing at least one pigment and at least one pigment dispersant in a dispersant medium to form a pigmented ink mixture wherein pigment is present in an amount up to 60% by weight based on the total weight of the mixture; (b) deflocculating the pigmented ink mixture by passing the pigmented ink mixture through at least a plurality of nozzles within a liquid jet interaction chamber at a liquid pressure of at least 1,000 psi to produce a substantially uniform dispersion of pigment particles in the dispersant medium.

Inventors

  • 👤 Robert D. Mitchell
  • 👤 Torence J. Trout

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-10-26 09:19
CPC Classifications
C; C09; C09D; C09D11/00; C09D11/30; C09D11/32; C09D11/324; C09D11/326; C09D11/322; B; B01; B01F; B01F23/00; B01F23/50; B01F23/51; B01F33/00; B01F33/80; B01F33/82; B01F33/821; C09D11/38; B01F2101/00; B01F2101/35; B01F23/56; B01F25/00; B01F25/20

Claims Analysis

Total Claims: 11
Claim 1
Independent Claim 124 words
A process for the preparation of pigmented ink jet inks comprising: (a) mixing at least one pigment and at least one water soluble pigment dispersant in a carrier liquid selected from the group consisting of water or a mixture of water and at least one water-soluble organic solvent to form a pigmented ink mixture wherein pigment is present in an amount from about 0.1% to about 30% by weight based on the total weight of the mixture; and (b) deflocculating the pigmented ink mixture by passing the pigmented ink mixture through at least a plurality of nozzles within a liquid jet interaction chamber at a liquid pressure of at least 1,000 psi to produce a substantially uniform dispersion of pigment in the carrier liquid.
Claim 2
Dependent Claim 124 words
A process for the preparation of pigmented ink jet inks comprising: (a) mixing at least one pigment and at least one water soluble pigment dispersant in a carrier liquid selected from the group consisting of water or a mixture of water and at least one water-soluble organic solvent to form a pigmented ink mixture wherein pigment is present in an amount from about 0.1% to about 30% by weight based on the total weight of the mixture; and (b) deflocculating the pigmented ink mixture by passing the pigmented ink mixture through at least a plurality of nozzles within a liquid jet interaction chamber at a liquid pressure of at least 1,000 psi to produce a substantially uniform dispersion of pigment in the carrier liquid.
Claim 3
Dependent Claim 74 words
A process according to claim 1 wherein the pigmented ink is diluted with at least one liquid which is compatible with the carrier liquid to form an ink containing pigment in the range of 0.1% to 10% by weight based on the total weight of the mixture when the mixture of step (a) has pigment present in an amount exceeding 10%, said dilution being made either before or after the deflocculation of step (b).
Claim 4
Dependent Claim 21 words
A process according to claim 1 wherein the dispersant is selected from the group consisting of surfactants and polymeric pigment dispersants.
Claim 5
Dependent Claim 156 words
A process according to claim 1 wherein the the liquid jet interaction chamber comprises, in combination, (a) a plurality of submerged nozzles providing elongated orifices arranged to eject under pressure a plurality of thin sheets of the pigmented ink jet mixture, the nozzles being arranged to effect turbulent jet action of the sheets along a common liquid jet interaction front and the sheets being ejected by the nozzles into a low pressure zone filled with the liquid futher creating turbulent jet interaction along a common boundary essentially defined and formed by the mixture in the low pressure zone and by the sheets ejected into the low pressure zone; (b) jet interaction chamber-defining means arranged to provide the low pressure to the nozzles; and (c) inlet channel means to deliver the mixture under pressure to the nozzles; and (d) means to withdraw the pigmented ink mixture in the form of a dispersion from the low pressure zone.
Claim 6
Dependent Claim 16 words
A process according to claim 2 wherein the pigmented ink is diluted with the dispersant medium.
Claim 7
Dependent Claim 28 words
A process according to claim 1 wherein the mixing in step (a) is conducted in liquid jet interaction chamber at a liquid pressure of at least 1000 psi.
Claim 8
Dependent Claim 155 words
A process according to claim 6 wherein the liquid jet interaction chamber comprises, in combination, (a) a plurality of submerged nozzles providing elongated orifices arranged to eject under pressure a plurality of thin sheets of the pigmented ink jet mixture, the nozzles being arranged to effect turbulent jet action of the sheets along a common liquid jet interaction front and the sheets being ejected by the nozzles into a low pressure zone filled with the liquid futher creating turbulent jet interaction along a common boundary essentially defined and formed by the mixture in the low pressure zone and by the sheets ejected into the low pressure zone; (b) jet interaction chamber-defining means arranged to provide the low pressure to the nozzles; and (c) inlet channel means to deliver the mixture under pressure to the nozzles; and (d) means to withdraw the pigmented ink mixture in the form of a dispersion from the low pressure zone.
Claim 9
Dependent Claim 25 words
A process according to claim 1 wherein the surface tension of the ink is in the range of about 20 dyne/cm to about 70 dyne/cm.
Claim 10
Dependent Claim 24 words
A process according to claim 1 wherein the viscosity of the ink is in the range of about 1.0 cP to about 5.0 cP.
Claim 11
Dependent Claim 28 words
A process according to claim 1 wherein the ink mixture contains at least one additive selected from the group consisting of biocides, humectants, chelating agents, and viscosity modifiers.

References Cited (Backward Citations)

GB818489A Cited
US4365035A Cited
US4597794A Cited
US4533254A Cited
JPS6157669A Cited
JPS61168677A Cited
US4742098A Cited
US4692188A Cited
EP0284034A2 Cited
US4783389A Cited

USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1994-06-24 1994-12-24 1995-06-25 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 1998-06-24 1998-12-24 1999-06-25 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 2002-06-24 2002-12-24 2003-06-25 $7700.00 Window Closed / Lapsed

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