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US5002647A Expired / Lapsed US ⏱️ 0.0 years remaining

Process for preparation of thick films by electrophoresis

Assignee: Mitsubishi Materials Corp
•
Filing: 1989-07-20
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Granted: 1991-03-26
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Expires: 2009-07-20
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Abstract

Abstract In the process for preparing thick films comprising dispersing powder of a starting material for thick films in a solvent system, applying direct electric potential between the electrodes provided in the solvent system and thus electrodepositing the powder material on a substrate connected to the cathode, an improvement wherein a mixed solvent comprising an alcohol or alcohols, a methyl-group-containing ketone or ketones and nitorcellulose is disclosed. By this process thick films of solid electrolytes can be economically formed.

Inventors

  • 👤 Hiroyoshi Tanabe
  • 👤 Seitaro Fukushima
  • 👤 Etsuji Kimura

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-11-09 12:44
CPC Classifications
C; C25; C25D; C25D13/00; C25D13/02

Claims Analysis

Total Claims: 6
Claim 1
Independent Claim 76 words
A process for electrophoretically depositing films of zirconia solid electrolyte comprising: (a) dispersing Y 2 O 3 stabilized zirconia powder in a solvent system consisting essentially of 30-50% by volume of one or more alcohols, 50-70% by volume of one or more methyl group-containing ketones and 0.001-0.5% by volume of nitrocellulose; (b) applying direct electric potential between electrodes which are provided in the solvent system, thereby depositing the powder on a substrate connected to the cathode.
Claim 2
Dependent Claim 76 words
A process for electrophoretically depositing films of zirconia solid electrolyte comprising: (a) dispersing Y 2 O 3 stabilized zirconia powder in a solvent system consisting essentially of 30-50% by volume of one or more alcohols, 50-70% by volume of one or more methyl group-containing ketones and 0.001-0.5% by volume of nitrocellulose; (b) applying direct electric potential between electrodes which are provided in the solvent system, thereby depositing the powder on a substrate connected to the cathode.
Claim 3
Dependent Claim 14 words
The process of claim 1 wherein said alcohols are methyl alcohol and hexyl alcohol.
Claim 4
Dependent Claim 20 words
The process of claim 1 wherein said solvent system consists essentially of methyl alcohol, hexyl alcohol, methylisobutyl ketone and nitrocellulose.
Claim 5
Dependent Claim 13 words
The process of claim 3 wherein said cathode is an insulator oxide material.
Claim 6
Dependent Claim 23 words
The process of claim 1 wherein an electrophoretic deposition is repeated with a different solid electrolyte powder, thereby forming a laminated multilayer film.

References Cited (Backward Citations)

US3770604A Cited
US4482447A Cited

USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1994-03-25 1994-09-24 1995-03-26 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 1998-03-25 1998-09-24 1999-03-26 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 2002-03-25 2002-09-24 2003-03-26 $7700.00 Window Closed / Lapsed

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