US4988480A
Expired / Lapsed
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Method for making a composite
Assignee: Institute of Structural Macrokinetics and Materials Science
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Filing: 1988-12-20
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Granted: 1991-01-29
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Expires: 2008-12-20
Abstract
Abstract PCT No. PCT/FR88/00270 Sec. 371 Date Aug. 23, 1990 Sec. 102(e) Date Aug. 23, 1990 PCT Filed Dec. 20, 1988 PCT Pub. No. WO90/07014 PCT Pub. Date Jun. 28, 1990.The proposed invention is used for the manufacture from the obtained composite of cutting tools, hard alloy tooling, dies and other products. A method according to the invention involves preparing a mixture, compacting it, placing the mixture into a synthesis zone, igniting the mixture, with subsequent reaction of components of the mixture under combustion conditions. Then cure is carried out during a period ranging from about 0.1 seconds to about 0.5 hours, and the hot combustion products are compacted under pressure at an average pressure rise rate ranging from about 10 to about 2000 kgf/cm2.s, with subsequent cure of the compacted product under isobaric conditions to complete homogenization of the composite, with subsequent cooling thereof to obtain an end composite.
Inventors
- 👤 Alexandr G. Merzhanov
- 👤 Inna P. Borovinskaya
- 👤 Alexandr N. Pitjulin
- 👤 Viktor I. Ratnikov
- 👤 Konstantin L. Epishin
- 👤 Vadim L. Kvanin
Bibliographic Details
Application Number
—
Jurisdiction
US
Data Source
google_patents
Last Synchronized
2026-11-02 19:40
CPC Classifications
C; C04; C04B; C04B35/00; C04B35/622; C04B35/64; C04B35/65; C04B35/651; C04B35/645; C22; C22C; C22C1/00; C22C1/04; C22C1/05; C22C1/051; C22C1/053
Claims Analysis
Total Claims: 20
Claim 1
Independent Claim
197 words
A method for making a composite, comprising blending a mixture containing at least one metallic element of groups III-VI, VIII of the periodic table of the chemical elements and at least one compound of at least one of the elements of said groups taken individually or in combination, at least one nonmetallic element of groups III-VI of the periodic table of the chemical elements and at least one compound of at least one of the elements of said groups taken individually or in combination, and a binder component, compacting the mixture, placing the mixture into a synthesis zone, igniting the mixture with subsequent reaction of the components of the mixture under combustion conditions, and compacting the hot combustion products to obtain an end composite, characterized in that after ignition the mixture is cured till compaction of hot products during a period ranging from about 0.1 seconds to about 0.5 hours, and compacting the hot combustion products is carried out under pressure at an average rate of pressure rise ranging from about 10 to about 2000 kgf/cm 2 ·s, with subsequent cure of the compacted product under isobaric conditions to complete homogenization of the composite and subsequent cooling.
Claim 2
Independent Claim
197 words
A method for making a composite, comprising blending a mixture containing at least one metallic element of groups III-VI, VIII of the periodic table of the chemical elements and at least one compound of at least one of the elements of said groups taken individually or in combination, at least one nonmetallic element of groups III-VI of the periodic table of the chemical elements and at least one compound of at least one of the elements of said groups taken individually or in combination, and a binder component, compacting the mixture, placing the mixture into a synthesis zone, igniting the mixture with subsequent reaction of the components of the mixture under combustion conditions, and compacting the hot combustion products to obtain an end composite, characterized in that after ignition the mixture is cured till compaction of hot products during a period ranging from about 0.1 seconds to about 0.5 hours, and compacting the hot combustion products is carried out under pressure at an average rate of pressure rise ranging from about 10 to about 2000 kgf/cm 2 ·s, with subsequent cure of the compacted product under isobaric conditions to complete homogenization of the composite and subsequent cooling.
Claim 3
Dependent Claim
20 words
A method as claimed in claim 1, characterized in that the composite is heat treated after homogenization and before cooling.
