US4767433A
Expired / Lapsed
US
⏱️ 0.0 years remaining
Spherical silica glass powder particles and process for their production
Assignee: AGC Inc
•
Filing: 1987-05-20
•
Granted: 1988-08-30
•
Expires: 2007-05-20
Abstract
Abstract A spherical silica glass powder particle having projections of network pattern on its surface is produced by gel-route formation.
Inventors
- 👤 Jun-ichi Iura
- 👤 Toshiyasu Kawaguchi
Bibliographic Details
Application Number
—
Jurisdiction
US
Data Source
google_patents
Last Synchronized
2026-11-01 18:06
CPC Classifications
C; C03; C03B; C03B19/00; C03B19/10; C03B19/1005; C03B19/106; C03B19/1065; C03C; C03C11/00; Y; Y10; Y10S; Y10S65/00; Y10S65/901
Claims Analysis
Total Claims: 8
Claim 1
Independent Claim
121 words
A process for producing spherical silica glass powder particles having projections of network pattern on their surface, which comprises hydrolyzing a silicon alkoxide with water in an amount of from 0.7 to 1.3 mols of water per mol of the silicon alkoxide in the presence of an acid and an alcohol, to form a sol of a partially condensed product of the silicon alkoxide; removing the alcohol from the sol to obtain a water-insoluble partially condensed product of the silicon alkoxide; dispersing the water-insoluble partially condensed product in water; treating the dispersion with a gelling agent to precipitate silica gel; and baking the precipitated silica gel for sufficient time and at sufficient temperature to thereby provide said spherical glass powder particles.
Claim 2
Dependent Claim
121 words
A process for producing spherical silica glass powder particles having projections of network pattern on their surface, which comprises hydrolyzing a silicon alkoxide with water in an amount of from 0.7 to 1.3 mols of water per mol of the silicon alkoxide in the presence of an acid and an alcohol, to form a sol of a partially condensed product of the silicon alkoxide; removing the alcohol from the sol to obtain a water-insoluble partially condensed product of the silicon alkoxide; dispersing the water-insoluble partially condensed product in water; treating the dispersion with a gelling agent to precipitate silica gel; and baking the precipitated silica gel for sufficient time and at sufficient temperature to thereby provide said spherical glass powder particles.
Claim 3
Dependent Claim
33 words
The process according to claim 1, wherein the silicon alkoxide and the alcohol have the same alkyl group which is a methyl group, an ethyl group, a propyl group or a butyl group.
Claim 4
Dependent Claim
36 words
The process according to claim 2, wherein the acid is hydrochloric acid, nitric acid, sulfuric acid, and is used in an amount of from 10 -3 to 10 -2 mol per mol of the silicon alkoxide.
Claim 5
Dependent Claim
29 words
The process according to claim 1, wherein the sol is heated at a temperature of not higher than 100° C. to remove the water, the alcohol and the acid.
Claim 6
Dependent Claim
43 words
The proccss according to claim 1, wherein the amount of water in which the water-insoluble partially condensed product of the silicon alkoxide is dispersed, is from 3 to 8 times by volume the amount of the partially condensed product of the silicon alkoxide.
Claim 7
Dependent Claim
19 words
The process according to claim 1, wherein the gelling agent is concentrated aqueous ammonia, ammonia gas or ammonium hydrogencarbonate.
Claim 8
Dependent Claim
21 words
The process according to claim 1, wherein the precipitated silica gel is washed with water and an acid, and then baked.
References Cited (Backward Citations)
USPTO Annuity & Maintenance Windows
| Annuity Stage | Window Opens | Payment Deadline | Surcharge Period Until | Estimated Fee | Status |
|---|---|---|---|---|---|
| 3.5 Years (Year 4) | 1991-08-30 | 1992-02-29 | 1992-08-30 | $2000.00 | Window Closed / Lapsed |
| 7.5 Years (Year 8) | 1995-08-30 | 1996-02-29 | 1996-08-30 | $3760.00 | Window Closed / Lapsed |
| 11.5 Years (Year 12) | 1999-08-30 | 2000-02-29 | 2000-08-30 | $7700.00 | Window Closed / Lapsed |