US4854977A
Expired / Lapsed
US
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Process for treating titanium alloy parts for use as compressor disks in aircraft propulsion systems
Assignee: Compagnie Europeenne du Zirconium Cezus SA
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Filing: 1988-04-14
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Granted: 1989-08-08
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Expires: 2008-04-14
Abstract
Abstract The process according to the invention comprises the following stages: (a) an ingot of the following composition is produced (% by weight): Al 3.8 to 5.4, Sn 1.5 to 2.5, Zr 2.8 to 4.8, Mo 1.5 to 4.5, Cr<2.5 and Cr+V 1.5 to 4.5, Fe<2.0, Si<0.3, 0<0.15, the remainder being Ti and impurities; (b) the ingot undergoes hot working, comprising a rough-shaping and then a final working preceded by preheating in the beta range; (c) the blank of the part obtained is solid solution heat treated by maintaining it at a temperature 10 DEG to 40 DEG C. lower than its real "beta transus"; (d) ageing for 4 to 12 h at between 550 DEG and 650 DEG C. is then carried out on the blank of the part or the part itself. The invention also relates to the process and the parts obtained under preferred conditions, said parts having in particular a good mechanical strength (Rm and Rp0.2 respectively at least equal to 1200 and 1100 MPa), a good tenacity and a good creep resistance at 400 DEG C. (under 600 MPa, elongation of 0.5% in more than 200 h).
Inventors
- 👤 Edouard Alheritiere
- 👤 Bernard Prandi
Bibliographic Details
Application Number
—
Jurisdiction
US
Data Source
google_patents
Last Synchronized
2026-11-08 08:24
CPC Classifications
C; C22; C22C; C22C14/00; C22F; C22F1/00; C22F1/16; C22F1/18; C22F1/183
Claims Analysis
Total Claims: 15
Claim 1
Independent Claim
214 words
Process for the production of a titanium alloy part comprising the steps of: (a) producing an ingot of composition (% by weight): Al 3.8 to 5.4, Sn 1.5 to 2.5, Zr 2.8 to 4.8, Mo 1.5 to 4.5, Cr equal to or below 2.5 and Cr+V=1.5 to 4.5, Fe<2.0, Si<0.3, O<0.15, Ti and impurities constituting the remainder; (b) hot working the ingot including a rough-shaping working of said ingot giving a hot blank, experimentally determining the real beta transus temperature from a sample of the hot blank, and performing a final hot working of at least a portion of said blank starting at a temperature at lest 10° C. higher than said real beta transus temperature and ending at a temperature below said real beta transus temperature, all said final hot working taking place at ±60° C. of said real beta transus temperature, said final hot working giving a blank of the part; (c) solid solution heat treating the hot worked part blank, while maintaining said part blank at a temperature between said real beta transus -40° C. and said real beta transus -10° C., followed by cooling said part blank to ambient temperature; (d) ageing heat treating for 4 to 12 h at between 550° and 650° C. the product of step (c).
Claim 2
Dependent Claim
214 words
Process for the production of a titanium alloy part comprising the steps of: (a) producing an ingot of composition (% by weight): Al 3.8 to 5.4, Sn 1.5 to 2.5, Zr 2.8 to 4.8, Mo 1.5 to 4.5, Cr equal to or below 2.5 and Cr+V=1.5 to 4.5, Fe<2.0, Si<0.3, O<0.15, Ti and impurities constituting the remainder; (b) hot working the ingot including a rough-shaping working of said ingot giving a hot blank, experimentally determining the real beta transus temperature from a sample of the hot blank, and performing a final hot working of at least a portion of said blank starting at a temperature at lest 10° C. higher than said real beta transus temperature and ending at a temperature below said real beta transus temperature, all said final hot working taking place at ±60° C. of said real beta transus temperature, said final hot working giving a blank of the part; (c) solid solution heat treating the hot worked part blank, while maintaining said part blank at a temperature between said real beta transus -40° C. and said real beta transus -10° C., followed by cooling said part blank to ambient temperature; (d) ageing heat treating for 4 to 12 h at between 550° and 650° C. the product of step (c).
Claim 3
Dependent Claim
16 words
Process according to claim 1, wherein Al=4.5 to 5.4, Sn=1.8 to 2.5 and Zr=3.5 to 4.8.
Claim 4
Dependent Claim
7 words
Process according to claim 1, wherein Fe<1.5.
Claim 5
Dependent Claim
9 words
Process according to claim 1, wherein O=0.07 to 0.13.
