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US4867562A Expired / Lapsed US ⏱️ 0.0 years remaining

Atomic absorption spectrophotometer

Assignee: Hitachi Ltd
•
Filing: 1988-05-20
•
Granted: 1989-09-19
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Expires: 2008-05-20
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Abstract

Abstract An atomic absorption spectrophotometer for simultaneously measuring a plurality of elements different in kind from each other. A cylindrical heating furnace is provided for heating a sample being analyzed to dry, ash and atomize the sample thereby producing atomic vapor. A plurality of hollow-cathode discharge tubes corresponding in number to the elements being detected are arranged for simultaneously emitting light beams respectively containing line spectra of the respective elements, to cause the light beams to be incident upon the heating furnace at respective angles of inclination with respect to a central axis of the heating furnace. A plurality of spectral detection systems are arranged behind the heating furnace in relation to the angles of inclination, for respectively spectral-diffracting and receiving the light beams having their respective line spectra absorbed by the atomic vapor. A signal processing device is provided for carrying out calculation to obtain concentrations or quantities of the respective elements in the sample being analyzed, on the basis of respective ratios of atomic resonance absorption of the respective line spectra spectral-detected.

Inventors

  • 👤 Konosuke Oishi
  • 👤 Masamichi Tsukada
  • 👤 Masatoshi Kitagawa
  • 👤 Toyoharu Okumoto
  • 👤 Hayato Tobe

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-10-26 08:35
CPC Classifications
G; G01; G01N; G01N21/00; G01N21/17; G01N21/25; G01N21/31; G01N21/3103; G01N2021/3111; G01N2021/3114; G01N21/62; G01N21/71; G01N21/74; G01N2201/00; G01N2201/06; G01N2201/061; G01N2201/06166

Claims Analysis

Total Claims: 8
Claim 1
Independent Claim 172 words
An atomic absorption spectrophotometer for simultaneously measuring a plurality of elements different in kind from each other, said atomic absorption spectrophotometer comprising: a cylindrical heating furnace for heating a sample being analyzed to dry, ash and atomize the sample thereby producing atomic vapor; a plurality of hollow-cathode discharge tubes corresponding in number to the elements being detected, for simultaneously emitting light beams respectively containing line spectra of the respective elements, to cause the light beams to be incident upon said heating furnace at respective angles of inclination with respect to a central axis of said heating furnace; a plurality of spectral detection systems arranged behind said heating furnace in relation corresponding to said angles of inclination, for respectively spectral-diffracting and receiving said light beams having their respective line spectra absorbed by said atomic vapor; and signal processing means for carrying out calculation to obtain concentrations or quantities of the respective elements in the sample being analyzed, on the basis of respective ratios of atomic resonance absorption of the respective line spectra spectral-detected.
Claim 2
Dependent Claim 172 words
An atomic absorption spectrophotometer for simultaneously measuring a plurality of elements different in kind from each other, said atomic absorption spectrophotometer comprising: a cylindrical heating furnace for heating a sample being analyzed to dry, ash and atomize the sample thereby producing atomic vapor; a plurality of hollow-cathode discharge tubes corresponding in number to the elements being detected, for simultaneously emitting light beams respectively containing line spectra of the respective elements, to cause the light beams to be incident upon said heating furnace at respective angles of inclination with respect to a central axis of said heating furnace; a plurality of spectral detection systems arranged behind said heating furnace in relation corresponding to said angles of inclination, for respectively spectral-diffracting and receiving said light beams having their respective line spectra absorbed by said atomic vapor; and signal processing means for carrying out calculation to obtain concentrations or quantities of the respective elements in the sample being analyzed, on the basis of respective ratios of atomic resonance absorption of the respective line spectra spectral-detected.
Claim 3
Dependent Claim 67 words
An atomic absorption spectrophotometer as defined in claim 1, wherein said signal processing means includes means for correcting errors caused due to the fact that the light beams incident upon said cylindrical heating furnace from the respective hollow-cathode discharge tubes are bent in their respective advancing directions by a rise in temperature of said heating furnace, and are not correctly incident upon the respective spectral detection systems.
Claim 4
Dependent Claim 32 words
An atomic absorption spectrophotometer as defined in claim 1 or claim 2, wherein said angles of inclination of the respective light beams are symmetrical about the central axis of said heating furnace.
Claim 5
Dependent Claim 224 words
An atomic absorption spectrophotometer for simultaneously measuring a plurality of elements different in kind from each other, said atomic absorption spectrophotometer comprising: a cylindrical heating furnace for heating a sample being analyzed to dry, ash and atomize the sample thereby producing atomic vapor; a plurality of hollow-cathode discharge tubes corresponding in number to the elements being detected, for simultaneously emitting light beams respectively containing line spectra of the respective elements; an optical system for turning back the light beams from the respective hollow-cathode discharge tubes to concentrate the light beams around the central axis of said heating furnace, to cause the light beams to be incident upon said heating furnace at respective angles of inclination with respect to the central axis of said heating furnace; an optical system arranged behind said heating furnace in relation corresponding to said angles of inclination, for turning back the light beams having their respective line spectra absorbed by said atomic vapor, thereby moving the light beams away from the central axis of said heating furnace; a plurality of spectral detection systems for respectively spectral-diffracting and receiving the transmitted light beams; and signal processing means for carrying out calculation to obtain concentrations or quantities of the respective elements in the sample being analyzed, on the basis of respective ratios of atomic resonance absorption of the respective line spectra spectral-detected.
Claim 6
Dependent Claim 224 words
An atomic absorption spectrophotometer for simultaneously measuring a plurality of elements different in kind from each other, said atomic absorption spectrophotometer comprising: a cylindrical heating furnace for heating a sample being analyzed to dry, ash and atomize the sample thereby producing atomic vapor; a plurality of hollow-cathode discharge tubes corresponding in number to the elements being detected, for simultaneously emitting light beams respectively containing line spectra of the respective elements; an optical system for turning back the light beams from the respective hollow-cathode discharge tubes to concentrate the light beams around the central axis of said heating furnace, to cause the light beams to be incident upon said heating furnace at respective angles of inclination with respect to the central axis of said heating furnace; an optical system arranged behind said heating furnace in relation corresponding to said angles of inclination, for turning back the light beams having their respective line spectra absorbed by said atomic vapor, thereby moving the light beams away from the central axis of said heating furnace; a plurality of spectral detection systems for respectively spectral-diffracting and receiving the transmitted light beams; and signal processing means for carrying out calculation to obtain concentrations or quantities of the respective elements in the sample being analyzed, on the basis of respective ratios of atomic resonance absorption of the respective line spectra spectral-detected.
Claim 7
Dependent Claim 67 words
An atomic absorption spectrophotometer as defined in claim 4, wherein said signal processing means includes means for correcting errors caused due to the fact that the light beams incident upon said cylindrical heating furnace from the respective hollow-cathode discharge tubes are bent in their respective advancing directions by a rise in temperature of said heating furnace, and are not correctly incident upon the respective spectral detection systems.
Claim 8
Dependent Claim 32 words
An atomic absorption spectrophotometer as defined in claim 4 or claim 5, wherein said angles of inclination of the respective light beams are symmetrical about the central axis of said heating furnace.

References Cited (Backward Citations)

US3552657A Cited
US3544789A Cited
JPS526586A Cited
JPS526587A Cited
DE2950105A1 Cited
JPH05262493A Cited

USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1992-09-18 1993-03-20 1993-09-19 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 1996-09-18 1997-03-20 1997-09-19 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 2000-09-18 2001-03-20 2001-09-19 $7700.00 Window Closed / Lapsed

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