US4963177A
Expired / Lapsed
US
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Method for making a grating assisted optical waveguide device
Assignee: École Polytechnique
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Filing: 1989-06-15
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Granted: 1990-10-16
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Expires: 2009-06-15
Abstract
Abstract The present disclosure makes a grating assisted optical waveguide device. The method includes cleaning a substrate made of glass by means of cleaning agents; depositing a first layer made of metal onto a surface of the substrate by an evaporation process; forming a first mask by making openings in the first layer to expose first parts of the surface, the first mask being formed by a photolithographic process; immersing the substrate in a first bath of molten salt having a first preselected temperature to make a waveguide by increasing the refractive index of the glass in the first parts by an ion-exchange process; removing the first mask from the surface; immersing the substrate in a second bath of molten salt in order to bury the waveguide; depositing a second layer made of metal on the surface of the substrate by an evaporation process; forming a second mask by making openings in the second layer to expose second parts of the surface, the second mask being formed by a photolithographic process; immersing the substrate in a third bath of molten salt having a third preselected temperature to change the refractive index of the glass in the second parts by an ion-exchange process in order to form a grating, the refractive index obtained in this third immersing step being different from the refractive index obtained in the first immersing step, the third preselected temperature being lower than the first preselected temperature to avoid further diffusion of ions diffused in substrate in the first bath; and removing the second mask from the surface to obtain the grating assisted optical waveguide device.
Inventors
- 👤 Seyed-Iraj Najafi
- 👤 Kenneth O. Hill
- 👤 Francois Bilodeau
- 👤 Derwyn C. Johnson
Bibliographic Details
Application Number
—
Jurisdiction
US
Data Source
google_patents
Last Synchronized
2026-11-04 21:41
CPC Classifications
G; G02; G02B; G02B6/00; G02B6/24; G02B6/26; G02B6/28; G02B6/293; G02B6/29346; G02B6/2935; G02B6/29352; G02B6/29353; C; C03; C03C; C03C17/00; C03C17/34; C03C17/36; C03C17/40; C03C21/00; C03C21/001; G02B6/10; G02B6/12; G02B6/122; G02B6/124; G02B6/13; G02B6/134; G02B6/1345
Claims Analysis
Total Claims: 10
Claim 1
Independent Claim
408 words
A method for making a grating assisted optical waveguide device, comprising the steps of: (a) cleaning a substrate made of glass having exchangeable cations by means of cleaning agents; (b) depositing a first layer made of metal onto a selected surface of said substrate by an evaporation process; (c) forming a first mask by making openings in said first layer to expose first parts of said surface in a pattern for forming waveguides, said first mask being formed by a photolithographic process; (d) immersing said substrate in a first bath of molten salt having a first preselected temperature to form waveguides by increasing the refractive index of glass immediately below said first parts of said surface by an ion-exchange in which refractive index increasing cations enter the glass through said openings in the first mask and replace said exchangeable cations; (e) withdrawing said substrate from said first bath and then removing said first mask from said selected surface; (f) immersing said substrate in a second bath of molten salt having a second preselected temperature and being a source of ions which will provide the same refractive index as the overall refractive index of the substrate to bury the waveguides by diffusion of cations away from said selected surface of said substrate; (g) withdrawing said substrate from said second bath and then depositing a second layer made of metal on said surface of said substrate by an evaporation process; (h) forming a second mask by making openings in said second layer to expose second parts of said surface in a pattern for forming a grating, said second mask being formed by a photolithographic process; (i) immersing said substrate in a third bath a molten salt having a third preselected temperature to change the refractive index of said glass below said second parts of said surface by an ion-exchange in which grating effecting ions enter the glass through the openings in the second mask and replace both said exchangeable ions and said index increasing ions in said glass substrate, the refractive index obtained in said step (i) being different from the refractive index obtained in said step (d), said third preselected temperature being sufficiently lower than said first preselected temperature such that diffusion of said index increasing ions in the glass does not occur; and (j) withdrawing said substrate from said third bath and then removing said second mask from said surface to obtain said grating assisted optical waveguide device.
