US4871559A
Expired / Lapsed
US
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Methods for preservation of foodstuffs
Assignee: Maxwell Technologies Inc
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Filing: 1988-04-28
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Granted: 1989-10-03
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Expires: 2008-04-28
Abstract
Abstract Methods and apparatus for food product preservation by inactivation of microorganisms and/or enzymes by applying pulses of very intense, very short duration pulses of light in the visible and near visible frequencies to the surface of food products to be preserved. Also disclosed are packaging methods and apparatus utilizing such intense, short pulses of polychromatic, incoherent light.
Inventors
- 👤 Joseph E. Dunn
- 👤 R. Wayne Clark
- 👤 John F. Asmus
- 👤 Jay S. Pearlman
- 👤 Keith Boyer
- 👤 Fraincois Painchaud
- 👤 Gunter A. Hofmann
Bibliographic Details
Application Number
—
Jurisdiction
US
Data Source
google_patents
Last Synchronized
2026-11-09 04:05
CPC Classifications
A; A23; A23B; A23B2/00; A23B2/50; A23B2/05; A23B2/08; A23B2/53; A61; A61L; A61L2/00; A61L2/02; A61L2/08; A61L2/10; B; B65; B65B; B65B55/00; B65B55/02; B65B55/04; B65B55/08; B65B55/12; B65B55/16
Claims Analysis
Total Claims: 32
Claim 1
Independent Claim
423 words
A method for preserving a perishable foodstuff to provide a preserved food product having improved keeping qualities with respect to deterioration resulting from microbiological surface growth or enzymatic degradation, comprising the steps of providing a solid food product to be treated, illuminating the surface of said solid food product with a first very short pulse of intense polychromatic incoherent light having a duration in the range of from about 0.001 to about 100 milliseconds, an energy density in the range of from about 0.01 to about 50 joules per square centimeter at the surface of the food product, a wavelength distribution such that at least about 70 percent of the energy of said pulse of intense polychromatic incoherent light is distributed at wavelengths between 170 nanometers and 2600 nanometers, substantially instantaneously with the duration of said first polychromatic incoherent light pulse, heating a superficial surface layer of said surface of said food product through absorption of said short intense polychromatic incoherent light pulse to a temperature effective to inactivate enzymes and microorganisms at said superficial surface layer of said solid food product before substantial thermal conduction occurs from said superficial surface layer to the interior of said food product, permitting the heat deposited in said superficial surface layer by said first very short intense pulse to dissipate from said superficial surface layer for a heat dissipation time period in the range of from about 0.001 to about 30 seconds, and illuminating the surface of said solid food product with at least one subsequent very short pulse of intense polychromatic incoherent light having a duration in the range of from about 0.001 to about 100 milliseconds, an energy density in the range of from about 0.01 to about 20 joules per square centimeter at the surface of the food product, a wavelength distribution such at least about 70 percent of the energy of said at least one subsequent pulse of intense polychromatic incoherent light is distributed at wavelengths between 170 nanometers and 2600 nanometers, substantially instantaneously with the duration of said at least one subsequent short intense polychromatic incoherent light pulse heating a superficial surface layer of said surface of said food product through absorption of said at least one subsequent short intense polychromatic incoherent light pulse to a temperature effective to inactivate enzymes or microorganisms at said superficial surface layer of said solid food product before substantial thermal conduction occurs from said superficial surface layer to the interior of said food product to provide a surface sterilized food product having improved keeping qualities.
