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US4760133A Expired / Lapsed US ⏱️ 0.0 years remaining

Process for preparing disazo dyes with bis-anilino methane coupling component

Assignee: Mitsubishi Chemical Corp
•
Filing: 1983-01-14
•
Granted: 1988-07-26
•
Expires: 2003-01-14
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Abstract

Abstract A process for preparing a disazo dye represented by the following formula: <IMAGE> wherein R1 and R2 each represents a hydrogen atom, a halogen atom, a nitro group, a trifluoromethyl group, a lower alkoxycarbonyl group or a lower alkylsulfonyl group, R3 represents a lower alkyl or allyl group which may optionally have a substituent or substituents, and R4 represents a lower alkyl or allyl group having a substituent or substituents, which comprises diazotizing an amine represented by the following formula: <IMAGE> wherein R1 and R2 are the same as defined above, and coupling the diazotized product with a bis(N,N-di-substituted anilino)methane represented by the following formula: <IMAGE> wherein R3 and R4 are the same as defined above.

Inventors

  • 👤 Toshio Niwa
  • 👤 Kiyoshi Himeno
  • 👤 Shuichi Maeda
  • 👤 Yukiharu Shimizu

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-11-08 16:26
CPC Classifications
C; C09; C09B; C09B31/00; C09B31/02; C09B31/04; C09B31/043

Claims Analysis

Total Claims: 2
Claim 1
Independent Claim 131 words
A process for preparing a disazo dye represented by the following formula: ##STR43## wherein R 1 and R 2 each represents hydrogen, halogen, nitro, trifluoromethyl, lower alkoxycarbonyl or lower alkylsulfonyl, R 3 represents lower alkyl or allyl or substituted lower alkyl or allyl, and R 4 represents substituted lower alkyl or allyl, said substituent in R 3 and R 4 being selected from the group consisting of hydroxy, lower alkoxy, phenoxy, lower alkanoyloxy, lower alkoxycarbonyloxy, lower alkoxycarbonyl, cyano, phenyl and tetrahydrofuryl, which comprises diazotizing an amine represented by the following formula: ##STR44## wherein R 1 and R 2 are the same as defined above, and coupling the diazotized product with a bis(N,N-disubstituted anilino)methane represented by the following formula: ##STR45## wherein R 3 and R 4 are the same as defined above.
Claim 2
Dependent Claim 131 words
A process for preparing a disazo dye represented by the following formula: ##STR43## wherein R 1 and R 2 each represents hydrogen, halogen, nitro, trifluoromethyl, lower alkoxycarbonyl or lower alkylsulfonyl, R 3 represents lower alkyl or allyl or substituted lower alkyl or allyl, and R 4 represents substituted lower alkyl or allyl, said substituent in R 3 and R 4 being selected from the group consisting of hydroxy, lower alkoxy, phenoxy, lower alkanoyloxy, lower alkoxycarbonyloxy, lower alkoxycarbonyl, cyano, phenyl and tetrahydrofuryl, which comprises diazotizing an amine represented by the following formula: ##STR44## wherein R 1 and R 2 are the same as defined above, and coupling the diazotized product with a bis(N,N-disubstituted anilino)methane represented by the following formula: ##STR45## wherein R 3 and R 4 are the same as defined above.

References Cited (Backward Citations)

US989953A Cited
US4180503A Cited
US4207233A Cited

USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1991-07-26 1992-01-25 1992-07-26 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 1995-07-26 1996-01-25 1996-07-26 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 1999-07-26 2000-01-25 2000-07-26 $7700.00 Window Closed / Lapsed

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