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US4990609A Expired / Lapsed US ⏱️ 0.0 years remaining

Sulfoethyl cellulose of high solution quality and a process for its production

Assignee: Dow Produktions und Vertriebs GmbH and Co OHG
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Filing: 1988-12-09
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Granted: 1991-02-05
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Expires: 2008-12-09
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Abstract

Abstract Sulfoethyl cellulose prepared by addition of an alkylating agent and subsequent addition of alkali shows particularly valuable properties.

Inventors

  • 👤 Dieter Herzog
  • 👤 Klaus Balser
  • 👤 Klaus Szablikowski

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-11-05 07:30
CPC Classifications
C; C08; C08B; C08B11/00; C08B11/02; C08B11/04; C08B11/10; C08B11/193

Claims Analysis

Total Claims: 11
Claim 1
Independent Claim 47 words
In the preparation of a sulfoethyl cellulose by reacting cellulose with a sulfoethylating agent, the improvement which comprises effecting the reaction by (a) grinding the cellulose, (b) combining the ground cellulose with the sulfoethylating agent, (c) adding alkali and (d) raising the temperature to effect the reaction.
Claim 2
Dependent Claim 47 words
In the preparation of a sulfoethyl cellulose by reacting cellulose with a sulfoethylating agent, the improvement which comprises effecting the reaction by (a) grinding the cellulose, (b) combining the ground cellulose with the sulfoethylating agent, (c) adding alkali and (d) raising the temperature to effect the reaction.
Claim 3
Dependent Claim 21 words
The process according to claim 1, including the further step (e) of neutralizing, filtering and washing the product of step (d).
Claim 4
Dependent Claim 34 words
The process according to claim 1, wherein between steps (c) and (d) the combined materials of step (b) are permitted to stand for about 60 to 180 minutes from about 0° to 35° C.
Claim 5
Dependent Claim 15 words
The process according to claim 1, wherein the sulfoethylating agent is a vinyl sulfonic acid.
Claim 6
Dependent Claim 22 words
The process according to claim 1, wherein the steps (a), (b), and (c) (d) are carried out consecutively in the same vessel.
Claim 7
Dependent Claim 26 words
The process according to claim 1, wherein the cellulose is selected from the group consisting of linters, softwood sulfite cellulose, softwood sulfate cellulose and hardwood cellulose.
Claim 8
Dependent Claim 23 words
The process according to claim 1, wherein step (d) is continued for sufficient time to result in a DS-sulfoethyl of at least 0.4.
Claim 9
Dependent Claim 23 words
The process according to claim 1, wherein step (d) is continued for sufficient time to result in a DS-sulfoethyl of at least 0.5.
Claim 10
Dependent Claim 15 words
The process according to claim 1, wherein step (b) is effected in an alcohol slurry.
Claim 11
Dependent Claim 11 words
The process according to claim 9, wherein the alcohol is isopropanol.

References Cited (Backward Citations)

US2580352A Cited
US2811519A Cited
GB1072021A Cited
SU757540A1 Cited
US4650863A Cited

USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1994-02-04 1994-08-06 1995-02-05 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 1998-02-04 1998-08-06 1999-02-05 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 2002-02-04 2002-08-06 2003-02-05 $7700.00 Window Closed / Lapsed

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