Claim 2
Independent Claim
423 words
A method for preserving a perishable foodstuff to provide a preserved food product having improved keeping qualities with respect to deterioration resulting from microbiological surface growth or enzymatic degradation, comprising the steps of providing a solid food product to be treated, illuminating the surface of said solid food product with a first very short pulse of intense polychromatic incoherent light having a duration in the range of from about 0.001 to about 100 milliseconds, an energy density in the range of from about 0.01 to about 50 joules per square centimeter at the surface of the food product, a wavelength distribution such that at least about 70 percent of the energy of said pulse of intense polychromatic incoherent light is distributed at wavelengths between 170 nanometers and 2600 nanometers, substantially instantaneously with the duration of said first polychromatic incoherent light pulse, heating a superficial surface layer of said surface of said food product through absorption of said short intense polychromatic incoherent light pulse to a temperature effective to inactivate enzymes and microorganisms at said superficial surface layer of said solid food product before substantial thermal conduction occurs from said superficial surface layer to the interior of said food product, permitting the heat deposited in said superficial surface layer by said first very short intense pulse to dissipate from said superficial surface layer for a heat dissipation time period in the range of from about 0.001 to about 30 seconds, and illuminating the surface of said solid food product with at least one subsequent very short pulse of intense polychromatic incoherent light having a duration in the range of from about 0.001 to about 100 milliseconds, an energy density in the range of from about 0.01 to about 20 joules per square centimeter at the surface of the food product, a wavelength distribution such at least about 70 percent of the energy of said at least one subsequent pulse of intense polychromatic incoherent light is distributed at wavelengths between 170 nanometers and 2600 nanometers, substantially instantaneously with the duration of said at least one subsequent short intense polychromatic incoherent light pulse heating a superficial surface layer of said surface of said food product through absorption of said at least one subsequent short intense polychromatic incoherent light pulse to a temperature effective to inactivate enzymes or microorganisms at said superficial surface layer of said solid food product before substantial thermal conduction occurs from said superficial surface layer to the interior of said food product to provide a surface sterilized food product having improved keeping qualities.
Claim 3
Dependent Claim
100 words
A method in accordance with claim 1 wherein said pulses have a duration in the range of from about 0.001 to about 5 milliseconds, an energy density in the range of from about 0.5 to about 20 joules per square centimeter at the surface of the food product, and a wavelength distribution such that at least about 60 percent of the pulse energy is distributed at wavelengths between 300 nanometers and 2500 nanometers, and wherein a superficial surface layer of said food product is heated by at least one of said pulses to a temperature of at least 100° C.
Claim 4
Dependent Claim
111 words
A method in accordance with claim 1 wherein said energy density is in the range of from about 2 to about 20 joules per aquare centimeter, wherein said pulse duration is from about 0.01 to about 1 milliseconds and wherein said first short pulse and at least one of said subsequent pulses of polychromatic incoherent light have an energy wavelength distribution such that at least about 10 percent of their respective energy is distributed at wavelengths between 300 and 400 nanometers, and wherein said first and said subsequent pulses provide a reduction of at least a factor of 10 in the population of microorganisms at said surface of said food product.
Claim 5
Dependent Claim
31 words
A method in accordance with claim 1 wherein said food product is selected from the group consisting of solid dairy products, beef, pork, poultry, vegetables, fruits, fresh fish, and bakery goods.
Claim 6
Dependent Claim
39 words
A method according to claim 1 wherein said surface of said food product is exposed to between about 5 and about 20 of said pulses each separated by a heat dissipation time period of less than about 10 seconds.
Claim 7
Dependent Claim
41 words
A method according to claim 1, further including the step of sealing said solid food product in a transparent package prior to illuminating said surface of said solid food product through said transparent package with said first and subsequent light pulses.
Claim 8
Dependent Claim
39 words
A method according to claim 1, wherein the number of said first and subsequent light pulses is limited so as to maintain the surface temperature of said food product, ten seconds after pulsed light exposure, below about 100° C.
Claim 9
Dependent Claim
25 words
A method in accordance with claim 1 wherein said food product is contacted with an absorption enhancing agent prior to application of said light pulses.
Claim 10
Dependent Claim
26 words
A method in accordance with claim 8 wherein said light pulses each have a duration in the range of from about 0.5 to about 3 milliseconds.
Claim 11
Independent Claim
145 words
A method for inactivating microorganisms on the surface of a packaging material or foodstuff comprising the steps of providing a packaging material of foodstuff surface to be sterilized, applying an absorption enhancing agent to said surface in sufficient amount such that at least about 10% of the incident light is absorbed within a 10 micron thick superficial layer of said surface, and illuminating said surface having said absorption enhancing agent applied thereto with at least one pulse of high intensity incoherent polychromatic light having a duration in the range of from about 0.001 to about 100 milliseconds, an energy distribution such that at least about 70% of the energy of said pulse is distributed in the wavelength range of from about 170 nanometers to about 2600 nanometers and an energy density of from about 0.01 to about 50 joules per square centimeter of said surface.