Claim 4
Dependent Claim
17 words
A method as claimed in claim 1, characterized in that the composite is heat treated after cooling.
Claim 5
Independent Claim
31 words
A method as claimed in claims 2 or 3, characterized in that cooling of said composite is carried out at an average rate ranging from about 10 to about 5000 deg./h.
Claim 6
Dependent Claim
46 words
A method as claimed in claim 1, characterized in that at least at the moment of ignition of mixture and during the initial stage of cure before compaction of the combustion products a pressure ranging from about 10 to about 1000 kgf/cm 2 is built up.
Claim 7
Dependent Claim
25 words
A method as claimed in claim 5, characterized in that said pressure is maintained during the entire cure period before compaction of said combustion products.
Claim 8
Dependent Claim
35 words
A method as claimed in claim 1, characterized in that the mixture is heated using an external energy supply to a temperature ranging from about 100° to about 1200° C. before ignition of said mixture.
Claim 9
Dependent Claim
26 words
A method as claimed in claim 1, characterized in that the mixture is placed into a heat insulating porous envelope after the compaction of the mixture.
Claim 10
Dependent Claim
37 words
A method as claimed in claim 8, characterized in that the heat insulating envelope has an open porosity, the volume of the open porosity being about 60% and less of the volume of the heat insulating envelope.
Claim 11
Dependent Claim
34 words
A method as claimed in claim 1 or 9, characterized in that the synthesis zone is evacuated to a residual pressure of about 10 -1 mmHg and below before said ignition of said mixture.
Claim 12
Dependent Claim
28 words
A method as claimed in claim 1, characterized in that compaction of said mixture is carried out to a relative density ranging from about 20% to about 90%.
Claim 13
Dependent Claim
19 words
A method as claimed in claim 11, characterized in that the mixture is molded during compaction of the mixture.
Claim 14
Dependent Claim
43 words
A method as claimed in claim 1, characterized in that the cure before compaction of the hot combustion products, the compaction of the hot combustion products and the cure of the compacted product under isobaric conditions are carried out in an ultrasonic field.
Claim 15
Dependent Claim
23 words
A method as claimed in claim 1, characterized in that the ignition of the mixture is carried out by means of ultrasonic oscillations.
Claim 16
Dependent Claim
67 words
A method as claimed in claim 1, characterized in that a perforated layer of a heat resistant material is placed on the surface of the mixture in the synthesis zone and an ignition composition having a combustion rate which is at least equal to that of the mixture is placed on this layer, the ignition of the mixture being carried out by means of the ignition composition.
Claim 17
Dependent Claim
37 words
A method as claimed in claim 1, characterized in that gas removal passages are formed in the mixture before the ignition, the volume of the passages being about 60% and less of the volume of the mixture.
Claim 18
Dependent Claim
38 words
A method as claimed in claim 1, characterized in that the metallic element is in the form of wastes of a metal of groups III-VI, VIII of the periodic table of the chemical elements and/or an alloy thereof.
Claim 19
Dependent Claim
36 words
A method as claimed in claim 1, characterized in that the nonmetallic element is in the form of a production waste of a nonmetallic element of groups III-VI of the periodic table of the chemical elements.
Claim 20
Dependent Claim
25 words
A method as claimed in claim 1, characterized in that the binder component is in the form of a production waste of a binder component.
References Cited (Backward Citations)
USPTO Annuity & Maintenance Windows
| Annuity Stage | Window Opens | Payment Deadline | Surcharge Period Until | Estimated Fee | Status |
|---|---|---|---|---|---|
| 3.5 Years (Year 4) | 1994-01-28 | 1994-07-30 | 1995-01-29 | $2000.00 | Window Closed / Lapsed |
| 7.5 Years (Year 8) | 1998-01-28 | 1998-07-30 | 1999-01-29 | $3760.00 | Window Closed / Lapsed |
| 11.5 Years (Year 12) | 2002-01-28 | 2002-07-30 | 2003-01-29 | $7700.00 | Window Closed / Lapsed |