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US4835016A Expired / Lapsed US ⏱️ 0.0 years remaining

Adhesive bonding

Assignee: United States Department of the Army
•
Filing: 1988-03-28
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Granted: 1989-05-30
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Expires: 2008-03-28
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Abstract

Abstract A method of pretreating a polyolefin for adhesive bonding. The method involves contacting the polyolefin with a non-chromate solution such as either lead dioxide, potassium iodate or ammonia persulfate in a combination of water and sulfuric acid.

Inventors

  • 👤 Roberta Rosty
  • 👤 David W. Levi

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-11-05 18:42
CPC Classifications
C; C08; C08J; C08J7/00; C08J7/12; C08J7/14; C08J2323/00; C08J2323/02

Claims Analysis

Total Claims: 7
Claim 1
Independent Claim 82 words
In an improved method of preparing a polyolefin surface for adhesive bonding, the improvement consisting essentially of contacting said polyolefin surface with a non-chromate solution selected from the group consisting of solutions A, B, and C wherein: Solution A is in ratio of about: 6.3 grams lead dioxide, 12 grams water, and 82 mls sulfuric acid; Solution B is in ratio of about 5.5 grams potassium iodate, 12 grams water, 82 mls sulfuric acid; and Solution C is in ratio of about
Claim 2
Dependent Claim 82 words
In an improved method of preparing a polyolefin surface for adhesive bonding, the improvement consisting essentially of contacting said polyolefin surface with a non-chromate solution selected from the group consisting of solutions A, B, and C wherein: Solution A is in ratio of about: 6.3 grams lead dioxide, 12 grams water, and 82 mls sulfuric acid; Solution B is in ratio of about 5.5 grams potassium iodate, 12 grams water, 82 mls sulfuric acid; and Solution C is in ratio of about
Claim 3
Dependent Claim 8 words
4 gram ammonium persulfate 204.1 grams sulfuric acid.
Claim 4
Dependent Claim 8 words
4 gram ammonium persulfate 204.1 grams sulfuric acid.
Claim 5
Dependent Claim 25 words
The method of claim 1 wherein said solution consists in ratio of about 6.3 g. lead dioxide, 12 g. water, and 82 mls sulfuric acid.
Claim 6
Dependent Claim 25 words
The method of claim 1 wherein said solution consists in ratio of about 5.5 g. potassium iodate, 12 g. water, and 82 mls sulfuric acid.
Claim 7
Dependent Claim 22 words
The method of claim 1 wherein said solution consists in ratio of about 4.4 g. ammonium persulfate, and 204.1 g. sulfuric acid.

References Cited (Backward Citations)

US3235426A Cited
US3553085A Cited
US4086128A Cited
US4386175A Cited
US4448811A Cited

USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1992-05-29 1992-11-28 1993-05-30 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 1996-05-29 1996-11-28 1997-05-30 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 2000-05-29 2000-11-28 2001-05-30 $7700.00 Window Closed / Lapsed

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