Claim 12
Independent Claim
145 words
A method for inactivating microorganisms on the surface of a packaging material or foodstuff comprising the steps of providing a packaging material of foodstuff surface to be sterilized, applying an absorption enhancing agent to said surface in sufficient amount such that at least about 10% of the incident light is absorbed within a 10 micron thick superficial layer of said surface, and illuminating said surface having said absorption enhancing agent applied thereto with at least one pulse of high intensity incoherent polychromatic light having a duration in the range of from about 0.001 to about 100 milliseconds, an energy distribution such that at least about 70% of the energy of said pulse is distributed in the wavelength range of from about 170 nanometers to about 2600 nanometers and an energy density of from about 0.01 to about 50 joules per square centimeter of said surface.
Claim 13
Dependent Claim
17 words
A method in accordance with claim 10 wherein said absorption enhancing agent is a natural food coloring.
Claim 14
Dependent Claim
100 words
A method in accordance with claim 10 wherein said absorption enhancing agent is an edible dye, and wherein said surface is illuminated with a plurality of at least 2 of said pulses, wherein the duration of said pulses is in the range of from about 0.01 to about 100 milliseconds, wherein said energy density of each of said pulses is at least about 1 joule per square centimeter of said surface and wherein at least about 70% of the energy of each of said pulses is distributed within the wavelength range of from about 170 nanometers to about 2600 nanometers.
Claim 15
Independent Claim
98 words
A method for preserving food products, comprising the steps of applying to the entire surface of the food product a plurality of intense incoherent light pulses having a duration from about 1×10 -6 to 1×10 -1 second, an energy density in the range of from about 0.01 to 50 joules per square centimeters and a broadband wavelength distribution such that at least 70% of the light is in the wavelength range of from 170 nanometers to 2600 nanometers to inactive enzymes and bacteria and molds at the surface and within the near surface region of the food product.
Claim 16
Independent Claim
98 words
A method for preserving food products, comprising the steps of applying to the entire surface of the food product a plurality of intense incoherent light pulses having a duration from about 1×10 -6 to 1×10 -1 second, an energy density in the range of from about 0.01 to 50 joules per square centimeters and a broadband wavelength distribution such that at least 70% of the light is in the wavelength range of from 170 nanometers to 2600 nanometers to inactive enzymes and bacteria and molds at the surface and within the near surface region of the food product.
Claim 17
Independent Claim
92 words
A method of inactivating microorganisms on a surface of a food product or packaging material comprising exposing the food product or packaging material surface to between about 1 and about 50 pulses of light spaced not more than about 10 seconds apart, the light having most of its energy distributed in the wavelength between 300 and 2500 nanometers, each pulse having a duration of between about 0.1 and about 1.0 millisecond, each pulse providing an energy density at the surface of between about 2 and about 20 joules per cm 2 .
Claim 18
Independent Claim
92 words
A method of inactivating microorganisms on a surface of a food product or packaging material comprising exposing the food product or packaging material surface to between about 1 and about 50 pulses of light spaced not more than about 10 seconds apart, the light having most of its energy distributed in the wavelength between 300 and 2500 nanometers, each pulse having a duration of between about 0.1 and about 1.0 millisecond, each pulse providing an energy density at the surface of between about 2 and about 20 joules per cm 2 .
Claim 19
Dependent Claim
21 words
A method according to claim 14 wherein the surface is exposed to between about 5 and about 20 of said pulses.
Claim 20
Dependent Claim
19 words
A method according to claim 14 wherein said pulses are spaced between about 0.1 and about 10 seconds apart.
Claim 21
Dependent Claim
13 words
A method according to claim 14 wherein said light is incoherent and polychromatic.
Claim 22
Dependent Claim
14 words
A method according to claim 14 wherein said light is generated by a flashlamp.
Claim 23
Dependent Claim
24 words
A method according to claim 14, including sealing said food product in a transparent package prior to exposing its surfaces to said light pulses.
