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US4861575A Expired / Lapsed US ⏱️ 0.0 years remaining

Method of producing carbon fibers by overwrappings tows

Assignee: BP Corp North America Inc
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Filing: 1986-05-08
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Granted: 1989-08-29
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Expires: 2006-05-08
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Abstract

Abstract Carbon fibers may be made by a process comprising: overwrapping a multifilament polyacrylonitrile tow with a thread of material to maintain the tow as an integral bundle, followed by stabilizing said tow by heating in an oxidizing atmosphere at a temperature between about 180° and about 400° C., thereby oxidizing the filaments comprising said tow, followed by carbonizing the tow thus stabilized by heating at a temperature sufficient to effect carbonization, thereby forming a carbon fiber. The carbon fibers may be used to make reinforced composites in thermoplastic or thermosetting matrix resins, particularly prepreg.

Inventors

  • 👤 Chris D. Levan

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-11-07 07:07
CPC Classifications
D; D01; D01F; D01F9/00; D01F9/08; D01F9/12; D01F9/14; D01F9/20; D01F9/21; D01F9/22

Claims Analysis

Total Claims: 7
Claim 1
Independent Claim 51 words
A method of making carbon fibers, comprising the steps of: (a) overwrapping a multifilament polyacrylonitrile tow with a 10 to 150 denier thread; (b) stabilizing said tow by heating in an oxidizing atmosphere at a temperature between about 180° and about 400° C.; and (c) carbonizing the stabilized tow by heating.
Claim 2
Independent Claim 51 words
A method of making carbon fibers, comprising the steps of: (a) overwrapping a multifilament polyacrylonitrile tow with a 10 to 150 denier thread; (b) stabilizing said tow by heating in an oxidizing atmosphere at a temperature between about 180° and about 400° C.; and (c) carbonizing the stabilized tow by heating.
Claim 3
Dependent Claim 66 words
In a process for the production of carbon fiber wherein a multifilament tow comprising a plurality of polyacrylonitrile fibers is oxidized by heating in an oxidizing atmosphere, then carbonized by heating at an elevated temperature for a time sufficient to carbonize an oxidized polyacrylonitrile fiber, the improvement comprising overwrapping said multifilament tow with at least one 10 to 150 denier thread prior to oxidizing the tow.
Claim 4
Dependent Claim 66 words
In a process for the production of carbon fiber wherein a multifilament tow comprising a plurality of polyacrylonitrile fibers is oxidized by heating in an oxidizing atmosphere, then carbonized by heating at an elevated temperature for a time sufficient to carbonize an oxidized polyacrylonitrile fiber, the improvement comprising overwrapping said multifilament tow with at least one 10 to 150 denier thread prior to oxidizing the tow.
Claim 5
Dependent Claim 15 words
The process of claim 2 wherein the thread is removed prior to the carbonizing step.
Claim 6
Dependent Claim 20 words
The process of claim 2 wherein the thread is selected from cellulosic thread, fiberglass thread, carbon thread and ceramic thread.
Claim 7
Dependent Claim 16 words
The process of claim 2 wherein the thread is oxidized and destroyed during the oxidizing step.

References Cited (Backward Citations)

US3775520A Cited
US3809673A Cited
US4237175A Cited
US4378343A Cited
US4501037A Cited
US4534919A Cited
JPS61113826A Cited

USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1992-08-28 1993-02-27 1993-08-29 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 1996-08-28 1997-02-27 1997-08-29 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 2000-08-28 2001-02-27 2001-08-29 $7700.00 Window Closed / Lapsed

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