US4801702A
Expired / Lapsed
US
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Process for the preparation and conditioning or organic pigments
Assignee: BASF Corp
•
Filing: 1986-10-30
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Granted: 1989-01-31
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Expires: 2006-10-30
Abstract
Abstract A process for the preparation and conditioning of organic pigments, which comprises the use of at least one tricyclodecane alcohol or tricyclodecene alcohol.
Inventors
- 👤 Fridolin Babler
Bibliographic Details
Application Number
—
Jurisdiction
US
Data Source
google_patents
Last Synchronized
2026-11-01 17:07
CPC Classifications
C; C09; C09B; C09B67/00; C09B67/0001; C09B25/00; C09B47/00; C09B47/04; C09B47/06; C09B67/0002; C09B67/0014; C09B67/0022
Claims Analysis
Total Claims: 17
Claim 1
Independent Claim
106 words
An improved process for the synthesis and concomitant conditioning of an organic pigment selected from the group consisting of the diketopyrrolopyrrole, perylene, quinacridone, phthalocyanine, perinone, quinophthalone, isoindolinone, isoindoline, dioxazine, anthraquinone, thioindigo, methine, azomethine and azo pigments and the metal salts or complexes of the azomethine, methine, azo and phthalocyanine pigments, wherein the improvement comprises carrying out the synthesis and concomitant conditioning of said pigment in the presence of a tricyclic alcohol which is 8(9)-hydroxytricyclo[5.2.1.0 2 ,6 ]dec-3-ene or which has the formula ##STR3## wherein n is 0 or 1, and X is hydrogen or the --CH 2 OH group; or a mixture of said tricyclic alcohols.
Claim 2
Dependent Claim
106 words
An improved process for the synthesis and concomitant conditioning of an organic pigment selected from the group consisting of the diketopyrrolopyrrole, perylene, quinacridone, phthalocyanine, perinone, quinophthalone, isoindolinone, isoindoline, dioxazine, anthraquinone, thioindigo, methine, azomethine and azo pigments and the metal salts or complexes of the azomethine, methine, azo and phthalocyanine pigments, wherein the improvement comprises carrying out the synthesis and concomitant conditioning of said pigment in the presence of a tricyclic alcohol which is 8(9)-hydroxytricyclo[5.2.1.0 2 ,6 ]dec-3-ene or which has the formula ##STR3## wherein n is 0 or 1, and X is hydrogen or the --CH 2 OH group; or a mixture of said tricyclic alcohols.
Claim 3
Dependent Claim
28 words
A process according to claim 1 wherein the organic pigment is selected from the group consisting of the anthraquinone, perylene, perinone, quinacridone, dioxazine, metal phthalocyanine and azo pigments.
Claim 4
Dependent Claim
18 words
A process according to claim 1, wherein the organic pigment is a metal phthalocyanine or an azo pigment.
Claim 5
Dependent Claim
28 words
A process according to claim 1, wherein the conditioning takes the form of a grinding procedure in the presence of small amounts of at least one tricyclic alcohol.
Claim 6
Dependent Claim
26 words
A process according to claim 4, wherein the amount of tricyclic alcohol is from 0.05 to 25% by weight, based on the pigment to be ground.
Claim 7
Dependent Claim
28 words
A process according to claim 1, wherein the tricyclodecane alcohol is 3(4),8(9)-bis(hydroxymethyl)tricyclo[5.2.1.0 2 ,6 ]decane, 8(9)-hydroxy-tricyclo[5.2.1.0 2 ,6 ]decane, 8(9)-hydroxymethyltricyclo[5.2.1.0 2 ,6 ]decane or 3(4)-hydroxymethyltricyclo[5.2.1.0 2 ,6 ]decane.
Claim 8
Dependent Claim
15 words
A process according to claim 6, wherein the tricyclodecane alcohol is 8(9)-hydroxymethyltricyclo[5.2.1.0 2 ,6 ]decane.
Claim 9
Dependent Claim
95 words
A process for the conditioning of an organic pigment selected from the group consisting of the diketopyrrolopyrrole, perylene, quinacridone, phthalocyanine, perinone, quinophthalone, isoindolinone, isoindoline, dioxazine, anthraquinone, thioindigo, methine, azomethine and azo pigments and the metal salts or complexes of the azomethine, methine, azo and phthalocyanine pigments which comprises conditioning the preformed crude pigment in the presence of a tricyclic alcohol which is 8(9)-hydroxytricyclo[5.2.1.0 2 ,6 ]dec-3-ene or which has the formula ##STR4## wherein n is 0 to 1, and X is hydrogen or the --CH 2 OH group; or a mixture of said tricyclic alcohols.
Claim 10
Dependent Claim
95 words
A process for the conditioning of an organic pigment selected from the group consisting of the diketopyrrolopyrrole, perylene, quinacridone, phthalocyanine, perinone, quinophthalone, isoindolinone, isoindoline, dioxazine, anthraquinone, thioindigo, methine, azomethine and azo pigments and the metal salts or complexes of the azomethine, methine, azo and phthalocyanine pigments which comprises conditioning the preformed crude pigment in the presence of a tricyclic alcohol which is 8(9)-hydroxytricyclo[5.2.1.0 2 ,6 ]dec-3-ene or which has the formula ##STR4## wherein n is 0 to 1, and X is hydrogen or the --CH 2 OH group; or a mixture of said tricyclic alcohols.
Claim 11
Dependent Claim
24 words
A process according to claim 8 wherein the organic pigment is selected from the group consisting of the diketopyrrolopyrrole, perylene, quinacridone and isoindolinone pigments.
Claim 12
Dependent Claim
27 words
A process according to claim 8 wherein conditioning takes the form of a grinding procedure in the presence of small amounts of at least one tricyclic alcohol.
Claim 13
Dependent Claim
26 words
A process according to claim 10 wherein the amount of tricyclic alcohol is from 0.05 to 25% by weight, based on the pigment to be ground.
Claim 14
Dependent Claim
14 words
A process according to claim 10 wherein the grinding procedure is a dry grinding.
Claim 15
Dependent Claim
14 words
A process according to claim 10 wherein the grinding procedure is a wet grinding.
Claim 16
Dependent Claim
24 words
A process according to claim 8, wherein the tricyclodecane alcohol is 3(4),8(9)-bis(hydroxymethyl)tricyclo[5.2.1.0 2 ,6 ]decane, 8(9)-hydroxytricyclo[5.2.1.0 2 ,6 ]decane or 3(4)-hydroxymethyltricyclo[5.2.1.0 2 ,6 ]decane.
Claim 17
Dependent Claim
15 words
A process according to claim 14, wherein the tricyclodecane alcohol is 8(9)-hydroxymethyltricyclo[5.2.1.0 2 ,6 ]decane.
References Cited (Backward Citations)
USPTO Annuity & Maintenance Windows
| Annuity Stage | Window Opens | Payment Deadline | Surcharge Period Until | Estimated Fee | Status |
|---|---|---|---|---|---|
| 3.5 Years (Year 4) | 1992-01-31 | 1992-08-01 | 1993-01-31 | $2000.00 | Window Closed / Lapsed |
| 7.5 Years (Year 8) | 1996-01-31 | 1996-08-01 | 1997-01-31 | $3760.00 | Window Closed / Lapsed |
| 11.5 Years (Year 12) | 2000-01-31 | 2000-08-01 | 2001-01-31 | $7700.00 | Window Closed / Lapsed |