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US4895696A Expired / Lapsed US ⏱️ 0.0 years remaining

Steam turbine preservative and method of preserving steam turbine components

Assignee: Westinghouse Electric Corp
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Filing: 1987-11-23
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Granted: 1990-01-23
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Expires: 2007-11-23
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Abstract

Abstract A steam turbine preservative and method of preserving steam turbine components involves the application of an amine polymer as a non-aqueous layer to the surfaces of such components. An organic solvent is mixed with the amine polymer to adjust its application viscosity.

Inventors

  • 👤 James C. Bellows

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-11-02 21:39
CPC Classifications
F; F01; F01D; F01D5/00; F01D5/12; F01D5/28; G; G21; G21D; G21D1/00; G21D1/006; C; C08; C08G; C08G12/00; C09; C09D; C09D5/00; C09D5/008; C09D5/08; C23; C23F; C23F11/00; F01D5/288; Y; Y02; Y02E; Y02E30/00; Y02E30/30

Claims Analysis

Total Claims: 24
Claim 1
Independent Claim 38 words
A method of preserving steam turbine components, comprising the steps of: producing an amine polymer from substantially synthesized compounds; and applying said amine polymer product in selected amounts as a non-aqueous layer upon the surfaces of the components.
Claim 2
Independent Claim 38 words
A method of preserving steam turbine components, comprising the steps of: producing an amine polymer from substantially synthesized compounds; and applying said amine polymer product in selected amounts as a non-aqueous layer upon the surfaces of the components.
Claim 3
Dependent Claim 12 words
The method according to claim 1, wherein said compounds are substantially halide-free.
Claim 4
Dependent Claim 35 words
The method according to claim 1, further comprising the step of mixing said amine polymer product with an organic solvent to a selected viscosity which is effective for application upon the surfaces of the components.
Claim 5
Dependent Claim 16 words
The method according to claim 3, wherein said organic solvent is substantially free of halogenated compounds.
Claim 6
Independent Claim 58 words
A method of preserving steam turbine components, comprising the steps of: mixing an amine polymer with an effective amount of a preselected organic solvent to adjust the viscosity of said mixture for application thereof to the components; and applying said mixture to the components as an effective non-aqueous layer for decomposition thereof over a predetermined period of time.
Claim 7
Independent Claim 58 words
A method of preserving steam turbine components, comprising the steps of: mixing an amine polymer with an effective amount of a preselected organic solvent to adjust the viscosity of said mixture for application thereof to the components; and applying said mixture to the components as an effective non-aqueous layer for decomposition thereof over a predetermined period of time.
Claim 8
Dependent Claim 12 words
The method according to claim 5, wherein said preselected solvent comprises naptha.
Claim 9
Dependent Claim 21 words
The method according to claim 5, wherein said effective layer applied to the components comprises a thickness of approximately 1 mil.
Claim 10
Dependent Claim 16 words
The method according to claim 5, wherein said predetermined period of time comprises approximately six months.
Claim 11
Dependent Claim 27 words
The method according to claim 5, further comprising the step of applying said mixture to the components in an effective layer for self-healing of cracks and scratches.
Claim 12
Dependent Claim 14 words
The method according to claim 9, wherein said effective layer comprises approximately 3 mils.
Claim 13
Dependent Claim 160 words
In a nuclear-powered system for generating a supply of steam to produce usable power therefrom, wherein the system includes at least one subsystem having a plurality of components which are exposed to the steam generated by the system, a method of preserving the components comprising the steps of: providing a supply of 1, 2-dichloroethane; condensing said 1, 2-dichloroethane with an effective amount of ammonia to yield a condensation product consisting essentially of an amine polymer and a condensation by-product of hydrogen chloride; removing said hydrogen chloride by-product of said condensation process; mixing an effective amount of naphtha with said amine polymer condensation product to adjust its viscosity for application thereof to the components; and applying said mixture to the components; whereby said naphtha evaporates upon application to the components leaving said amine polymer upon the components whereupon, in the presence of the steam, said amine polymer decomposes to a plurality of compounds innocuous to the operation of the nuclear-powered system.
Claim 14
Dependent Claim 160 words
