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US5014541A Expired / Lapsed US ⏱️ 0.0 years remaining

Continuous air monitoring apparatus and method

Assignee: OI Corp
•
Filing: 1989-02-21
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Granted: 1991-05-14
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Expires: 2009-02-21
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Abstract

Abstract A continuous air monitoring apparatus utilizes a solid sorbent preconcentrator to concentrate airborne sorbent compounds for gas chromatographic analysis. Direct connection between the preconcentrator and gas chromatographic column allows direct desorption of the compounds into the column with minimal dead space. Temperature control on the column allows sharp chromatographic peaks to be attained without cryogenic focussing.

Inventors

  • 👤 Gary D. Sides
  • 👤 Marion Cates

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-11-09 06:13
CPC Classifications
G; G01; G01N; G01N30/00; G01N30/02; G01N30/04; G01N30/06; G01N30/08; G01N30/12; G01N2030/121; G01N2030/122; G01N30/26; G01N30/28; G01N30/30; G01N2030/3053; G01N2030/3061; G01N30/60; G01N30/6047

Claims Analysis

Total Claims: 4
Claim 1
Independent Claim 118 words
Apparatus for use in gas chromatography comprising: (a) a gas chromatographic column; (b) a solid sorbent preconcentrator tube in communication with said gas chromatographic column; (c) an inlet check valve connected to said solid sorbent preconcentrator tube to permit a sampling air stream therethrough in one direction and to prevent airflow in opposition to said sampling air stream; (d) a reservoir of carrier gas, connected to said solid sorbent preconcentrator tube intermediate said preconcentrator tube and said inlet check valve to selectively pass carrier gas therethrough; (e) means for selectively venting said carrier gas intermediate said preconcentrator tube and said gas chromatographic column; and (f) means for desorbing sampled material from said preconcentrator tube into said carrier gas.
Claim 2
Dependent Claim 118 words
Apparatus for use in gas chromatography comprising: (a) a gas chromatographic column; (b) a solid sorbent preconcentrator tube in communication with said gas chromatographic column; (c) an inlet check valve connected to said solid sorbent preconcentrator tube to permit a sampling air stream therethrough in one direction and to prevent airflow in opposition to said sampling air stream; (d) a reservoir of carrier gas, connected to said solid sorbent preconcentrator tube intermediate said preconcentrator tube and said inlet check valve to selectively pass carrier gas therethrough; (e) means for selectively venting said carrier gas intermediate said preconcentrator tube and said gas chromatographic column; and (f) means for desorbing sampled material from said preconcentrator tube into said carrier gas.
Claim 3
Dependent Claim 18 words
Apparatus as defined in claim 1 further comprises means for backflushing said gas chromatographic column with a gas.
Claim 4
Dependent Claim 30 words
Apparatus as defined in claim 1 wherein said means for desorbing includes means for controlling the temperature regime of said solid sorbent preconcentrator tube within predetermined temporal and thermal levels.

References Cited (Backward Citations)

US3357232A Cited
US4805441A Cited

USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1994-05-13 1994-11-12 1995-05-14 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 1998-05-13 1998-11-12 1999-05-14 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 2002-05-13 2002-11-12 2003-05-14 $7700.00 Window Closed / Lapsed

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