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US4725390A Expired / Lapsed US ⏱️ 0.0 years remaining

Process for making ceramic spheroids

Assignee: Kinetico Inc
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Filing: 1986-06-13
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Granted: 1988-02-16
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Expires: 2006-06-13
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Abstract

Abstract A process for making ceramic spheriods by mixing and converting spheroids, with the aid of water, raw materials of 50-99.8 parts by weight mineral particulate (e.g. blend of orthoclase, nepheline, hornblende and diopside) which particulate includes at least one mineral having chemically bound water or sulphur in a form which is not substantially water soluble and in amounts sufficient to yield 0.5 to 5 weight percent water or 0.04 to 2 weight percent sulphur in the total mass; 0.1 to 50 parts by weight silicon carbide; and 0.1 to 15 parts binder. The wet spheroids are dried and the dry spheroids are fired in contact with a parting agent (e.g. aluminum oxide) for a sufficiently long time to form a shell containing parting agent on the ceramic mineral having a fired density of less than about 2.9 grams per cubic centimeter when fired above 1,100° C. The binder is typically bentonite clay.

Inventors

  • 👤 James A. Laird
  • 👤 Warren R. Beck

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-11-03 05:12
CPC Classifications
B; B01; B01J; B01J19/00; B01J19/30; B01D; B01D39/00; B01D39/02; B01D39/06; C; C04; C04B; C04B20/00; C04B20/02; C04B20/04; C04B20/06; C04B20/068; C09; C09K; C09K8/00; C09K8/60; C09K8/80; E; E21; E21B; E21B43/00; E21B43/25; E21B43/26; E21B43/267

Claims Analysis

Total Claims: 5
Claim 1
Independent Claim 211 words
A process of making ceramic spheroids comprising the following steps: (a) mixing and converting to spheroids, with the aid of water, raw materials comprising: 50 to 99.8 parts by weight of a mineral particulate comprising a ceramic mineral which has a fired density of less than about 2.9 grams per cubic centimeter when fired above about 1100° C. and includes at least one mineral having chemically bound water or sulfur, in a form which is not substantially water soluble, in amounts sufficient to yield 0.5 to 5.0 weight percent water or 0.04 to 2.0 weight percent sulfur in the total mass of mineral particulates; 0.1 to 50 parts by weight silicon carbide; and 0.1 to 15 parts by weight binder characterized by adhering the raw materials together into unified masses after their conversion to spheroids but before firing; (b) drying the wet spheroids from step (a); and (c) firing the dry spheroids from step (b), in contact with a parting agent comprising a particulate selected from aluminum oxide, magnesium oxide, and their precursors, at a sufficiently high temperature and for a sufficiently long time to form a shell, containing parting agent, on the ceramic spheroids, said fired ceramic spheroids having a fired density less then about 2.2 grams per cubic centimeter.
Claim 2
Dependent Claim 211 words
A process of making ceramic spheroids comprising the following steps: (a) mixing and converting to spheroids, with the aid of water, raw materials comprising: 50 to 99.8 parts by weight of a mineral particulate comprising a ceramic mineral which has a fired density of less than about 2.9 grams per cubic centimeter when fired above about 1100° C. and includes at least one mineral having chemically bound water or sulfur, in a form which is not substantially water soluble, in amounts sufficient to yield 0.5 to 5.0 weight percent water or 0.04 to 2.0 weight percent sulfur in the total mass of mineral particulates; 0.1 to 50 parts by weight silicon carbide; and 0.1 to 15 parts by weight binder characterized by adhering the raw materials together into unified masses after their conversion to spheroids but before firing; (b) drying the wet spheroids from step (a); and (c) firing the dry spheroids from step (b), in contact with a parting agent comprising a particulate selected from aluminum oxide, magnesium oxide, and their precursors, at a sufficiently high temperature and for a sufficiently long time to form a shell, containing parting agent, on the ceramic spheroids, said fired ceramic spheroids having a fired density less then about 2.2 grams per cubic centimeter.
Claim 3
Dependent Claim 45 words
The process of claim 1 wherein the mineral particulate is selected from the group consisting of: perlite; mixtures of orthoclase, nepheline, hornblende, and diopside; and mixtures of plagioclase and orthoclase feldspar containing at least one mineral selected from apatite, hornblende, biotite, pyrite, perlite, and vermiculite.
Claim 4
Dependent Claim 24 words
The process of claim 1 wherein the binder is selected from the group consisting of bentonite, cellulose gum, starch, polyvinylalcohol, polyvinylacetate, and sodium lignosulphonate.
Claim 5
Dependent Claim 13 words
The process of claim 1 wherein the firing temperature is above 1100° C.

References Cited (Backward Citations)

US2123536A Cited
US3657847A Cited
US3690622A Cited
US3666506A Cited
GB2090275A Cited
US4502983A Cited

USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1991-02-15 1991-08-17 1992-02-16 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 1995-02-15 1995-08-17 1996-02-16 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 1999-02-15 1999-08-17 2000-02-16 $7700.00 Window Closed / Lapsed

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