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US5017785A Expired / Lapsed US ⏱️ 0.0 years remaining

IR-spectrometric analyzing procedure and means

Assignee: Dailab Inc Oy
•
Filing: 1989-12-07
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Granted: 1991-05-21
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Expires: 2009-12-07
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Abstract

Abstract An IR-spectrometric analyzing procedure, the measuring absorbance and reference absorbance being detected simultaneously from an IR light beam conducted to pass through the sample and diffracted to a spectrum. An IR spectrometer comprising a light source (1), a sample cuvette (5), a diffraction member (6), detectors (7) and a calculating means (9) for determining the content values of the sample corresponding to the measuring absorbance, the detectors (7) having been arranged to detect the measuring absorbance and the reference absorbance simultaneously from the beam that has passed through the sample and been diffracted to a spectrum.

Inventors

  • 👤 Jaakko Rasanen

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-11-02 16:24
CPC Classifications
G; G01; G01N; G01N21/00; G01N21/17; G01N21/25; G01N21/31; G01N21/35; G01J; G01J3/00; G01J3/12; G01J3/18; G01J3/20; G01J3/28; G01J3/42; G01J3/427; G01N33/00; G01N33/02; G01N33/04; G01J3/30; G01J3/36; G01N21/3577

Claims Analysis

Total Claims: 16
Claim 1
Independent Claim 140 words
An IR-spectrometric analyzing procedure for analyzing the components of a dispersed system subject to turbulence affecting the spectrometric analysis, wherein an IR light beam is produced; the IR light beam is conducted through a single sample cuvette containing the sample; the IR light beam thus obtained is diffracted to a spectrum; the measuring the absorbance and reference absorbance are detected at a plurality of pairs of predetermined, fixed, adjacent points in the spectrum by dual beam detectors and a quantitative analysis value is determined from the ratio of the difference between the pairs of detected measuring and reference absorbances, characterized in that the pairs of measuring absorbance and reference absorbance are detected simultaneously from the IR light beam conducted through the single sample and diffracted to a spectrum and detected at predetermined pairs of fixed points by dual beam detectors.
Claim 2
Dependent Claim 140 words
An IR-spectrometric analyzing procedure for analyzing the components of a dispersed system subject to turbulence affecting the spectrometric analysis, wherein an IR light beam is produced; the IR light beam is conducted through a single sample cuvette containing the sample; the IR light beam thus obtained is diffracted to a spectrum; the measuring the absorbance and reference absorbance are detected at a plurality of pairs of predetermined, fixed, adjacent points in the spectrum by dual beam detectors and a quantitative analysis value is determined from the ratio of the difference between the pairs of detected measuring and reference absorbances, characterized in that the pairs of measuring absorbance and reference absorbance are detected simultaneously from the IR light beam conducted through the single sample and diffracted to a spectrum and detected at predetermined pairs of fixed points by dual beam detectors.
Claim 3
Dependent Claim 49 words
Procedure according to claim 1, characterized in that the IR beam is conducted from the single sample to a diffraction member placed substantially on the periphery of a circle and the measuring absorbance and reference absorbance are detected at a plurality of peripheral adjacent points of the same circle.
Claim 4
Dependent Claim 27 words
Procedure according to claim 1, characterized in that each measuring absorbance and reference absorbance pair is detected in two mutually adjacent wavelength intervals of he IR spectrum.
Claim 5
Dependent Claim 32 words
Procedure according to claim 3, characterized in that each measuring absorbance is detected at a peak of the IR spectrum, and each reference absorbance at a minimum immediately adjacent to said peak.
Claim 6
Dependent Claim 23 words
Procedure according to claim 4, characterized in that the difference of the measuring and reference absorbances is formed in each dual beam detector.
Claim 7
Dependent Claim 27 words
Procedure according to claim 4, characterized in that the dispersed system to be measured is an emulsion selected from the group consisting of fat and protein emulsions.
Claim 8
Dependent Claim 28 words
Procedure according to claim 6, characterized in that the dispersed system contains a substance selected from the group consisting of carbohydrates, urea and other ketone substances, and antibiotics.
Claim 9
Dependent Claim 162 words
An IR spectrometer for analyzing the components of a dispersed system subject to turbulence affecting the spectrometric analysis comprising an IR light source (1) for forming a light beam; a single sample cuvette (5) which has been placed in the path of said beam; a diffraction member (6) for diffracting to a spectrum the light beam that has passed through the sample; a plurality of dual beam detectors (7) for detecting measuring absorbances at desired adjacent points in the spectrum and for detecting the reference absorbances at corresponding points of the spectrum, and a calculation means (9) for determining the content value of the sample corresponding to the measuring absorbances, on the basis of the ratio between the detected measuring and reference absorbances, characterized in that the dual beam detectors (7) have been arranged to detect the pairs of measuring absorbances and reference absorbances simultaneously from the light beam that has passed through the sample and has been diffracted to a spectrum.
Claim 10
Dependent Claim 162 words
An IR spectrometer for analyzing the components of a dispersed system subject to turbulence affecting the spectrometric analysis comprising an IR light source (1) for forming a light beam; a single sample cuvette (5) which has been placed in the path of said beam; a diffraction member (6) for diffracting to a spectrum the light beam that has passed through the sample; a plurality of dual beam detectors (7) for detecting measuring absorbances at desired adjacent points in the spectrum and for detecting the reference absorbances at corresponding points of the spectrum, and a calculation means (9) for determining the content value of the sample corresponding to the measuring absorbances, on the basis of the ratio between the detected measuring and reference absorbances, characterized in that the dual beam detectors (7) have been arranged to detect the pairs of measuring absorbances and reference absorbances simultaneously from the light beam that has passed through the sample and has been diffracted to a spectrum.
Claim 11
Dependent Claim 38 words
The IR spectrometer according to claim 8, characterized in that the diffraction member (6) has been placed substantially on a circular arc (10) and the detectors (6) have been placed substantially on an arc of the same circle.
Claim 12
Dependent Claim 37 words
The IR spectrometer according to claim 8, characterized in that the dual beam detectors (6) have been arranged to detect the measuring absorbance and the reference absorbance in two mutually adjacent wavelength intervals of the IR spectrum.
Claim 13
Dependent Claim 40 words
The IR spectrometer according to claim 10, characterized in that the detectors (6) have been arranged to detect the measuring absorbance at a peak in the IR spectrum and the reference absorbance, at a minimum immediately adjacent to said peak.
Claim 14
Dependent Claim 31 words
The IR spectrometer according to claim 11, characterized in that the light source (1), the diffraction member (6) and the detectors (7) are mounted substantially fixedly in relation to each other.
Claim 15
Dependent Claim 15 words
The IR spectrometer according to claim 12, characterized in that the detectors (6) are separate.
Claim 16
Dependent Claim 31 words
The IR spectrometer according to claim 10, characterized in that each dual beam detector (8 1 ) comprises means for forming the difference of the measuring absorbance and the reference absorbance.

References Cited (Backward Citations)

US3174037A Cited
US4030828A Cited
US4279511A Cited
JPS54159289A Cited
US4214835A Cited
US4557601A Cited
US4571074A Cited
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USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1994-05-20 1994-11-19 1995-05-21 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 1998-05-20 1998-11-19 1999-05-21 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 2002-05-20 2002-11-19 2003-05-21 $7700.00 Window Closed / Lapsed

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