US4865811A
Expired / Lapsed
US
⏱️ 0.0 years remaining
Apparatus for automatic chemical analysis
Assignee: BIOTECH INSTRUMENTS Ltd A CORP OF ENGLAND
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Filing: 1987-06-26
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Granted: 1989-09-12
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Expires: 2007-06-26
Abstract
Abstract A sample duct in a carrier line is isolated by three-way valves blocking the flow of carrier or flushing liquid from reservoirs. The sample duct may be connected to a loading syringe and to a sample reservoir respectively by the valves. When the sample duct is connected into the carrier line, pressurized carrier fluid may convey the sample for analysis through a manifold comprising valves through which reagents may be introduced from reservoirs. The sample then passes through a thermostatically controlled reaction tube to a valve which switches it between waste and an outlet leading to a detector for analysis. The carrier and flushing fluids and the reagents are pressurized by gas from an inlet which is conveyed via an overpressure vent to the reservoir by lines. Rigid inert tubing is used throughout the carrier line, sample duct, manifold and reaction tube.
Inventors
- 👤 Raymond Newton
- 👤 David Malcolm-Lawes
Bibliographic Details
Application Number
—
Jurisdiction
US
Data Source
google_patents
Last Synchronized
2026-11-02 01:07
CPC Classifications
G; G01; G01N; G01N35/00; G01N35/08; G01N35/085; Y; Y10; Y10T; Y10T436/00; Y10T436/11; Y10T436/117497; Y10T436/118339
Claims Analysis
Total Claims: 11
Claim 1
Independent Claim
133 words
Apparatus for flow injection analysis, comprising: a sample duct of predetermined volume; a reaction tube; a carrier line connecting the sample duct and the reagent tube, whereby a sample to be analysed can be conveyed by pressurized carrier fluid with added reagent from the sample duct to the reagent tube; isolating valves upstream and downstream of the sample duct operable to stop the flow of carrier fluid and to isolate the sample duct from the carrier line; sample loading means comprising a solenoid operable syringe connected to the upstream isolating valve to suck a sample into the sample duct via the downstream isolating valve; and a waste valve positioned between the sample duct and the upstream valve, said waste valve enabling sample surplus to the said predetermined volume to be passed to waste.
Claim 2
Dependent Claim
133 words
Apparatus for flow injection analysis, comprising: a sample duct of predetermined volume; a reaction tube; a carrier line connecting the sample duct and the reagent tube, whereby a sample to be analysed can be conveyed by pressurized carrier fluid with added reagent from the sample duct to the reagent tube; isolating valves upstream and downstream of the sample duct operable to stop the flow of carrier fluid and to isolate the sample duct from the carrier line; sample loading means comprising a solenoid operable syringe connected to the upstream isolating valve to suck a sample into the sample duct via the downstream isolating valve; and a waste valve positioned between the sample duct and the upstream valve, said waste valve enabling sample surplus to the said predetermined volume to be passed to waste.
Claim 3
Dependent Claim
29 words
Apparatus according to claim 1 in which said isolating valves comprise three-way valves, one being located on the upstream and one on the downstream side of the sample duct.
Claim 4
Dependent Claim
40 words
Apparatus according to claim 1 further including at least one valve on the upstream side of the upstream isolating valve to provide for the carrier line to be connected to any one of a plurality of carrier and/or flushing fluids.
Claim 5
Dependent Claim
50 words
Apparatus according to claim 1 including a three-way valve on the downstream side of the downstream isolating valve, said three-way valve used for priming, allowing for intake of a small amount of sample and its ejection to waste before loading the sample duct with a predetermined volume to be analysed.
Claim 6
Dependent Claim
36 words
Apparatus according to claim 1 and further including a reagent manifold having a series of three-way valves, each including means for connection with an individual reagent reservoir to enable reagent to be added to the sample.
Claim 7
Dependent Claim
36 words
Apparatus according to claim 1 further including a by-pass line connected between the carrier line and the reaction tube, to enable a reaction mixture to be passed on to a detector while sample loading takes place.
Claim 8
Dependent Claim
15 words
Apparatus according to claim 1 in which said reaction tube includes a thermostatic control means.
Claim 9
Dependent Claim
31 words
Apparatus according to claim 7 in which said reaction tube includes at its downstream end a three-way valve which is connected to waste and to an outlet leading to a detector.
Claim 10
Dependent Claim
19 words
Apparatus according to claim 1 including means for driving the carrier fluid and the reagent by positive pressure displacement.
Claim 11
Dependent Claim
20 words
Apparatus according to claim 9 in which said means for driving comprises a common gas inlet and an overpressure vent.
References Cited (Backward Citations)
US4177677A
Cited
US4224033A
Cited
US4207074A
Cited
US4272483A
Cited
US4283262A
Cited
US4362699A
Cited
US4411157A
Cited
US4713974A
Cited
JPH10175A
Cited
USPTO Annuity & Maintenance Windows
| Annuity Stage | Window Opens | Payment Deadline | Surcharge Period Until | Estimated Fee | Status |
|---|---|---|---|---|---|
| 3.5 Years (Year 4) | 1992-09-11 | 1993-03-13 | 1993-09-12 | $2000.00 | Window Closed / Lapsed |
| 7.5 Years (Year 8) | 1996-09-11 | 1997-03-13 | 1997-09-12 | $3760.00 | Window Closed / Lapsed |
| 11.5 Years (Year 12) | 2000-09-11 | 2001-03-13 | 2001-09-12 | $7700.00 | Window Closed / Lapsed |