US4788052A
Expired / Lapsed
US
⏱️ 0.0 years remaining
Stable hydrogen peroxide dental gel containing fumed silicas
Assignee: Colgate Palmolive Co
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Filing: 1987-04-17
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Granted: 1988-11-29
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Expires: 2007-04-17
Abstract
Abstract A stable aqueous hydrogen peroxide gel dentifrice for oral anti-gingivitis application having an acid pH of about 3-6 comprising a combination of hydrophilic and hydrophobic fumed silica gelling agent, hydrogen peroxide, about 20-40% by weight of a polyethylene glycol humectant, flavor, sweetening agent, sodium benzoate, and a nonionic surfactant as the essential ingredients, prepared by a process which comprises controlling the order of addition of the essential ingredients. Distilled (deionized) water is preferred in the formulation to prevent minimal contamination.
Inventors
- 👤 Shirley M. Ng
- 👤 Denise-Marie DiTomasso
Bibliographic Details
Application Number
—
Jurisdiction
US
Data Source
google_patents
Last Synchronized
2026-10-26 19:00
CPC Classifications
A; A61; A61K; A61K8/00; A61K8/02; A61K8/04; A61K8/042; A61K8/18; A61K8/19; A61K8/22; A61K8/25; A61K8/30; A61K8/33; A61K8/39; A61Q; A61Q11/00
Claims Analysis
Total Claims: 8
Claim 1
Independent Claim
164 words
A cosmetic and chemically stable aqueous hydrogen peroxide dental gel having a pH between about 3-6, comprising hydrogen peroxide as the sole chemically active agent in an amount of 1.5-3.5% by weight, a combination of hydrophilic and hydrophobic fumed silica gelling agent, about 20-40% by weight of a polyethylene glycol humectant, a nonionic surfactant, a sweetener, sodium benzoate and a flavor prepared by homogenizing the fumed silicas in the polyethylene glycol and water phases and the sequential addition of the premixed homogenized hydrophobic fumed silica in the polyethylene glycol (Phase A) to the premixed homogenized hydrophilic fumed silica in water containing hydrogen peroxide (Phase B) and mixing for about 30 minutes while maintaining the temperature at room temperature, adding the predissolved sodium saccharin and sodium benzoate in water (Phase C) with mixing which effects immediate gellation, adding the pre-solubilized flavor in the nonionic surfactant and water (Phase D) and mixing for about 5-10 minutes until a clear, homogeneous rigid stable dental gel is obtained.
Claim 2
Dependent Claim
164 words
A cosmetic and chemically stable aqueous hydrogen peroxide dental gel having a pH between about 3-6, comprising hydrogen peroxide as the sole chemically active agent in an amount of 1.5-3.5% by weight, a combination of hydrophilic and hydrophobic fumed silica gelling agent, about 20-40% by weight of a polyethylene glycol humectant, a nonionic surfactant, a sweetener, sodium benzoate and a flavor prepared by homogenizing the fumed silicas in the polyethylene glycol and water phases and the sequential addition of the premixed homogenized hydrophobic fumed silica in the polyethylene glycol (Phase A) to the premixed homogenized hydrophilic fumed silica in water containing hydrogen peroxide (Phase B) and mixing for about 30 minutes while maintaining the temperature at room temperature, adding the predissolved sodium saccharin and sodium benzoate in water (Phase C) with mixing which effects immediate gellation, adding the pre-solubilized flavor in the nonionic surfactant and water (Phase D) and mixing for about 5-10 minutes until a clear, homogeneous rigid stable dental gel is obtained.
Claim 3
Dependent Claim
18 words
The dental gel according to claim 1, wherein the pH is adjusted to about 4.5-5 with an acid.
Claim 4
Dependent Claim
34 words
The dental gel according to claim 1, wherein the hydrophilic fumed silica constitutes about 8 to 10% by weight and the hydrophilic fumed silica constitutes about 0.1 to 1.5% by weight of the composition.
Claim 5
Dependent Claim
18 words
The dental gel according to claim 1, wherein the polyethylene glycol humectant has a molecular weight of 600.
Claim 6
Dependent Claim
34 words
The dental gel according to claim 1 wherein the nonionic surfactant is a polyoxyethylene monoester or sorbitol with a C 10 to C 18 fatty acid in an amount of about 0.5-3% by weight.
Claim 7
Dependent Claim
17 words
The dental gel according to claim 1, wherein the sodium benzoate constitutes 0.35 to 0.5% by weight.
Claim 8
Dependent Claim
23 words
The dental gel according to claim 1, wherein the sweetening agent is sodium saccharine and the nonionic surfactant is polyethylene (20) sorbitan monolaurate.
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USPTO Annuity & Maintenance Windows
| Annuity Stage | Window Opens | Payment Deadline | Surcharge Period Until | Estimated Fee | Status |
|---|---|---|---|---|---|
| 3.5 Years (Year 4) | 1991-11-29 | 1992-05-30 | 1992-11-29 | $2000.00 | Window Closed / Lapsed |
| 7.5 Years (Year 8) | 1995-11-29 | 1996-05-30 | 1996-11-29 | $3760.00 | Window Closed / Lapsed |
| 11.5 Years (Year 12) | 1999-11-29 | 2000-05-30 | 2000-11-29 | $7700.00 | Window Closed / Lapsed |