Claim 2
Independent Claim
408 words
A method for making a grating assisted optical waveguide device, comprising the steps of: (a) cleaning a substrate made of glass having exchangeable cations by means of cleaning agents; (b) depositing a first layer made of metal onto a selected surface of said substrate by an evaporation process; (c) forming a first mask by making openings in said first layer to expose first parts of said surface in a pattern for forming waveguides, said first mask being formed by a photolithographic process; (d) immersing said substrate in a first bath of molten salt having a first preselected temperature to form waveguides by increasing the refractive index of glass immediately below said first parts of said surface by an ion-exchange in which refractive index increasing cations enter the glass through said openings in the first mask and replace said exchangeable cations; (e) withdrawing said substrate from said first bath and then removing said first mask from said selected surface; (f) immersing said substrate in a second bath of molten salt having a second preselected temperature and being a source of ions which will provide the same refractive index as the overall refractive index of the substrate to bury the waveguides by diffusion of cations away from said selected surface of said substrate; (g) withdrawing said substrate from said second bath and then depositing a second layer made of metal on said surface of said substrate by an evaporation process; (h) forming a second mask by making openings in said second layer to expose second parts of said surface in a pattern for forming a grating, said second mask being formed by a photolithographic process; (i) immersing said substrate in a third bath a molten salt having a third preselected temperature to change the refractive index of said glass below said second parts of said surface by an ion-exchange in which grating effecting ions enter the glass through the openings in the second mask and replace both said exchangeable ions and said index increasing ions in said glass substrate, the refractive index obtained in said step (i) being different from the refractive index obtained in said step (d), said third preselected temperature being sufficiently lower than said first preselected temperature such that diffusion of said index increasing ions in the glass does not occur; and (j) withdrawing said substrate from said third bath and then removing said second mask from said surface to obtain said grating assisted optical waveguide device.
Claim 3
Dependent Claim
47 words
Method according to claim 1, wherein said first parts of said surface comprise two longitudinal sections, each section has two extremities adjacent to the edge of said surface, one section having two areas sufficiently adjacent to two areas of the other section for coupling of wave energy.
Claim 4
Dependent Claim
34 words
Method according to claim 2, wherein said second parts of said surface comprise portions of said first parts, said portions being situated on each section of said first parts between said two adjacent areas.
Claim 5
Dependent Claim
10 words
Method according to claim 1, wherein said metal is aluminum.
Claim 6
Dependent Claim
16 words
Method according to claim 1, wherein said cleaning agents consist of soap, trichloroethane, acetone and methanol.
Claim 7
Dependent Claim
24 words
Method according to claim 1, wherein said first bath of molten salt comprises potassium nitrate, and said third bath of molten comprises silver nitrate.
Claim 8
Dependent Claim
24 words
Method according to claim 1, wherein said first and second preselected temperature are approximately 400°, and said third preselected temperature is approximately 250° C.
Claim 9
Dependent Claim
32 words
Method according to claim 1, wherein said third bath includes a molten salt selected from the group consisting of AgNO 3 , AgNO 3 :TlNO 3 and NaNO 3 :TlNO 3 .
Claim 10
Dependent Claim
22 words
Method according to claim 1, 2 or 3, wherein said obtained grating assisted optical waveguide is a narrow-band wavelength tap and combiner.
References Cited (Backward Citations)
USPTO Annuity & Maintenance Windows
| Annuity Stage | Window Opens | Payment Deadline | Surcharge Period Until | Estimated Fee | Status |
|---|---|---|---|---|---|
| 3.5 Years (Year 4) | 1993-10-15 | 1994-04-16 | 1994-10-16 | $2000.00 | Window Closed / Lapsed |
| 7.5 Years (Year 8) | 1997-10-15 | 1998-04-16 | 1998-10-16 | $3760.00 | Window Closed / Lapsed |
| 11.5 Years (Year 12) | 2001-10-15 | 2002-04-16 | 2002-10-16 | $7700.00 | Window Closed / Lapsed |