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US4871580A Expired / Lapsed US ⏱️ 0.0 years remaining

Method of treating surfaces of substrates with the aid of a plasma

Assignee: EINDHOVEN UNIVERSITY OF TECHNOLOGY FACULTY OF PHYSICS
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Filing: 1988-06-13
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Granted: 1989-10-03
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Expires: 2008-06-13
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Abstract

Abstract A method of treating substrate surfaces with the aid of a plasma such as etching, deposition etc. In the practice of the method, the plasma flows from its place of generation to the treatment-chamber, and in which method the plasma-generator is flushed through with a flushing gas. Preferably, and firstly after the flushing gas has passed the cathodes, the reactant is fed to the plasma-generator. The invention includes the reactor necessary for carrying out the method.

Inventors

  • 👤 Daniel C. Schram
  • 👤 Gerardus M. W. Kroesen

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-11-06 18:07
CPC Classifications
H; H05; H05H; H05H1/00; H05H1/24; H05H1/26; H05H1/32; H05H1/42; C; C23; C23C; C23C16/00; C23C16/44; C23C16/50; C23C16/513

Claims Analysis

Total Claims: 20
Claim 1
Independent Claim 105 words
A method of treating the surfaces of substrates with the aid of a plasma, comprising the steps: (a) supporting a substrate in a plasma treatment chamber, (b) providing at least one plasma-generator connected by at least one plasma-inlet to the plasma treatment chamber, (c) introducing a reactant via at least one inlet into said plasma-generator, (d) generating a plasma in said plasma-generator, (e) maintaining in the treatment chamber a pressure lower than that in the said plasma-generator whereby a stream of plasma flows through the plasma-inlet from the said plasma-generator to the said plasma treatment chamber, and (f) flushing through the plasma-generator a flushing gas.
Claim 2
Independent Claim 105 words
A method of treating the surfaces of substrates with the aid of a plasma, comprising the steps: (a) supporting a substrate in a plasma treatment chamber, (b) providing at least one plasma-generator connected by at least one plasma-inlet to the plasma treatment chamber, (c) introducing a reactant via at least one inlet into said plasma-generator, (d) generating a plasma in said plasma-generator, (e) maintaining in the treatment chamber a pressure lower than that in the said plasma-generator whereby a stream of plasma flows through the plasma-inlet from the said plasma-generator to the said plasma treatment chamber, and (f) flushing through the plasma-generator a flushing gas.
Claim 3
Dependent Claim 30 words
A method as set forth in claim 1 wherein, during the treatment of the substrate, forming an extra discharge in the plasma treatment chamber using the substrate as an electrode.
Claim 4
Dependent Claim 39 words
A method as claimed in claim 1, wherein the plasma-generator contains cathode and anode electrodes, the reactant is gas-like or liquid, and the reactant is first fed upstream in the plasma-generator after the flushing gas has passed the cathode.
Claim 5
Dependent Claim 28 words
A method as claimed in claim 3, wherein the flushing gas is built-up of molecules which contain no fragments which would react with the material of the cathode.
Claim 6
Dependent Claim 34 words
A method as claimed in claim 1, wherein the flushing gas is flowed through the plasma-generator at a rate of at least 1 meter/second in order to retard or prevent back-diffusion of the reactant.
Claim 7
Dependent Claim 18 words
A method as claimed in claim 5 wherein the flushing gas flow rate is at least 10 meters/second.
Claim 8
Dependent Claim 25 words
A method as claimed in claim 3 wherein during the treatment, the temperature of the cathode is maintained below the melting temperature of the cathode.
Claim 9
Dependent Claim 36 words
A method as claimed in claim 1 wherein the reactant is a liquid and is injected into the plasma-generator through at least one aperture in its wall with a diameter of between 0.0001 and 0.5 mm.
Claim 10
Dependent Claim 20 words
A method as claimed in claim 8, wherein the wall aperture has a diameter of between 0.005 and 0.1 mm.
Claim 11
Dependent Claim 28 words
A method as claimed in claim 8, wherein the liquid pressure in front of the aperture is maintained at a pressure greater than the pressure in the plasma-generator.
Claim 12
Dependent Claim 41 words
A method as claimed in claim 1, wherein the reactant is in the form of solid matter, and at least one discharge is established in the plasma treatment chamber or in the plasma-generator and which converts reactant into a gas-like phase.
Claim 13
Dependent Claim 25 words
A method as claimed in claim 1, wherein the treatment chamber is pumped out at a rate which is adjustable between 0 and 100,000 liters/second.
Claim 14
Dependent Claim 17 words
A method as claimed in claim 12, wherein the pumping rate is between 50 and 1000 liters/second.
Claim 15
Dependent Claim 22 words
A method as claimed in claim 1, wherein the diameter of the stream of plasma flowing into the treatment chamber is controlled.
Claim 16
Dependent Claim 22 words
A method as claimed in claim 14, wherein the plasma stream diameter is controlled by passing the plasma stream through a skimmer.
Claim 17
Dependent Claim 21 words
A method as claimed in claim 14, wherein the plasma stream diameter is controlled by subjecting it to a magnetic field.
Claim 18
Dependent Claim 20 words
A method as claimed in claim 1, wherein the reactant introduced to the plasma-generator in the vicinity of the plasma-inlet.
Claim 19
Dependent Claim 21 words
A method as claimed in claim 1, wherein the substrate is maintained at a temperature of between 70° and 1500° Kelvin.
Claim 20
Dependent Claim 18 words
A method as claimed in claim 18, wherein the temperature is maintained at between 273° and 1000° Kelvin.

References Cited (Backward Citations)

No citation records indexed.

USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1992-10-02 1993-04-03 1993-10-03 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 1996-10-02 1997-04-03 1997-10-03 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 2000-10-02 2001-04-03 2001-10-03 $7700.00 Window Closed / Lapsed

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