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US4842625A Expired / Lapsed US ⏱️ 0.0 years remaining

Control method to maximize argon recovery from cryogenic air separation units

Assignee: Air Products and Chemicals Inc
•
Filing: 1988-04-29
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Granted: 1989-06-27
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Expires: 2008-04-29
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Abstract

Abstract The present invention relates to an improvement to a conventional cryogenic air separation process having an argon sidearm column. The improvement to the process comprises reducing the pressure of the feed gas to the argon sidearm column across a control valve and operating the argon sidearm column at the lowest possible pressure consistent with a minimum temperature difference across the overhead condenser and the unrestricted return of crude oxygen vapor from the overhead condenser to the low pressure column.

Inventors

  • 👤 Rodney J. Allam
  • 👤 Alan L. Prentice

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-10-31 11:34
CPC Classifications
F; F25; F25J; F25J3/00; F25J3/02; F25J3/04; F25J3/04763; F25J3/04769; F25J3/04793; F25J3/048; C; C01; C01B; C01B23/00; F25J3/04151; F25J3/04163; F25J3/04169; F25J3/04181; F25J3/04187; F25J3/04193; F25J3/04206; F25J3/04248; F25J3/04284; F25J3/04309; F25J3/04406; F25J3/04412; F25J3/04642; F25J3/04648; F25J3/04654; F25J3/04666; F25J3/04672; F25J3/04678; F25J3/04866; F25J3/04872; F25J3/04884; F25J2240/00; F25J2240/40; F25J2245/00; F25J2245/40; F25J2250/00; F25J2250/30; F25J2250/40; F25J2250/50; F25J2250/58; Y; Y10; Y10S; Y10S62/00; Y10S62/923; Y10S62/924

Claims Analysis

Total Claims: 6
Claim 1
Independent Claim 131 words
In a process for the separation of mixtures, which comprise oxygen, nitrogen, and argon, by cryogenic distillation in a distillation unit comprising an argon sidearm column with an overhead condenser and a low pressure column, wherein the argon sidearm column integrally communicates with the low pressure column, the improvement for increasing argon recovery comprises reducing the pressure of feed gas withdrawn from a lower-intermediate location of the low pressure column and fed to a lower location of the argon sidearm column whereby the operating pressure of the argon sidearm column is controlled at the lowest effective pressure which is consistent with a minimum temperature difference across the overhead condenser and an unrestricted return of crude oxygen vapor from the overhead condenser of the argon sidearm column to the low pressure column.
Claim 2
Dependent Claim 131 words
In a process for the separation of mixtures, which comprise oxygen, nitrogen, and argon, by cryogenic distillation in a distillation unit comprising an argon sidearm column with an overhead condenser and a low pressure column, wherein the argon sidearm column integrally communicates with the low pressure column, the improvement for increasing argon recovery comprises reducing the pressure of feed gas withdrawn from a lower-intermediate location of the low pressure column and fed to a lower location of the argon sidearm column whereby the operating pressure of the argon sidearm column is controlled at the lowest effective pressure which is consistent with a minimum temperature difference across the overhead condenser and an unrestricted return of crude oxygen vapor from the overhead condenser of the argon sidearm column to the low pressure column.
Claim 3
Dependent Claim 15 words
The process of claim 1 wherein the mixture comprising oxygen, nitrogen and argon is air.
Claim 4
Dependent Claim 18 words
The process of claim 1 wherein the low pressure column and argon sidearm column have structured packing internals.
Claim 5
Dependent Claim 18 words
The process of claim 1 wherein the low pressure column and argon sidearm column have distillation tray internals.
Claim 6
Dependent Claim 30 words
The process of claim 1 wherein the reduced pressure of the feed gas to the argon sidearm column is in the range from about 1.5 psig to about 15 psig.

USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1992-06-26 1992-12-26 1993-06-27 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 1996-06-26 1996-12-26 1997-06-27 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 2000-06-26 2000-12-26 2001-06-27 $7700.00 Window Closed / Lapsed

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