Claim 6
Dependent Claim
53 words
Process according to claim 1, wherein the final hot working is carried out by starting at a temperature between the real beta transus +20° C. and the real beta transus +40° C. and is ended at a temperature below said beta transus and at least equal to the real beta transus -50° C.
Claim 7
Dependent Claim
10 words
Process according to claim 2, in which Zr=4.1 to 4.8.
Claim 8
Dependent Claim
29 words
Process according to claim 5, wherein the final hot working is concluded at a temperature between the real beta transus -10° C. and the real beta transus -40° C.
Claim 9
Dependent Claim
21 words
Process according to claim 7, wherein ageing is performed for between 6 and 10 hours at between 570° and 640° C.
Claim 10
Dependent Claim
16 words
Process according to claims 1, 2 or 6, wherein Mo=2.0 to 4.5 and Cr=1.5 to 2.5.
Claim 11
Dependent Claim
37 words
Process according to claim 1 or 2, wherein at least the end of the rough-shaping of the ingot takes place at a temperature between the real "beta transus" -100° C. and the real "beta transus" -20° C.
Claim 12
Dependent Claim
14 words
Process according to claim 1, 2, 6, 3 or 4, wherein Fe=0.7 to 1.5.
Claim 13
Dependent Claim
244 words
Process for the production of a titanium alloy part comprising the steps of: (a) producing an ingot of the following composition (% by weight): Al 4.5 to 5.4, Sn 1.8 to 2.5, Zr 3.5 to 4.8, Mo 2.0 to 4.5, Cr 1.5 to 2.5 and Cr+V=1.5 to 4.5, Fe 0.7 to 1.5, O 0.07 to 0.13 and Ti and impurities constitute the residue; (b) a rough-shaping of the ingot to give a final hot blank, where the end of the shaping at least comprises forging at a temprature between the real "beta transus" -100° C. and the real "beta transus" -20° C., the working ratio of said forging being at a minimum 1.5; (c) experimentally determining said real "beta transus" temperature of the alloy on the basis of samples taken from the forged hot blank; (d) performing a final working of said blank by forging and/or die forging, starting at a temperature between the real "beta transus" +20° C. and the real "beta transus" +40° C. and ending at a temperature between the real "beta transus" -40° C. and the real "beta transus" -10° C.; (e) solid solution heat treating the final worked blank, the temperature being maintained at between the real "beta transus" -40° C. and the real "beta transus" -10° C. and then cooling to ambient temperature; (f) performing an ageing heat treatment for 6 to 10 hours at a temperature between 580° and 630° C. on the product of step (e).
Claim 14
Dependent Claim
244 words
Process for the production of a titanium alloy part comprising the steps of: (a) producing an ingot of the following composition (% by weight): Al 4.5 to 5.4, Sn 1.8 to 2.5, Zr 3.5 to 4.8, Mo 2.0 to 4.5, Cr 1.5 to 2.5 and Cr+V=1.5 to 4.5, Fe 0.7 to 1.5, O 0.07 to 0.13 and Ti and impurities constitute the residue; (b) a rough-shaping of the ingot to give a final hot blank, where the end of the shaping at least comprises forging at a temprature between the real "beta transus" -100° C. and the real "beta transus" -20° C., the working ratio of said forging being at a minimum 1.5; (c) experimentally determining said real "beta transus" temperature of the alloy on the basis of samples taken from the forged hot blank; (d) performing a final working of said blank by forging and/or die forging, starting at a temperature between the real "beta transus" +20° C. and the real "beta transus" +40° C. and ending at a temperature between the real "beta transus" -40° C. and the real "beta transus" -10° C.; (e) solid solution heat treating the final worked blank, the temperature being maintained at between the real "beta transus" -40° C. and the real "beta transus" -10° C. and then cooling to ambient temperature; (f) performing an ageing heat treatment for 6 to 10 hours at a temperature between 580° and 630° C. on the product of step (e).
Claim 15
Dependent Claim
9 words
Process according to claim 12, wherein Zr=4.1 to 4.8.
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USPTO Annuity & Maintenance Windows
| Annuity Stage | Window Opens | Payment Deadline | Surcharge Period Until | Estimated Fee | Status |
|---|---|---|---|---|---|
| 3.5 Years (Year 4) | 1992-08-07 | 1993-02-06 | 1993-08-08 | $2000.00 | Window Closed / Lapsed |
| 7.5 Years (Year 8) | 1996-08-07 | 1997-02-06 | 1997-08-08 | $3760.00 | Window Closed / Lapsed |
| 11.5 Years (Year 12) | 2000-08-07 | 2001-02-06 | 2001-08-08 | $7700.00 | Window Closed / Lapsed |