In a nuclear-powered system for generating a supply of steam to produce usable power therefrom, wherein the system includes at least one subsystem having a plurality of components which are exposed to the steam generated by the system, a method of preserving the components comprising the steps of: providing a supply of 1, 2-dichloroethane; condensing said 1, 2-dichloroethane with an effective amount of ammonia to yield a condensation product consisting essentially of an amine polymer and a condensation by-product of hydrogen chloride; removing said hydrogen chloride by-product of said condensation process; mixing an effective amount of naphtha with said amine polymer condensation product to adjust its viscosity for application thereof to the components; and applying said mixture to the components; whereby said naphtha evaporates upon application to the components leaving said amine polymer upon the components whereupon, in the presence of the steam, said amine polymer decomposes to a plurality of compounds innocuous to the operation of the nuclear-powered system.
Claim 15
Dependent Claim 13 words
The method according to claim 12, wherein said naphtha comprises a synthesized naphtha.
Claim 16
Dependent Claim 25 words
The method according to claim 12, wherein said effective amount of naptha comprises an amount approximately equivalent to the amount of amine polymer condensation product.
Claim 17
Dependent Claim 16 words
The method according to claim 12, wherein said 1, 2-dichloroethane comprises an essentially pure 1, 2-dichloroethane.
Claim 18
Dependent Claim 44 words
The method according to claim 14, further comprising the step of adding an effective amount of chloroethane to said condensation product to reduce the degree of chain formation and branching to form said amine polymer upon reaction between said 1, 2-dichloroethane and said ammonia.
Claim 19
Dependent Claim 155 words
In a nuclear-powered system for generating a supply of steam to produce usable power therefrom, wherein the system includes at least one subsystem having a plurality of components which are exposed to the steam generated by the system, a method of preserving the components comprising the steps of: producing an amine polymer through reductive amination of glyoxal with ethylene diamine, said glyoxal and said ethylene diamine being combined together in molar ratios within a predetermined range to facilitate chain formation and branching of the amine polymer; mixing an effective amount of synthesized naptha with said amine polymer product to adjust its viscosity for application thereof to the components; and applying said mixture to the components; whereby said naptha evaporates upon application to the components leaving said amine polymer upon the components whereupon, in the presence of the steam, said amine polymer decomposes to a plurality of compounds innocuous to the operation of the nuclear-powered system.
Claim 20
Dependent Claim 155 words
In a nuclear-powered system for generating a supply of steam to produce usable power therefrom, wherein the system includes at least one subsystem having a plurality of components which are exposed to the steam generated by the system, a method of preserving the components comprising the steps of: producing an amine polymer through reductive amination of glyoxal with ethylene diamine, said glyoxal and said ethylene diamine being combined together in molar ratios within a predetermined range to facilitate chain formation and branching of the amine polymer; mixing an effective amount of synthesized naptha with said amine polymer product to adjust its viscosity for application thereof to the components; and applying said mixture to the components; whereby said naptha evaporates upon application to the components leaving said amine polymer upon the components whereupon, in the presence of the steam, said amine polymer decomposes to a plurality of compounds innocuous to the operation of the nuclear-powered system.
Claim 21
Dependent Claim 18 words
The method according to claim 16, wherein said predetermined range of molar ratios comprises from 2.5:1 to 3.5:1.
Claim 22
Dependent Claim 26 words
The method according to claim 16, wherein said effective amount of synthesized naptha comprises an amount approximately equivalent to the amount of said amine polymer product.
Claim 23
Dependent Claim 39 words
The method according to claim 16, further comprising an effective amount of a monofunctional aldehyde to reduce the degree of chain formation and branching to form said amine polymer upon reductive amination of said glyoxal and said ethylene diamine.
Claim 24
Dependent Claim 12 words
The method according to claim 19, wherein said monofunctional aldehyde comprises acetaldehyde.

References Cited (Backward Citations)

US3965027A Cited
US4018702A Cited
US4071639A Cited
US4595723A Cited
US4596849A Cited

USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1993-01-22 1993-07-24 1994-01-23 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 1997-01-22 1997-07-24 1998-01-23 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 2001-01-22 2001-07-24 2002-01-23 $7700.00 Window Closed / Lapsed

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