US5019423A
Expired / Lapsed
US
⏱️ 0.0 years remaining
Equipment and method for supply of organic metal compound
Assignee: Mitsui Toatsu Chemicals Inc
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Filing: 1988-12-21
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Granted: 1991-05-28
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Expires: 2008-12-21
Abstract
Abstract Supply equipment for providing a stable supply of feed gas of an organic metal compound at a constant concentration comprises a cylindrical vessel with an organic metal compound housed, an inlet tube of carrier gas for vaporizing said organic metal compound, an outlet tube for letting out the carrier gas substantially saturated with the vaporized organic metal compound, a room provided in the lower part of the vessel which is connected to said carrier gas inlet tube, a packed bed of an organic metal compound formed above said room, and a partition with a plurarity of pores partitioning said room and said packed bed.
Inventors
- 👤 Atsuhiko Hiai
- 👤 Kazuo Wakimura
Bibliographic Details
Application Number
—
Jurisdiction
US
Data Source
google_patents
Last Synchronized
2026-11-09 07:22
CPC Classifications
C; C03; C03B; C03B31/00; C23; C23C; C23C16/00; C23C16/44; C23C16/448; C23C16/4481; B; B01; B01J; B01J7/00
Claims Analysis
Total Claims: 11
Claim 1
Independent Claim
211 words
Supply equipment for stable supply of feed gas of an organic metal compound at a constant concentration which comprises a generally cylindrical vessel having a solid organic metal compound housed therein, said vessel comprising an upper cylinder supported on and extending upwardly from a smaller diameter, coaxial lower cylinder, an inlet tube communicating with said lower cylinder for providing carrier gas for vaporizing said organic metal compound, an outlet tube communicating with said upper cylinder for letting out the carrier gas substantially saturated with the vaporized organic metal compound, a room provided in the lower part of the lower cylinder of the vessel, said room being connected to said carrier gas inlet tube, a packet bed of a solid organic metal compound formed above said room and extending upwardly from said lower cylinder into said upper cylinder, and a partition with a plurality of pores in said lower cylinder partitioning said room and said packed bed, the carrier gas introduced into said room in said lower cylinder being passed through said partition to and through said packed bed whereby it becomes substantially saturated with the organic metal compound, said organic metal compound-saturated carrier gas emerging from said packed bed into said upper cylinder and exiting said equipment through said outlet tube.
Claim 2
Dependent Claim
211 words
Supply equipment for stable supply of feed gas of an organic metal compound at a constant concentration which comprises a generally cylindrical vessel having a solid organic metal compound housed therein, said vessel comprising an upper cylinder supported on and extending upwardly from a smaller diameter, coaxial lower cylinder, an inlet tube communicating with said lower cylinder for providing carrier gas for vaporizing said organic metal compound, an outlet tube communicating with said upper cylinder for letting out the carrier gas substantially saturated with the vaporized organic metal compound, a room provided in the lower part of the lower cylinder of the vessel, said room being connected to said carrier gas inlet tube, a packet bed of a solid organic metal compound formed above said room and extending upwardly from said lower cylinder into said upper cylinder, and a partition with a plurality of pores in said lower cylinder partitioning said room and said packed bed, the carrier gas introduced into said room in said lower cylinder being passed through said partition to and through said packed bed whereby it becomes substantially saturated with the organic metal compound, said organic metal compound-saturated carrier gas emerging from said packed bed into said upper cylinder and exiting said equipment through said outlet tube.
Claim 3
Dependent Claim
12 words
Equipment according to claim 1 wherein the organic metal compound is solid.
Claim 4
Dependent Claim
22 words
Equipment according to claim 1 wherein the portion above the partition in the vessel is substantially filled with the organic metal compound.
Claim 5
Dependent Claim
12 words
Equipment according to claim 1 wherein the partition is a multipore plate.
Claim 6
Dependent Claim
11 words
Equipment according to claim 1 wherein the partition is a mesh.
Claim 7
Dependent Claim
12 words
Equipment according to claim 1 wherein the partition is a perforated plate.
Claim 8
Dependent Claim
16 words
Equipment according to claim 1 including a tapered section interconnecting said upper cylinder and lower cylinder.
Claim 9
Dependent Claim
21 words
Equipment according to claim 1 wherein the carrier gas inlet tube and the outlet tube are respectively provided with a valve.
Claim 10
Dependent Claim
130 words
Method for providing stable supply of feed gas substantially saturated with an organic metal compound which comprises soaking the equipment of claim 1 in a thermostatic chamber, introducing carrier gas into said lower cylinder through a carrier gas inlet tube maintained at a constant temperature sufficient to vaporize said solid organic metal compound, and flowing said carrier gas through said packed bed to vaporize said solid organic metal compound thereby substantially saturating the gas with the compound, said compound-saturated carrier gas emerging from said packed bed into said upper cylinder at a decreased gas flow rate relative to said gas flow rate through said lower cylinder for avoiding association of fine particles of said solid organic metal compound with said carrier gas as said compound-saturated carrier gas exits said vessel.
Claim 11
Dependent Claim
25 words
Method according to claim 9 wherein the gas substantially saturated with the organic metal compound is suitable for use as feed gas for film formation.
References Cited (Backward Citations)
USPTO Annuity & Maintenance Windows
| Annuity Stage | Window Opens | Payment Deadline | Surcharge Period Until | Estimated Fee | Status |
|---|---|---|---|---|---|
| 3.5 Years (Year 4) | 1994-05-27 | 1994-11-26 | 1995-05-28 | $2000.00 | Window Closed / Lapsed |
| 7.5 Years (Year 8) | 1998-05-27 | 1998-11-26 | 1999-05-28 | $3760.00 | Window Closed / Lapsed |
| 11.5 Years (Year 12) | 2002-05-27 | 2002-11-26 | 2003-05-28 | $7700.00 | Window Closed / Lapsed |