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US4962010A Expired / Lapsed US ⏱️ 0.0 years remaining

Method for producing amino-formaldehyde microcapsules and photosensitive microcapsules produced thereby

Assignee: Eastman Kodak Co
•
Filing: 1989-06-22
•
Granted: 1990-10-09
•
Expires: 2009-06-22
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Abstract

Abstract A method for forming microcapsules by enwrapping an oily core material in a formaldehyde condensation product formed in situ wherein methylated polygalacturonic acid is used in combination with a sulfonated polystyrene as an emulsion stabilizer; the method is particularly useful in forming photosensitive microcapsules in that uniform small microcapsules size is obtained.

Inventors

  • 👤 E. Keith Colyer
  • 👤 Joseph G. O'Connor
  • 👤 W. A. Hammann, IV

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-10-27 12:20
CPC Classifications
G; G03; G03F; G03F7/00; G03F7/002; B; B01; B01J; B01J13/00; B01J13/02; B01J13/06; B01J13/14; B01J13/18; Y; Y10; Y10T; Y10T428/00; Y10T428/29; Y10T428/2982; Y10T428/2984; Y10T428/2985; Y10T428/2989

Claims Analysis

Total Claims: 16
Claim 1
Independent Claim 56 words
A process for forming microcapsules having discrete capsule walls comprising the steps of forming an emulsion of an oily core material in a continuous aqueous phase containing methylated polygalacturonic acid and sulfonated polystyrene and enwrapping particles of said oily core material in an amine-formaldehyde condensation product produced by in situ condensation of an amine and formaldehyde.
Claim 2
Dependent Claim 56 words
A process for forming microcapsules having discrete capsule walls comprising the steps of forming an emulsion of an oily core material in a continuous aqueous phase containing methylated polygalacturonic acid and sulfonated polystyrene and enwrapping particles of said oily core material in an amine-formaldehyde condensation product produced by in situ condensation of an amine and formaldehyde.
Claim 3
Dependent Claim 12 words
The process of claim 1 wherein said amine is urea or melamine.
Claim 4
Dependent Claim 11 words
The process of claim 2 wherein said polygalacturonic acid is pectin.
Claim 5
Dependent Claim 14 words
The process of claim 3 wherein said formaldehyde condensation product is a melamine-formaldehyde resin.
Claim 6
Dependent Claim 14 words
The process of claim 3 wherein said formaldehyde condensation product is a urea-formaldehyde resin.
Claim 7
Dependent Claim 17 words
The process of claim 3 wherein said pectin exhibits a methylation degree of about 40 to 70%.
Claim 8
Dependent Claim 18 words
The process of claim 1 wherein said sulfonated polystyrene is characterized by a sulfonation degree greater than 85%.
Claim 9
Dependent Claim 16 words
The process of claim 7 wherein the sulfonation degree of said polystyrene is greater than 95%.
Claim 10
Dependent Claim 17 words
The process of claim 4 wherein said pectin exhibits a methylation degree of about 40 to 70%.
Claim 11
Dependent Claim 16 words
The process of claim 7 wherein said sulfonated polystyrene exhibits a sulfonation degree greater than 85%.
Claim 12
Dependent Claim 16 words
The process of claim 8 wherein said sulfonated polystyrene has a molecular weight greater than 100,000.
Claim 13
Dependent Claim 16 words
The process of claim 11 wherein said sulfonated polystyrene has a molecular weight greater than 500,000.
Claim 14
Dependent Claim 16 words
The process of claim 12 wherein said sulfonated polystyrene has a sulfonation degree greater than 95%.
Claim 15
Dependent Claim 13 words
The process of claim 1 wherein said core material is a photopolymerizable composition.
Claim 16
Dependent Claim 14 words
The process of claim 14 wherein said photopolymerizable composition contains an ethylenically unsaturated compound.

References Cited (Backward Citations)

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USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1993-10-08 1994-04-09 1994-10-09 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 1997-10-08 1998-04-09 1998-10-09 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 2001-10-08 2002-04-09 2002-10-09 $7700.00 Window Closed / Lapsed

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