Claim 24
Dependent Claim
38 words
A method according to claim 14 limiting the number of said light pulses so as to maintain the measurable surface temperature of the food product or packaging material, ten seconds after pulsed light exposure, below about 130° C.
Claim 25
Dependent Claim
13 words
A method according to claim 14 wherein said material is a food product.
Claim 26
Dependent Claim
14 words
A method according to claim 14 wherein said material is a food packaging material.
Claim 27
Independent Claim
195 words
A method for preserving a perishable foodstuff having surface enzyme activity resulting from the presence of a plurality of active enzymes, to provide a preserved food product having improved keeping qualitites, comprising the steps of providing a solid food product to be treated having degradative enzymes at the food product surface, illuminating the surface of said solid food product with at least one very short pulse of intense polychromatic incoherent light having a duration in the range of from about 0.001 to about 100 milliseconds, an energy density in the range of from about 0.01 to about 50 joules per square centimeter at the surface of the food product, a wavelength distribution such that at least about 70 percent of the energy of said pulse of intense polychromatic incoherent light is distributed at wavelengths between 170 nanometers and 2600 nanometers, substantially instantaneously with the duration of said first polychromatic incoherent light pulse, to substantially simultaneously reduce the activity of each of a plurality of at least two different specific enzymes to less than 75 percent of their respective initial values at the food product surface, to provide a preserved food product having increased shelf life.
Claim 28
Independent Claim
195 words
A method for preserving a perishable foodstuff having surface enzyme activity resulting from the presence of a plurality of active enzymes, to provide a preserved food product having improved keeping qualitites, comprising the steps of providing a solid food product to be treated having degradative enzymes at the food product surface, illuminating the surface of said solid food product with at least one very short pulse of intense polychromatic incoherent light having a duration in the range of from about 0.001 to about 100 milliseconds, an energy density in the range of from about 0.01 to about 50 joules per square centimeter at the surface of the food product, a wavelength distribution such that at least about 70 percent of the energy of said pulse of intense polychromatic incoherent light is distributed at wavelengths between 170 nanometers and 2600 nanometers, substantially instantaneously with the duration of said first polychromatic incoherent light pulse, to substantially simultaneously reduce the activity of each of a plurality of at least two different specific enzymes to less than 75 percent of their respective initial values at the food product surface, to provide a preserved food product having increased shelf life.
Claim 29
Dependent Claim
32 words
A method in accordance with claim 23 wherein the activity of each of said plurality of enzymes is reduced to less than 10 percent of the initial activity of said respective enzyme.
Claim 30
Dependent Claim
19 words
A method in accordance with claim 23 wherein said food product is a fruit, fish, shellfish, vegetable or meat.
Claim 31
Dependent Claim
17 words
A method in accordance with claim 25 wherein said food product has a cut or bruised surface.
Claim 32
Dependent Claim
45 words
A method in accordance with claim 23 wherein said food product has microbial colony forming units on the food product surface, and wherein the number of colony forming units initially present at the food product surface is reduced by a factor of at least 10.
References Cited (Backward Citations)
US2072416A
Cited
US2072417A
Cited
US2482507A
Cited
US2930706A
Cited
GB1052513A
Cited
US3817703A
Cited
GB1346521A
Cited
US3814680A
Cited
US3955921A
Cited
GB1448411A
Cited
GB1548997A
Cited
US4042325A
Cited
GB1581998A
Cited
US4265747A
Cited
US4391080A
Cited
US4464336A
Cited
US4424188A
Cited
USPTO Annuity & Maintenance Windows
| Annuity Stage | Window Opens | Payment Deadline | Surcharge Period Until | Estimated Fee | Status |
|---|---|---|---|---|---|
| 3.5 Years (Year 4) | 1992-10-02 | 1993-04-03 | 1993-10-03 | $2000.00 | Window Closed / Lapsed |
| 7.5 Years (Year 8) | 1996-10-02 | 1997-04-03 | 1997-10-03 | $3760.00 | Window Closed / Lapsed |
| 11.5 Years (Year 12) | 2000-10-02 | 2001-04-03 | 2001-10-03 | $7700.00 | Window Closed / Lapsed |